Carbon fiber from oriented vinylidene halide polymers
    71.
    发明授权
    Carbon fiber from oriented vinylidene halide polymers 失效
    碳纤维从定向的乙烯基硬脂酸聚合物

    公开(公告)号:US3840649A

    公开(公告)日:1974-10-08

    申请号:US19369671

    申请日:1971-10-29

    申请人: DOW CHEMICAL CO

    发明人: FEAY D LEDBETTER H

    CPC分类号: D01F9/21 C01B32/00

    摘要: 1. A PROCESS FOR PREPARING A CARBONACEOUS FIBER FROM A VINYLIDENE CHLORIDE POLYMER FILAMENT COMPRISING THE SEQUENTIAL STEPS OF: (1) TREATING SAID VINYLIDENE CHLORIDE POLYMER FILAMENT WITH AN ORGANIC AMINE HAVING THE FORMULA R-NH2 WHEREIN R IS ALKYL CONTAINING FROM 1 TO 4 CARBON ATOMS AT A TEMPERATURE LESS THAN ABOUT 125*C. IN THE ESSENTIAL ABSENCE OF MOISTURE UNTIL SAID FILAMENT IS FROM ABOUT 25 TO 80 PERCENT DEHYDROHALOGENATED BYT WUTHO OUT SIGNIFICANT LOSS IN FILAMENT STRUCTURAL INTEGRITY, AND (2) CARBONIZING SAID FILAMENT BY SUBJECTING THE SAME TO A TEMPERATURE WHICH IS INCREASED FROM AN INITIAL VALUE OF AT LEAST ABOUT 90*C. TO A FINAL VALUE OF UP TO ABOUT 1500*C. OVER A PERIOD OF AT LEAST 5 MINUTES.

    NANOFIBERS AND PREPARATION METHODS THEREFOR

    公开(公告)号:US20220213620A1

    公开(公告)日:2022-07-07

    申请号:US17608989

    申请日:2020-11-13

    发明人: CHAO GAO Jiaqing WANG

    IPC分类号: D01F9/21 D01D5/00

    摘要: The present invention discloses a method for preparing graphene nanofibers and non-woven fabrics using a fluid with a ultra-high draw ratio by means of a high-voltage electrospinning method. Compared with other methods for preparing graphene fibers (such as wet spinning, air-assisted spinning, etc.), the graphene fibers obtained by the present method have smaller diameters (about 100 nm to 500 nm) and a higher yield. The fibers themselves have better mechanical and electrical properties. The invention discloses a method for preparing ultra-fine graphene nanofibers and non-woven fabrics by electrospinning a mixed spinning liquid system of polymer and graphene oxide (the polymer is sodium polyacrylate). This method is highly efficient and environmentally friendly, and the resulted graphene nanofibers are the thinnest graphene fibers as currently known.

    Method for manufacturing carbon fibers and fiber joining method

    公开(公告)号:US10988862B2

    公开(公告)日:2021-04-27

    申请号:US16074685

    申请日:2017-01-31

    摘要: A carbon fiber manufacturing method includes joining first and second target fiber bundles with a joining fiber bundle, and carbonizing the joined bundles by feeding them through one or more carbonization furnaces. The joining includes forming an overlap between a first end of the joining fiber bundle and a second end of the first target fiber bundle and jetting a fluid to the overlap to form a first entangled portion, and forming an overlap between a second end of the joining fiber bundle and a first end of the second target fiber bundle and jetting a fluid to the overlap to form a second entangled portion. When the first and second entangled portions each have two or more entangling points with a tensile strength not less than 400 N, the relationship defined by the inequality is satisfied: 40>{L2/(L2−A)}×(S+13), where L2 is a length (mm) of an elongation section inside a first carbonization furnace upstream in a feeding direction of the fiber bundles, A is a maximum distance (mm) between an entangling point in the first entangled portion and an entangling point in the second entangled portion, and S is an elongation (%) of the joined fiber bundles fed through the carbonization furnace.