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    Azo dyes with a diazo component of the 3-amino thiophene series and a coupling component of the pyridine, pyridone or pyrazole series
    61.
    发明授权
    Azo dyes with a diazo component of the 3-amino thiophene series and a coupling component of the pyridine, pyridone or pyrazole series 失效
    具有3-氨基噻吩系列的重氮组分的偶氮染料和吡啶，吡啶酮或吡唑系的偶联组分

    公开(公告)号：US4994564A

    公开(公告)日：1991-02-19

    申请号：US269646

    申请日：1988-11-10

    申请人： Karl-Heinz Etzbach ,  Helmut Reichelt ,  Guenter Hansen ,  Ernst Schefczik ,  Helmut Hagen ,  Gunther Lamm

    发明人： Karl-Heinz Etzbach ,  Helmut Reichelt ,  Guenter Hansen ,  Ernst Schefczik ,  Helmut Hagen ,  Gunther Lamm

    IPC分类号： C09B29/09 ,  C09B29/00 ,  C09B29/42 ,  C09B29/48

    CPC分类号： C09B29/0059 ,  C09B29/3621 ,  C09B29/3634 ,  C09B29/3656

    摘要： Thien-3-ylazo dyes of the formula: ##STR1## where X is cyano, nitro, C.sub.1 -C.sub.6 -alkanoyl, substituted or unsubstituted benzoyl, substituted or unsubstituted phenyl or the radical COOR.sup.1 or CONR.sup.1 R.sup.2 where R.sup.1 and R.sup.2 are identical or different and each is independently of each other substituted or unsubstituted C.sub.1 -C.sub.8 -alkyl, C.sub.5 -C.sub.7 -cycloalkyl, C.sub.3 -C.sub.4 -alkenyl, substituted or unsubstituted phenyl or together with the nitrogen atom linking them a 5- or 6-membered saturated heterocyclic radical, and R.sup.2 may additionally be hydrogen, Y is hydrogen, cyano, C.sub.1 -C.sub.6 -alkanoyl, substituted or unsubstituted benzoyl, C.sub.1 -C.sub.4 -alkylsulfonyl, substituted or unsubstituted phenylsulfonyl, substituted or unsubstituted phenyl or the radical COOR.sup.1 or CONR.sup.1 R.sup.2 where R.sup.1 and R.sup.2 are each as defined above, Z is hydrogen, substituted or unsubstituted C.sub.1 -C.sub.8 -alkyl, substituted or unsubstituted phenyl, substituted or unsubstituted C.sub.1 -C.sub.6 -alkylthio, substituted or unsubstituted phenylthio, substituted or unsubstituted C.sub.1 -C.sub.6 -alkylsulfonyl or phenylsulfonyl or together with the radical Y a fused benzo ring which may be substituted, and K is the radical of a coupling component of the 2,6-diaminopyridine, 6-hydroxypyrid-2-one or 5-aminopyrazole series, are used for dyeing synthetic fiber materials, in particular synthetic polyesters, in yellow to red shades and are notable for good light fastness, fastness to dry heat setting and pleating and for good affinity.

    摘要翻译： 噻吩-3-基偶氮染料，其结构式如下：其中X为氰基，硝基，C 1 -C 6烷酰基，取代或未取代的苯甲酰基，取代或未取代的苯基或基团COOR1或CONR1R2，其中R 1和R 2相同或不同， 各自独立地为取代或未取代的C 1 -C 8 - 烷基，C 5 -C 7 - 环烷基，C 3 -C 4 - 烯基，取代或未取代的苯基或与连接它们的氮原子一起形成5-或6-元饱和杂环基， R 2可另外为氢，Y为氢，氰基，C 1 -C 6烷酰基，取代或未取代的苯甲酰基，C 1 -C 4 - 烷基磺酰基，取代或未取代的苯基磺酰基，取代或未取代的苯基或基团COOR1或CONR1R2，其中R1和R2为 Z是氢，取代或未取代的C 1 -C 8 - 烷基，取代或未取代的苯基，取代或未取代的C 1 -C 6 - 烷硫基，取代或未取代的苯硫基，取代或未取代的C 1 -C 6 - 烷基磺酰基 或与苯基磺酰基或与基团Y一起可以被取代的稠合苯并环，K是2,6-二氨基吡啶，6-羟基吡啶-2-酮或5-氨基吡唑系列的偶联组分的基团 用于将合成纤维材料，特别是合成聚酯染色为黄色至红色，并且具有良好的耐光性，耐干燥定型和打褶的牢度以及良好的亲和力。

    Method of using 1,2-benzisothiazoles
    65.
    发明授权
    Method of using 1,2-benzisothiazoles 失效
    使用1,2-苯并异噻唑的方法

    公开(公告)号：US4277477A

    公开(公告)日：1981-07-07

    申请号：US81059

    申请日：1979-10-02

    申请人： Helmut Hagen ,  Rolf-Dieter Kohler ,  Juergen Markert

    发明人： Helmut Hagen ,  Rolf-Dieter Kohler ,  Juergen Markert

    IPC分类号： C07D275/04

    CPC分类号： C07D275/04 ,  Y10S514/821

    摘要： Novel 1,2-benzisothiazoles and a process for the manufacture of 1,2-benzisothiazoles by reacting o-haloaryl ketones with ammonia and elementary sulfur. The compounds are starting materials for the manufacture of dyes, crop protection agents and drugs.

    摘要翻译： 新的1,2-苯并异噻唑和通过邻卤代芳基酮与氨和基本硫反应制备1,2-苯并异噻唑的方法。 这些化合物是用于制造染料，作物保护剂和药物的起始原料。

    2-Substituted-1-alkyl-nitroimidazoles
    66.
    发明授权
    2-Substituted-1-alkyl-nitroimidazoles 失效
    2-取代的-1-烷基 - 硝基咪唑

    公开(公告)号：US4232165A

    公开(公告)日：1980-11-04

    申请号：US38175

    申请日：1979-05-11

    申请人： Helmut Hagen ,  Rolf-Dieter Kohler

    发明人： Helmut Hagen ,  Rolf-Dieter Kohler

    IPC分类号： C07D233/92 ,  C07D233/93 ,  C07D233/94

    CPC分类号： C07D233/92 ,  C07D233/93 ,  C07D233/94

    摘要： Novel 2-substituted 1-alkyl-nitroimidazoles and a process for their preparation by reaction of 2-methyl-nitroimidazoles with oxalic acid diesters, followed by reaction of the resulting nitroimidazol-2-yl-pyruvic acid esters with chlorine, in turn followed, if desired, by reaction of the resulting 2-dihalomethyl-nitroimidazoles with water.Both the novel and the known compounds obtainable by the process of the invention are valuable starting materials for the preparation of dyes, pesticides and drugs.

    摘要翻译： 新的2-取代的1-烷基 - 硝基咪唑及其通过2-甲基 - 硝基咪唑与草酸二酯反应制备的方法，然后将所得的硝基咪唑-2-基 - 丙酮酸酯与氯反应， 如果需要，通过所得2-二卤代甲基 - 硝基咪唑与水的反应。 通过本发明的方法获得的新颖和已知的化合物都是用于制备染料，农药和药物的有价值的起始材料。