Narrowing of poly (tetramethylene ether) glycol
    41.
    发明授权
    Narrowing of poly (tetramethylene ether) glycol 有权
    聚(四亚甲基醚)二醇缩窄

    公开(公告)号:US06355846B1

    公开(公告)日:2002-03-12

    申请号:US09690650

    申请日:2000-10-17

    CPC classification number: C08G65/10 C07C41/42 C08G65/20 C07C43/11

    Abstract: A process for producing a poly(tetramethylene ether) glycol (PTMEG) or copolymer having a narrowed molecular weight ratio of 1.9 to 2.07 and a dispersity of 1.2 to 1.65 from a starting PTMEG or copolymer with a broader molecular weight distribution having a dispersity of 1.9 to 2.3 and a molecular weight ratio of 2.3 to 2.6 is provided by feeding the PTMEG or copolymer and an effective amount of an inert solvent to a stripping apparatus and stripping at a temperature of 150 to 220 degrees C. and a pressure of 0.5 to 5 mm of mercury.

    Abstract translation: 从具有分散度为1.9的较宽分子量分布的起始PTMEG或共聚物制备分子量分数为1.9至2.07的分子量分布为1.9至2.07的聚四亚甲基醚二醇(PTMEG)或共聚物的分散度为1.2至1.65的方法 通过将PTMEG或共聚物和有效量的惰性溶剂进料至汽提装置并在150-220℃的温度和0.5至5的压力下汽提来提供2.3至2.6的分子量比 毫米汞柱。

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