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    2,4,5-TRIAMINOPHENOLS AND RELATED COMPOUNDS
    73.
    发明申请
    2,4,5-TRIAMINOPHENOLS AND RELATED COMPOUNDS 审中-公开
    2,4,5-三硝基苯酚及相关化合物

    公开(公告)号：US20130053573A1

    公开(公告)日：2013-02-28

    申请号：US13516820

    申请日：2010-12-21

    申请人： Rajiv Dhawan ,  Joachim C. Ritter

    发明人： Rajiv Dhawan ,  Joachim C. Ritter

    IPC分类号： C07C213/08 ,  C07D213/803

    CPC分类号： C07C63/26 ,  C07C63/333 ,  C07C63/38 ,  C07C65/03 ,  C07C65/11 ,  C07C65/24 ,  C07C215/80

    摘要： New triaminophenol compositions and related compounds are disclosed, as are processes for their preparation and for the preparation of novel salts and diacid complexes from such compounds. Polymers prepared from these compositions can be made into high strength fiber, film, and tape and are useful in applications such as protective apparel, aircraft, automotive components, personal electronics, and sports equipment.

    摘要翻译： 公开了新的三氨基苯酚组合物和相关化合物，以及它们的制备方法以及从这些化合物制备新的盐和二酸配合物。 由这些组合物制备的聚合物可以制成高强度纤维，薄膜和胶带，并且可用于诸如保护性服装，飞机，汽车部件，个人电子设备和运动器材的应用中。

    INTEGRATED PROCESSES FOR THE PREPARATION OF POLYBENZIMIDAZOLE PRECURSORS
    74.
    发明申请
    INTEGRATED PROCESSES FOR THE PREPARATION OF POLYBENZIMIDAZOLE PRECURSORS 审中-公开
    用于制备聚苯并咪唑前体的综合方法

    公开(公告)号：US20130046109A1

    公开(公告)日：2013-02-21

    申请号：US13517283

    申请日：2010-12-21

    申请人： Rajiv Dhawan ,  Joachim C. Ritter

    发明人： Rajiv Dhawan ,  Joachim C. Ritter

    IPC分类号： C07C213/02

    CPC分类号： C07C213/08 ,  C07C51/412 ,  Y02P20/125 ,  C07C65/05 ,  C07C63/26 ,  C07C63/38 ,  C07C215/80

    摘要： An integrated process is provided for efficiently preparing 2,4,5-triaminaphenol, starting with nitration of 2,6-dihalobenzene; high purity salts thereof; and complexes of 2,4,5-triaminophenol aromatic diacids, which are precursors for making polybenzimidazole polymer for high performance fibers. The process design eliminates several costly intermediate drying and recrystallization steps. The handling of solid materials with possible skin sensitizing properties and toxicity is avoided, thereby eliminating human and environmental exposure.

    摘要翻译： 提供了一种综合方法，用于有效地制备2,4,5-三氨基苯酚，从2,6-二卤代苯的硝化开始; 其高纯度盐; 以及2,4,5-三氨基苯酚芳族二酸的络合物，其是用于制备用于高性能纤维的聚苯并咪唑聚合物的前体。 该工艺设计消除了几个昂贵的中间干燥和重结晶步骤。 避免了具有可能的皮肤敏感性和毒性的固体材料的处理，从而消除了人体和环境的暴露。

    Process for the preparation of monomers for polybenzimidazole materials
    77.
    发明授权
    Process for the preparation of monomers for polybenzimidazole materials 失效
    制备聚苯并咪唑物质单体的方法

    公开(公告)号：US08163961B2

    公开(公告)日：2012-04-24

    申请号：US12634799

    申请日：2010-02-22

    申请人： Rajiv Dhawan ,  Joachim C. Ritter

    发明人： Rajiv Dhawan ,  Joachim C. Ritter

    IPC分类号： C07C211/00

    CPC分类号： C07C209/36 ,  C07C211/50

    摘要： Complexes of 2,3,5,6-tetraaminotoluene with an aromatic diacid are prepared by reaction with a divalent salt of the aromatic diacid while maintaining the pH of the reaction solution between 3 and 10. The resulting complexes are suitable for making high molecular weight polybenzimidazole polymers for high-performance fibers.

    摘要翻译： 通过与芳族二酸的二价盐反应制备2,3,5,6-四氨基甲苯与芳族二酸的络合物，同时保持反应溶液的pH在3和10之间。所得的络合物适于制备高分子量 用于高性能纤维的聚苯并咪唑聚合物。

    Process for the synthesis of ethers of aromatic acids
    79.
    发明授权
    Process for the synthesis of ethers of aromatic acids 失效
    合成芳香族醚的方法

    公开(公告)号：US07985825B2

    公开(公告)日：2011-07-26

    申请号：US12518170

    申请日：2007-12-18

    申请人： Joachim C. Ritter

    发明人： Joachim C. Ritter

    IPC分类号： C08G63/00 ,  C08G64/00

    CPC分类号： C08G63/00 ,  C07C51/367 ,  C07C65/24 ,  C07C65/21

    摘要： Ethers of aromatic acids are produced from halogenated aromatic acids in a reaction mixture containing a halogenated aromatic acid such as is described by the structure of Formula II wherein each X is independently Cl, Br or I; the reaction mixture further comprising; (i) a polar protic solvent, a polar aprotic solvent or an alcoholic solvent containing the alcoholate RO-M+ (wherein M is Na or K), wherein the polar protic solvent, polar aprotic solvent or alcoholic solvent is either ROH or is a solvent that is less acidic than ROH; (ii) a copper (I) or copper (II) source; and (iii) an amino acid ligand that coordinates to copper, wherein the ligand comprises an amino acid in which the amine nitrogen and the carboxyl carbon are separated by no more than two carbon atoms.

    摘要翻译： 芳族酸的醚由卤代芳族酸在含有卤代芳族酸的反应混合物中制备，如式II结构所述，其中每个X独立地为Cl，Br或I; 所述反应混合物还包含 （i）极性质子溶剂，极性非质子溶剂或含有醇化物RO-M +（其中M为Na或K）的醇溶剂，其中极性质子溶剂，极性非质子溶剂或醇溶剂为ROH或溶剂 比ROH酸性低; （ii）铜（I）或铜（II）源; 和（iii）与铜配位的氨基酸配体，其中配体包含其中胺氮和羧基碳不超过两个碳原子分离的氨基酸。

    PROCESS FOR THE SYNTHESIS OF FLUORINATED ETHERS OF AROMATIC ACIDS
    80.
    发明申请
    PROCESS FOR THE SYNTHESIS OF FLUORINATED ETHERS OF AROMATIC ACIDS 审中-公开
    合成芳香族化合物的方法

    公开(公告)号：US20110065892A1

    公开(公告)日：2011-03-17

    申请号：US12874474

    申请日：2010-09-02

    申请人： Joachim C. Ritter ,  Kenneth Gene Moloy ,  Joel M. Pollino ,  Surbhi Mahajan Du

    发明人： Joachim C. Ritter ,  Kenneth Gene Moloy ,  Joel M. Pollino ,  Surbhi Mahajan Du

    IPC分类号： C08G69/40 ,  C07C65/21

    CPC分类号： C08G63/6826 ,  C07C51/367 ,  C07C65/21

    摘要： Fluorinated ethers of aromatic acids are produced from halogenated aromatic acids in a reaction mixture containing a copper (I) or copper (II) source and an amino acid ligand that coordinates to copper. The fluorinated ethers of aromatic acids made using the process described herein can be applied to, e.g., fibers, yarns, carpets, garments, films, molded parts, paper and cardboard, stone, and tile to impart soil, water and oil resistance. By incorporating the fluorinated ethers of aromatic acids, or diesters thereof, into polymer backbones, more lasting soil, water and oil resistance, as well as improved flame retardance, can be achieved.

    摘要翻译： 芳族酸的氟化醚由含有铜（I）或铜（II）源的氨基酸配体与铜配位的反应混合物中的卤代芳香酸生成。 使用本文所述方法制备的芳族酸的氟化醚可以应用于例如纤维，纱线，地毯，衣服，薄膜，模制部件，纸和纸板，石头和瓦片，以赋予土壤，水和耐油性。 通过将芳族酸或其二酯的氟化醚引入聚合物主链中，可以实现更持久的土壤，耐水和耐油性以及改进的阻燃性。