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公开(公告)号：US5356612A
公开(公告)日：1994-10-18
申请号：US088278
申请日：1993-07-06
申请人： Maria A. Curtin , Alan M. Phipps
发明人： Maria A. Curtin , Alan M. Phipps
CPC分类号： A61K8/25 , A61K8/26 , A61K8/28 , A61Q15/00 , Y10S424/05 , Y10S514/938
摘要： Antiperspirant effectiveness of basic aluminum chloride is increased by mixing it with monosilicic acid in aqueous solution. The product can be dried to a solid, and the antiperspirant effectiveness does not decrease in contact with water. The product can also be characterized by size exclusion chromatography of its approximately 10% by weight aqueous solution. Zirconyl hydroxy chloride may also be present.
摘要翻译： 通过将其与水溶液中的单硅酸混合，可以增加碱性氯化铝的止汗效果。 产品可以干燥成固体，止汗效果与水接触不会降低。 该产品还可以通过其约10重量％水溶液的尺寸排阻色谱来表征。 氧化锆羟基氯也可以存在。
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公开(公告)号：US5330751A
公开(公告)日：1994-07-19
申请号：US594349
申请日：1990-10-03
申请人： Maria A. Curtin , Alan M. Phipps
发明人： Maria A. Curtin , Alan M. Phipps
CPC分类号： A61Q15/00 , A61K8/25 , A61K8/26 , A61K8/28 , Y10S424/05
摘要： Antiperspirant effectiveness of basic aluminum chloride is increased by mixing it with monosilicic acid in aqueous solution. The product can be dried to a solid, and the antiperspirant effectiveness does not decrease in contact with water. The product can also be characterized by size exclusion chromatography of its approximately 10% by weight aqueous solution. Zirconyl hydroxy chloride may also be present.
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公开(公告)号：US5486347A
公开(公告)日：1996-01-23
申请号：US452554
申请日：1995-05-25
IPC分类号： A61K8/26 , A61K8/28 , A61K8/44 , A61K33/06 , A61K33/24 , A61Q15/00 , C01F7/00 , C01G1/06 , C01G25/04 , C07F9/00 , A61K7/34 , A61K7/38 , C01G9/02
CPC分类号： A61Q15/00 , A61K8/26 , A61K8/28 , A61K8/44 , Y10S424/05
摘要： A composition of zirconyl hydroxy chloride and aluminum chlorhydroxide in stable solid form having improved antiperspirant efficacy when dissolved in water is made by heating a 2-20% by weight aqueous solution containing at least the aluminum chlorhydroxide component of the composition at a temperature of at least 50.degree. C. until the ratio of the height of peak 4 at Kd=0.7 to that of peak 3 at Kd=0.5 as measured by gel permeation chromatography on cross-linked dextran is at least 2:1, then subjecting the solution to rapid drying to solid form.
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公开(公告)号：US5298640A
公开(公告)日：1994-03-29
申请号：US939808
申请日：1992-09-03
IPC分类号： A61K8/26 , A61K8/28 , A61K8/44 , A61K33/24 , A61Q15/00 , C01F7/00 , C01G25/04 , C07F9/00 , A61K7/34 , A61K7/38 , B01D11/00
摘要： A composition of zirconyl hydroxy chloride and aluminum chlorhydroxide in stable solid form having improved antiperspirant efficacy when dissolved in water is made by heating a 2-20% by weight aqueous solution containing at least the aluminum chlorhydroxide component of the composition at a temperature of at least 50.degree. C. until the ratio of the height of peak 4 at Kd=0.7 to that of peak 3 at Kd=0.5 as measured by gel permeation chromatography on cross-linked dextran is at least 2:1, then subjecting the solution to rapid drying to solid form.
摘要翻译： 通过在至少含有至少含有组合物的氢氧化铝组分的2-20重量％的水溶液中加热至少含有氯化氢氧化铝的组合物来制备具有稳定固体形式的稳定固体形式的羟基氧化锆和氢氧化铝的组合物，其具有改善的止汗效力 直到在交联葡聚糖上通过凝胶渗透色谱法测定的Kd = 0.7时的峰4的高度与K 3的峰3的比例至少为2:1，然后使溶液迅速 干燥至固体形式。
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公开(公告)号：US5770186A
公开(公告)日：1998-06-23
申请号：US771364
申请日：1996-12-16
IPC分类号： A61K8/26 , A61K8/28 , A61K8/44 , A61K33/06 , A61K33/24 , A61Q15/00 , C01F7/00 , C01G1/06 , C01G25/04 , C07F9/00 , A61K7/32 , C01G25/00
CPC分类号： A61Q15/00 , A61K8/26 , A61K8/28 , A61K8/44 , Y10S424/05
摘要： A composition of zirconyl hydroxy chloride and aluminum chlorhydroxide in stable solid form having improved antiperspirant efficacy when dissolved in water is made by heating a 2-20% by weight aqueous solution containing at least the aluminum chlorhydroxide component of the composition at a temperature of at least 50.degree. C. until the ratio of the height of peak 4 at Kd=0.7 to that of peak 3 at Kd=0.5 as measured by gel permeation chromatography on cross-linked dextran is at least 2:1, then subjecting the solution to rapid drying to solid form.
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公开(公告)号：US5114705A
公开(公告)日：1992-05-19
申请号：US287096
申请日：1988-12-20
CPC分类号： A61Q15/00 , A61K8/26 , A61K8/28 , A61K8/44 , Y10S424/05 , Y10S514/938
摘要： A composition of zirconyl hydroxy chloride and aluminum chlorhydroxide in stable solid form having improved antiperspirant efficacy when dissolved in water is made by heating a 2-20% by weight aqueous solution containing at least the aluminum chlorhydroxide component of the composition at a temperature of at least 50.degree. C. until the ratio of the height of peak 4 at Kd=0.7 to that of peak 3 at Kd=0.5 as measured by gel permeation chromatography on cross-linked dextran is at least 2:1, then subjecting the solution to rapid drying to solid form.
摘要翻译： 通过在至少含有至少含有组合物的氢氧化铝组分的2-20重量％的水溶液中加热至少含有氯化氢氧化铝的组合物来制备具有稳定固体形式的稳定固体形式的羟基氧化锆和氢氧化铝的组合物，其具有改善的止汗效力 直到在交联葡聚糖上通过凝胶渗透色谱法测定的Kd = 0.7时峰4的高度与K 3 = 3的峰3的比例至少为2:1，然后使溶液快速 干燥至固体形式。
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公开(公告)号：US5589196A
公开(公告)日：1996-12-31
申请号：US252376
申请日：1994-06-01
IPC分类号： A61K8/26 , A61K8/28 , A61K8/44 , A61K33/06 , A61K33/24 , A61Q15/00 , C01F7/00 , C01G1/06 , C01G25/04 , C07F9/00 , A61K7/32 , C01G25/00
CPC分类号： A61Q15/00 , A61K8/26 , A61K8/28 , A61K8/44 , Y10S424/05
摘要： A composition of zirconyl hydroxy chloride and aluminum chlorhydroxide in stable solid form having improved antiperspirant efficacy when dissolved in water is made by heating a 2-20% by weight aqueous solution containing at least the aluminum chlorhydroxide component of the composition at a temperature of at least 50.degree. C. until the ratio of the height of peak 4 at Kd=0.7 to that of peak 3 at Kd=0.5 as measured by gel permeation chromatography on cross-linked dextran is at least 2:1, then subjecting the solution to rapid drying to solid form.
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公开(公告)号：US4775528A
公开(公告)日：1988-10-04
申请号：US036262
申请日：1987-04-09
CPC分类号： A61K8/44 , A61K8/26 , A61K8/28 , A61Q15/00 , Y10S424/05
摘要： A composition of zirconyl hydroxy chloride and aluminum chlorhydroxide in stable solid form having improved antiperspirant efficacy when dissolved in water is made by heating a 2-20% by weight aqueous solution containing at least the aluminum chlorhydroxide component of the composition at a temperature of at least 50.degree. C. until the ratio of the height of peak 4 at Kd=0.7 to that of peak 3 at Kd=0.5 as measured by gel permeation chromotography on cross-linked dextran is at least 2:1, then subjecting the solution to rapid drying to solid form.
摘要翻译： 通过在至少含有至少含有组合物的氢氧化铝组分的2-20重量％的水溶液中加热至少含有氯化氢氧化铝的组合物来制备具有稳定固体形式的稳定固体形式的羟基氧化锆和氢氧化铝的组合物，其具有改善的止汗效力 直到在交联葡聚糖上通过凝胶渗透色谱法测量的Kd = 0.7处的峰4的高度与K 3的峰3的比例至少为2:1，然后将溶液快速 干燥至固体形式。
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公开(公告)号：US5384117A
公开(公告)日：1995-01-24
申请号：US974673
申请日：1992-11-12
申请人： Tuan M. Vu , Thomas J. Krafton , Alan M. Phipps
发明人： Tuan M. Vu , Thomas J. Krafton , Alan M. Phipps
CPC分类号： A61Q15/00 , A61K8/26 , A61K8/28 , A61K8/37 , A61K8/8111 , A61K8/8135 , A61K2800/31 , Y10S514/944
摘要： A substantially clear, anhydrous suspension-type antiperspirant product includes an effective amount of an active antiperspirant component in particulate form suspended in an anhydrous vehicle such that there is no significant dissolution of the active antiperspirant ingredient in the vehicle, and the refractive indices of the active antiperspirant component and the vehicle are matched.
摘要翻译： 基本上透明的无水悬浮型止汗产品包括有效量的悬浮在无水载体中的颗粒形式的活性止汗组分，使得活性止汗组分在载体中没有显着溶解，活性物质的折射率 止汗剂组分和车辆匹配。
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