公开(公告)号：US4123504A

公开(公告)日：1978-10-31

申请号：US784593

申请日：1977-04-04

Applicant: Alexandr A. Shulzhenko ,  Anatoly F. Getman

Inventor： Alexandr A. Shulzhenko ,  Anatoly F. Getman

IPC: B01J3/06 ,  C01B31/06

CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/0655 ,  B01J2203/068

Abstract: A method of diamond synthesis, by which a reaction mixture is prepared comprising, taken in direct contact, a carbon-containing material and a combination of components selected from the group containing silver chloride, calcium carbonate, calcium oxide and from a group containing aluminium and boron. Then the reaction mixture is subjected to the action of a temperature of at least about 1800.degree. C and a pressure corresponding to a selected temperature within the diamond stable region during the time required for forming a diamond.

Abstract translation: 一种金刚石合成方法，通过该方法制备反应混合物，其包括直接接触含碳材料和选自含氯化银，碳酸钙，氧化钙和含有铝的组的组分的组合，以及 硼。 然后在形成金刚石所需的时间内将反应混合物进行至少约1800℃的温度和对应于金刚石稳定区域内的选定温度的压力。

公开(公告)号：US4349517A

公开(公告)日：1982-09-14

申请号：US199273

申请日：1980-10-21

Applicant: Vladislav S. Lysanov ,  Viktor V. Digonsky ,  Leon I. Feldgun ,  Valery M. Davidenko ,  Nikolai V. Novikov ,  Alexandr I. Borimsky ,  Alexandr A. Shulzhenko ,  Valerian D. Yakimenko ,  Eduard Y. Dovgal ,  Vitaly Y. Egorov ,  Vyacheslav S. Rovsha ,  Alexei I. Prikhna ,  Alexandr N. Sokolov

Inventor： Vladislav S. Lysanov ,  Viktor V. Digonsky ,  Leon I. Feldgun ,  Valery M. Davidenko ,  Nikolai V. Novikov ,  Alexandr I. Borimsky ,  Alexandr A. Shulzhenko ,  Valerian D. Yakimenko ,  Eduard Y. Dovgal ,  Vitaly Y. Egorov ,  Vyacheslav S. Rovsha ,  Alexei I. Prikhna ,  Alexandr N. Sokolov

IPC: C04B35/5831 ,  C01B35/14

CPC classification number: C04B35/5831

Abstract: Disclosed is a method of producing cubic boron nitride, which comprises the steps of subjecting to a pressure of from 40 to 70 kilobars and to a temperature of from 1100.degree. to 2000.degree. C. a charge including hexagonal boron nitride and a conversion initiator selected from the group consisting of alkali and alkaline earth metals and borides of the foregoing metals, doping the charge with crystallohydrate in the form of a compound selected from the group consisting of sulfur-, halogen- or nitrogen-containing salts and their mixtures incorporating at least 5 molecules of crystallization water. According to another embodiment, the aforesaid charge is doped with a member selected from the group consisting of alkali metal hydroxide or alkaline earth metal hydroxide.

Abstract translation: 公开了一种制备立方氮化硼的方法，其包括以下步骤：施加40至70千巴的压力和1100至2000℃的温度。包含六方氮化硼和选自以下的转化引发剂的电荷 由碱金属和碱土金属组成的组和前述金属的硼化物，以选自硫，卤素或含氮盐的化合物形式的晶体水合物掺杂电荷，并且其混合物至少掺入5 分子结晶水。 根据另一个实施方案，上述电荷掺杂有选自碱金属氢氧化物或碱土金属氢氧化物的成员。