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公开(公告)号：US5274149A
公开(公告)日：1993-12-28
申请号：US848505
申请日：1992-03-09
CPC分类号： C07F9/723 , C23C16/301 , Y02P20/582 , Y10S252/951 , Y10S438/935
摘要： Alkyl arsines are made by a reaction of gaseous arsine and the corresponding gaseous olefin in contact with at least one Bronsted acid catalyst. Products produced thereby are mono- and di-substituted arsines, e.g. alkyl and di-alkyl arsines, which contain substantially no metallic or oxygenating impurities.
摘要翻译： 烷基胂通过气态胂和与至少一种布朗斯台德酸催化剂接触的相应气态烯烃的反应制备。 由此产生的产物是单 - 和二 - 取代的胂，例如 烷基和二烷基胂，其基本上不含金属或含氧杂质。
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公开(公告)号：US5847056A
公开(公告)日：1998-12-08
申请号：US886228
申请日：1997-07-01
摘要： A process is disclosed for the formation of highly anionic hydroxamic acid polymers whereby (meth) acrylic acid polymers are esterified in aqueous solution to poly (meth) acrylates. The resultant polymers are then reacted with an hydroxylamine to produce hydroxamated (meth) acrylic acid containing polymers. The esterified polymers, their hydroxamated derivatives and their use to flocculate Bayer Process streams are also disclosed.
摘要翻译： 公开了用于形成高度阴离子的异羟肟酸聚合物的方法，由此（甲基）丙烯酸聚合物在水溶液中酯化成聚（甲基）丙烯酸酯。 然后将得到的聚合物与羟胺反应，生成含羟肟基（甲基）丙烯酸的聚合物。 还公开了酯化聚合物，它们的异羟肟化衍生物及其用于絮凝拜耳法工艺流的用途。
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3.发明授权Process of making alkyl phosphine compounds by reacting an olefin and a phosphine in the vapor phase over a mineral acid catalyst 失效通过使无机酸催化剂中的气相中的烯烃和膦反应制备烷基膦化合物的方法
公开(公告)号：US5260485A
公开(公告)日：1993-11-09
申请号：US848504
申请日：1992-03-09
IPC分类号： C07F9/50
CPC分类号： C07F9/5059
摘要： Alkylphosphines are made by a reaction of gaseous phosphine and the corresponding gaseous olefin in contact with at least one non-oxidizing acid catalyst. Products produced thereby are alkylphosphines which contain substantially no metallic or oxygenating impurities. The process is a continuous process and employs a mineral acid catalyst either in solid form or as a liquid supported on a solid, inert material.
摘要翻译： 烷基膦通过气态膦和与至少一种非氧化性酸催化剂接触的相应气态烯烃的反应制备。 由此生产的产品是基本上不含金属或含氧杂质的烷基膦。 该方法是连续的方法，并采用固体形式的无机酸催化剂或负载在固体惰性材料上的液体。
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公开(公告)号：US07973195B2
公开(公告)日：2011-07-05
申请号：US12507122
申请日：2009-07-22
申请人： Mohan Nair , C. Joseph Calbick
发明人： Mohan Nair , C. Joseph Calbick
IPC分类号： C07C69/52
CPC分类号： C07C213/08 , Y02P20/582 , C07C219/08
摘要： An unsaturated quaternary ammonium salt is produced by a process that includes reacting methyl chloride in a first vessel with a stoichiometric excess of an unsaturated tertiary amine in the presence of water to form a reaction mixture that includes the unsaturated quaternary ammonium salt and residual unsaturated tertiary amine. The reaction mixture is transferred to a second vessel and phase separated to yield a first fraction in which the unsaturated quaternary ammonium salt is concentrated, and a second fraction in which the residual unsaturated tertiary amine is concentrated. At least a portion of the second fraction is recycled from the second vessel to the first vessel for use in the reaction with methyl chloride. The process, which is preferably operated continuously, allows the use of reduced reaction pressures compared to processes utilizing a stoichiometric excess of methyl chloride, and it also reduces or eliminates the problems associated with recycling methyl chloride and removing methyl chloride from the unsaturated quaternary ammonium salt product.
摘要翻译： 不饱和季铵盐通过包括在水存在下使第一容器中的甲基氯与化学计量过量的不饱和叔胺反应以形成包含不饱和季铵盐和残余不饱和叔胺的反应混合物的方法来生产 。 将反应混合物转移到第二容器中并进行相分离，得到其中不饱和季铵盐被浓缩的第一级分和残留的不饱和叔胺浓缩的第二级分。 第二级分的至少一部分从第二容器再循环到第一容器中以用于与甲基氯反应。 与使用化学计量过量的氯甲烷的方法相比，优选连续操作的方法允许使用降低的反应压力，并且还减少或消除与循环甲基氯并从不饱和季铵盐中除去甲基氯相关的问题 产品。
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公开(公告)号：US20110021808A1
公开(公告)日：2011-01-27
申请号：US12507122
申请日：2009-07-22
申请人： Mohan Nair , C. Joseph Calbick
发明人： Mohan Nair , C. Joseph Calbick
IPC分类号： C07C227/18
CPC分类号： C07C213/08 , Y02P20/582 , C07C219/08
摘要： An unsaturated quaternary ammonium salt is produced by a process that includes reacting methyl chloride in a first vessel with a stoichiometric excess of an unsaturated tertiary amine in the presence of water to form a reaction mixture that includes the unsaturated quaternary ammonium salt and residual unsaturated tertiary amine. The reaction mixture is transferred to a second vessel and phase separated to yield a first fraction in which the unsaturated quaternary ammonium salt is concentrated, and a second fraction in which the residual unsaturated tertiary amine is concentrated. At least a portion of the second fraction is recycled from the second vessel to the first vessel for use in the reaction with methyl chloride. The process, which is preferably operated continuously, allows the use of reduced reaction pressures compared to processes utilizing a stoichiometric excess of methyl chloride, and it also reduces or eliminates the problems associated with recycling methyl chloride and removing methyl chloride from the unsaturated quaternary ammonium salt product.
摘要翻译： 不饱和季铵盐通过包括在水存在下使第一容器中的甲基氯与化学计量过量的不饱和叔胺反应以形成包含不饱和季铵盐和残余不饱和叔胺的反应混合物的方法来生产 。 将反应混合物转移到第二容器中并进行相分离，得到其中不饱和季铵盐被浓缩的第一级分和残留的不饱和叔胺浓缩的第二级分。 第二级分的至少一部分从第二容器再循环到第一容器中以用于与甲基氯反应。 与使用化学计量过量的氯甲烷的方法相比，优选连续操作的方法允许使用降低的反应压力，并且还减少或消除与循环甲基氯并从不饱和季铵盐中除去甲基氯相关的问题 产品。
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公开(公告)号：US5415129A
公开(公告)日：1995-05-16
申请号：US71085
申请日：1993-06-04
CPC分类号： C07F9/723 , C23C16/301 , Y02P20/582 , Y10S252/951 , Y10S438/935
摘要： Alkyl arsines are made by a reaction of gaseous arsine and the corresponding gaseous olefin in contact with at least one Bronsted acid catalyst. Products produced thereby are mono- and di-substituted arsines, e.g. alkyl and di-alkyl arsines, which contain substantially no metallic or oxygenating impurities.
摘要翻译： 烷基胂通过气态胂和与至少一种布朗斯台德酸催化剂接触的相应气态烯烃的反应制备。 由此产生的产物是单 - 和二 - 取代的胂，例如 烷基和二烷基胂，其基本上不含金属或含氧杂质。
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