Process for separating soap from black liquor
    49.
    发明授权
    Process for separating soap from black liquor 失效
    将皂与黑液分离的方法

    公开(公告)号:US4022653A

    公开(公告)日:1977-05-10

    申请号:US618396

    申请日:1975-10-01

    申请人: Hong H. Lee

    发明人: Hong H. Lee

    IPC分类号: B03D1/14 C11B13/00 D21C11/00

    摘要: Soap is separated from spent, cellulosic pulping liquor by strenuously percolating a gaseous, aliphatic hydrocarbon through a quantity of liquor volume under such temperature and pressure conditions that an equilibrious strata of liquid phase hydrocarbon is sustained on the surface of the liquor. Following strenuous combination and agitation, the gas-liquor mixture is allowed to settle so that the entrained, gaseous hydrocarbon and coagulated soap floc gravimetrically rises to the liquor surface and stratifies with the soap layer between the residual liquor solution and a liquid phase layer of hydrocarbon. Thereafter, the liquid hydrocarbon and soap layer are decanted away from the residual liquor solution and depressurized to vaporize the hydrocarbon leaving a reservoir of isolated soap.

    摘要翻译: 将肥皂与废纤维素制浆液分离,在这样的温度和压力条件下,通过在液体表面上维持平衡的液相烃层,将气态脂族烃剧烈地渗透一定量的液体体积。 在剧烈的组合和搅拌之后,使气液混合物沉降,使得夹带的气态烃和凝结的皂絮体重力地升高到液体表面,并与残留液体和液相层之间的皂层分层 。 此后,将液体烃和皂层从剩余液体溶液中倾析出并减压以蒸发出离开皂的储存器的烃。

    Freeze concentration recovery process for wood pulping
    50.
    发明授权
    Freeze concentration recovery process for wood pulping 失效
    冷冻浓缩回收方法

    公开(公告)号:US3987641A

    公开(公告)日:1976-10-26

    申请号:US546423

    申请日:1975-02-03

    申请人: Hong H. Lee

    发明人: Hong H. Lee

    IPC分类号: B01D9/04 D21C11/00 F26B5/14

    摘要: Pulping liquor borne solids are concentrated within an aqueous solution by a successive plurality of freezing steps wherein a discrete quantity of the solution is crystallized in each step by freezing. The water crystals from each freezing step are subsequently separated from the remaining liquid solution by screening and applying axial pressure to the crystalline mass. Greater efficiencies may be obtained in some cases by mixing or reslurrying a pressed, crystalline mass and pressing a second time. Another auxiliary separation step comprises a quiescent thaw of the crystalline mass from the first two press steps to permit additional dissolved solids to be drained away from the purified water ice.