公开(公告)号：US5177301A

公开(公告)日：1993-01-05

申请号：US822803

申请日：1992-01-21

申请人： John F. Knifton

发明人： John F. Knifton

IPC分类号： C07C7/148

CPC分类号： C07C7/14891

摘要： Disclosed is a two-step method for separating isobutylene from a C-4 hydrocarbon fraction comprising:a) Reacting the C-4 fraction with a glycol in the presence of a catalyst comprising heteropoly acid on an inert support at a temperature of about 60.degree. to 160.degree. C. to yield the corresponding glycol mono-t-butyl ether, and subsequentlyb) reacting the intermediate glycol ether product over the same class of catalyst at a temperature of about 100.degree. to 220.degree. C. to regenerate the isolatable isobutylene.

摘要翻译： 公开了一种用于从C-4烃馏分分离异丁烯的两步法，其包括：a）在约60℃的温度下在惰性载体上，在包含杂多酸的催化剂存在下，用二醇反应C-4馏分 至160℃以产生相应的二醇单叔丁基醚，随后b）在约100℃至220℃的温度下使中间体二醇醚产物在相同类别的催化剂上反应以再生可分离的异丁烯 。

公开(公告)号：US5169550A

公开(公告)日：1992-12-08

申请号：US534080

申请日：1990-06-06

申请人： John R. Sanderson ,  Edward T. Marquis

发明人： John R. Sanderson ,  Edward T. Marquis

IPC分类号： C07C2/74 ,  C10M109/00 ,  C10M111/04

CPC分类号： C10M109/00 ,  C07C2/74 ,  C10M111/04 ,  C07C2521/16 ,  C10M2203/02 ,  C10M2203/0206 ,  C10M2203/022 ,  C10M2203/024 ,  C10M2203/04 ,  C10M2205/028 ,  C10M2205/0285 ,  C10M2207/023 ,  C10M2207/0235 ,  C10N2220/02

摘要： Synthetic lubricant base stocks having an increased viscosity are disclosed. These synthetic lubricant base stocks comprise a mixture of (1) oligomers prepared from a linear olefin having from 10 to 24 carbon atoms; and (2) alkylated cyclohexanol having an alkyl group containing from 10 to 24 carbon atoms. These synthetic lubricant base stocks may be prepared by hydrogenating the co-reaction products of a linear olefin having from 10 to 24 carbon atoms and phenol.

摘要翻译： 公开了具有增加粘度的合成润滑剂基础油料。 这些合成润滑剂基础油料包含（1）由具有10-24个碳原子的直链烯烃制备的低聚物的混合物; 和（2）具有含有10-24个碳原子的烷基的烷基化环己醇。 这些合成润滑剂基础油料可以通过氢化具有10-24个碳原子的直链烯烃和苯酚的共反应产物来制备。

公开(公告)号：US5162388A

公开(公告)日：1992-11-10

申请号：US709931

申请日：1991-06-04

申请人： Dudley J. Primeaux, II

发明人： Dudley J. Primeaux, II

IPC分类号： C08G18/10 ,  C08G18/50 ,  C08G18/65 ,  C08G18/66 ,  C08G18/73 ,  C08G18/76

CPC分类号： C08G18/765 ,  C08G18/10 ,  C08G18/5024 ,  C08G18/6685 ,  C08G2150/50

摘要： An aliphatic polyurea elastomer is disclosed. The elastomer comprises an (A) and a (B) component. The (A) component includes an aliphatic isocyanate. The (B) component includes an amine terminated polyoxyalkylene polyol and a chain extender including an aliphatic spray polyurea elastomer comprising an (a) component which includes an aliphatic isocyanate and a (b) component which includes (1) an amine terminated polyoxyalkylene polyol and (2) a chain extender including cis-1,4-diaminocyclohexane, isophoronediamine, m-xylenediamine, 4,4'-methylenedicyclohexylamine, methanediamine, 1,4-diaminoethylcyclohexane and substituted derivatives thereof. Preferably, the chain extender includes cis-1,4-diaminocyclohexane, isophoronediamine or mixtures thereof.

公开(公告)号：US5160587A

公开(公告)日：1992-11-03

申请号：US786856

申请日：1991-11-01

申请人： Edward T. Marquis ,  George P. Speranza ,  Yu-Hwa E. Sheu ,  William K. Culbreth, III ,  David G. Pottratz

发明人： Edward T. Marquis ,  George P. Speranza ,  Yu-Hwa E. Sheu ,  William K. Culbreth, III ,  David G. Pottratz

IPC分类号： C07D301/19 ,  B01D3/40 ,  C07D301/32 ,  C07D303/04

CPC分类号： B01D3/40 ,  C07D301/32

摘要： An extractive distillation agent consisting essentially of dipropylene glycol is fed to an extractive distillation column used for the distillation of propylene oxide contaminated with water, acetone and methanol to obtain an overhead distillate fraction consisting of essentially anhydrous propylene oxide contaminated with reduced quantities of acetone and methanol, and a heavier bottoms distillation fraction containing substantially all of the dipropylene glycol, water and acetone and some of the methanol introduced into the distillation column.

公开(公告)号：US5159101A

公开(公告)日：1992-10-27

申请号：US833199

申请日：1992-02-10

申请人： Donald H. Champion ,  George P. Speranza

发明人： Donald H. Champion ,  George P. Speranza

IPC分类号： C07C255/13

CPC分类号： C07C255/13

摘要： Disclosed is a process wherein cyanoethylation is accomplished by reacting a compound of the formula: ##STR1## where R=H or CH.sub.3, n=1 to 3 and m=0 to 50, and acrylonitrile over a heterogeneous catalyst comprising, potassium fluoride or cesium fluoride supported on an oxide of an element from the group consisting of Group IA, IIA or IIIA of the Periodic Table.

摘要翻译： 公开了一种方法，其中氰基乙基化是通过使下式化合物（其中R = H或CH 3，n = 1-3和m = 0至50）与丙烯腈反应，在包含氟化钾或铯 氟化物负载在元素的氧化物上，该元素来自元素周期表的IA，IIA或IIIA族元素。

公开(公告)号：US5154803A

公开(公告)日：1992-10-13

申请号：US787509

申请日：1991-11-01

申请人： Edward T. Marquis ,  George P. Speranza ,  Yu-Hwa E. Sheu ,  William K. Culbreth, III ,  David G. Pottratz

发明人： Edward T. Marquis ,  George P. Speranza ,  Yu-Hwa E. Sheu ,  William K. Culbreth, III ,  David G. Pottratz

IPC分类号： B01D3/40 ,  C07D301/32

CPC分类号： B01D3/40 ,  C07D301/32

摘要： An extractive distillation agent consisting essentially of 2-methyl-2,4-pentanediol is fed to an extractive distillation column used for the distillation of propylene oxide contaminated with water, acetone and methanol to obtain an overhead distillate fraction consisting of essentially anhydrous propylene oxide contaminated with reduced quantities of acetone and methanol, and a heavier bottoms distillation fraction containing substantially all of the 2-methyl-2,4-pentanediol, water and acetone and some of the methanol introduced into the distillation column.

摘要翻译： 基本上由2-甲基-2,4-戊二醇组成的萃取蒸馏剂进料到用于蒸馏被水，丙酮和甲醇污染的环氧丙烷蒸馏的萃取蒸馏塔中，得到由基本上无水环氧丙烷污染的塔顶馏分馏分 减少丙酮和甲醇的量，以及含有基本上所有2-甲基-2,4-戊二醇，水和丙酮以及引入蒸馏塔中的一些甲醇的较重的塔底蒸馏馏分。

公开(公告)号：US5146030A

公开(公告)日：1992-09-08

申请号：US733794

申请日：1991-07-22

申请人： John R. Sanderson ,  John F. Knifton ,  Edward T. Marquis

发明人： John R. Sanderson ,  John F. Knifton ,  Edward T. Marquis

IPC分类号： B01J21/16 ,  B01J27/053 ,  B01J27/18 ,  B01J27/25 ,  B01J31/04 ,  C07B61/00 ,  C07C2/04 ,  C07C2/14 ,  C07C2/16 ,  C07C2/18 ,  C07C2/26 ,  C07C9/00 ,  C10M143/08

CPC分类号： C07C2/14 ,  B01J21/16 ,  C07C2/16 ,  C07C2/18 ,  C07C2/26 ,  C10M143/08 ,  C07C2521/16 ,  C07C2527/053 ,  C07C2527/167 ,  C07C2527/232 ,  C07C2527/25 ,  C07C2529/04 ,  C07C2531/04 ,  C10M2205/028 ,  C10N2220/02

摘要： An improved process is disclosed for preparing synthetic lubricant base stocks. Synthetic lubricant base stocks are prepared in good yield by oligomerizing linear olefins using cation-exchangeable layered clays that have been treated with a non-halogenated titanium salt or non-halogenated zirconium salt.

摘要翻译： 公开了用于制备合成润滑剂基础油料的改进方法。 通过使用已经用非卤化钛盐或非卤化锆盐处理的可阳离子交换层状粘土使线性烯烃低聚来制备合成润滑剂基础油料。

公开(公告)号：US5140090A

公开(公告)日：1992-08-18

申请号：US712817

申请日：1991-06-10

申请人： Donald H. Champion ,  George P. Speranza

发明人： Donald H. Champion ,  George P. Speranza

IPC分类号： C08G18/32 ,  C08G18/10 ,  C08G18/50 ,  C08G18/65 ,  C08G18/66 ,  C08G18/72 ,  C08G18/73 ,  C08G18/76

CPC分类号： C08G18/765 ,  C08G18/10 ,  C08G18/5024 ,  C08G18/6685 ,  C08G2120/00

摘要： Disclosed is a method for preparing aliphatic polyureas in varying reaction times which comprises reacting polyoxyalkylene polyamines, an aliphatic diisocyanate and a sym-dialkylethylenediamine.

摘要翻译： 公开了一种在不同反应时间内制备脂族聚脲的方法，其中包括使聚氧化烯多胺，脂族二异氰酸酯和对称二烷基乙二胺反应。

公开(公告)号：US5139622A

公开(公告)日：1992-08-18

申请号：US770493

申请日：1991-10-03

申请人： Edward T. Marquis ,  George P. Speranza ,  Yu-Hwa E. Sheu ,  William K. Culbreth, III ,  David G. Pottratz

发明人： Edward T. Marquis ,  George P. Speranza ,  Yu-Hwa E. Sheu ,  William K. Culbreth, III ,  David G. Pottratz

IPC分类号： B01D3/40 ,  C07D301/32 ,  C07D303/04

CPC分类号： B01D3/40 ,  C07D301/32

摘要： An extractive distillation agent consisting essentially of triethylene glycol is fed to an extractive distillation column used for the distillation of propylene oxide contaminated with water, acetone and methanol to obtain an overhead distillate fraction consisting of essentially anhydrous propylene oxide contaminated with reduced quantities of acetone and methanol, and a heavier bottoms distillation fraction containing substantially all of the triethylene glycol, water and acetone and some of the methanol introduced into the distillation column.

公开(公告)号：US5138095A

公开(公告)日：1992-08-11

申请号：US594465

申请日：1990-10-09

申请人： George P. Speranza ,  John R. Sanderson

发明人： George P. Speranza ,  John R. Sanderson

IPC分类号： C08G65/324 ,  C08G65/326 ,  C08G65/338 ,  C11D1/16

CPC分类号： C11D1/16 ,  C08G65/324 ,  C08G65/326 ,  C08G65/338

摘要： Bisulfite addition products, which exhibit surface active properties, prepared by reacting a ketone-terminated polyoxyalkylene compound, such as a diketone of a polyoxypropylene glycol, a monoketone of a polyoxyalkylene alcohol, etc. with an ammonium or alkali metal bisulfite are disclosed.

摘要翻译： 公开了通过使酮封端的聚氧化烯化合物如聚氧丙烯二醇的二酮，聚氧化烯醇的单酮等与铵或碱金属亚硫酸氢盐反应制备的表现出表面活性的亚硫酸氢盐加成产物。