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    Process for producing 1-octene from butadiene in the presence of titanium catalysts
    4.
    发明申请
    Process for producing 1-octene from butadiene in the presence of titanium catalysts 有权
    在钛催化剂存在下由丁二烯生产1-辛烯的方法

    公开(公告)号：US20070179327A1

    公开(公告)日：2007-08-02

    申请号：US10576463

    申请日：2004-10-11

    申请人： Daniele Delledonne ,  Franco Rivetti

    发明人： Daniele Delledonne ,  Franco Rivetti

    IPC分类号： C07C2/00

    CPC分类号： C07C2/406 ,  A61K9/006 ,  C07C2/403 ,  C07C5/05 ,  C07C2531/14 ,  C07C2531/22 ,  C07C2531/24 ,  C07C2531/28 ,  C07C11/12

    摘要： A method is described for the preparation of 1-octene starting from butadiene, wherein in a first step (a) the bis-hydrodimerization of butadiene to 1,7-octadiene is effected in the presence of a catalyst based on palladium containing one or more tri-substituted monodentate phosphines, in an aprotic polar solvent, in a second step (b) the partial catalytic hydrogenation of 1,7-octadiene to 1-octene is effected in the presence of a titanium compound activated with one or more metal alkyls of group 13 (selected from boron, aluminum, gallium, indium).

    摘要翻译： 描述了从丁二烯开始制备1-辛烯的方法，其中在第一步（a）中，丁二烯至1,7-辛二烯的双加氢二聚作用是在催化剂存在下进行的，所述催化剂基于含有一种或多种 在非质子极性溶剂中，三取代的单齿膦在第二步（b）中，将1,7-辛二烯部分催化氢化成1-辛烯在钛化合物的存在下进行，所述钛化合物用一种或多种金属烷基 13族（选自硼，铝，镓，铟）。

    Method for removing acidic and salt impurities from an aqueous condensed phase containing dimethylcarbonate
    6.
    发明授权
    Method for removing acidic and salt impurities from an aqueous condensed phase containing dimethylcarbonate 失效
    从含碳酸二甲酯的水相凝析相中除去酸性和盐杂质的方法

    公开(公告)号：US5685957A

    公开(公告)日：1997-11-11

    申请号：US455697

    申请日：1995-05-31

    申请人： Franco Rivetti ,  Daniele Delledonne

    发明人： Franco Rivetti ,  Daniele Delledonne

    IPC分类号： C07C68/00 ,  C07C68/08 ,  C07C69/96 ,  B01D3/00

    CPC分类号： C07C68/08 ,  C07C68/005 ,  Y10S159/10 ,  Y10S203/90

    摘要： Acidic and salt impurities are removed from a condensed phase obtained from dimethyl carbonate synthesis by obtaining the condensed phase from the effluent of a reactor in which carbon monoxide, oxygen and methanol are reacted to form dimethyl carbonate, the condensed phase containing acid and salt impurities, and partially evaporating the condensed phase in an evaporator thereby preparing an evaporated stream substantially free of impurities and a residual bottom stream.

    摘要翻译： 通过从反应器的流出物中获得凝结相，从碳酸二甲酯合成得到的凝聚相中除去酸性和盐杂质，其中一氧化碳，氧气和甲醇反应生成碳酸二甲酯，所述冷凝相含有酸和盐杂质， 并在蒸发器中部分地蒸发冷凝相，从而制备基本上不含杂质的蒸发物流和残留的底部物流。

    Process for the preparation of 1-octene
    8.
    发明授权
    Process for the preparation of 1-octene 有权
    1-辛烯的制备方法

    公开(公告)号：US07368622B2

    公开(公告)日：2008-05-06

    申请号：US10576144

    申请日：2004-10-11

    申请人： Daniele Delledonne ,  Franco Rivetti

    发明人： Daniele Delledonne ,  Franco Rivetti

    IPC分类号： C07C2/04 ,  C07C5/05

    CPC分类号： C07C5/05 ,  A23P20/20 ,  A61K9/006 ,  C07C2/406 ,  C07C2531/22 ,  C07C2531/24 ,  Y02P20/582

    摘要： Process in two steps for the preparation of 1-octene starting from butadiene which comprises: a first step (a) in which the bis-hydrodimerization of butadiene to 1,7-octadiene is effected in the presence of a catalyst based on a palladium complex containing one or more tri-substituted monodentate phosphines, in an aprotic polar solvent optionally containing an organic base; a second step (b) in which the partial catalytic hydrogenation of 1,7-octadiene to 1-octene is effected, the above process being characterized in that: (i) in the first step the aprotic polar solvent is selected from disubstituted cyclic ureas; (ii) in the second step the catalyst is selected from non supported ruthenium complexes having general formula (II): RuXmLn (II).

    摘要翻译： 从丁二烯开始制备1-辛烯的两步法，其包括：第一步骤（a），其中丁二烯至1,7-辛二烯的双加氢二聚在催化剂存在下进行，所述催化剂基于钯络合物 含有一种或多种三取代的单齿膦，任选地含有有机碱的非质子极性溶剂; 其中进行1,7-辛二烯部分催化氢化至1-辛烯的第二步（b），上述方法的特征在于：（i）在第一步中，非质子极性溶剂选自二取代的环脲 ; （ii）在第二步中，催化剂选自具有通式（II）的非负载钌络合物：RuX m L（II）。

    Process for the preparation of 1-octene
    9.
    发明申请
    Process for the preparation of 1-octene 有权
    1-辛烯的制备方法

    公开(公告)号：US20070129585A1

    公开(公告)日：2007-06-07

    申请号：US10576144

    申请日：2004-10-11

    申请人： Daniele Delledonne ,  Franco Rivetti

    发明人： Daniele Delledonne ,  Franco Rivetti

    IPC分类号： C07C2/00 ,  C07C4/00

    CPC分类号： C07C5/05 ,  A23P20/20 ,  A61K9/006 ,  C07C2/406 ,  C07C2531/22 ,  C07C2531/24 ,  Y02P20/582

    摘要： Process in two steps for the preparation of 1-octene starting from butadiene which comprises: a first step (a) in which the bis-hydrodimerization of butadiene to 1,7-octadiene is effected in the presence of a catalyst based on a palladium complex containing one or more tri-substituted monodentate phosphines, in an aprotic polar solvent optionally containing an organic base; a second step (b) in which the partial catalytic hydrogenation of 1,7-octadiene to 1-octene is effected, the above process being characterized in that: (i) in the first step the aprotic polar solvent is selected from disubstituted cyclic ureas; (ii) in the second step the catalyst is selected from non supported ruthenium complexes having general formula (II): RuXmLn (II).

    摘要翻译： 从丁二烯开始制备1-辛烯的方法分为两步，其包括：第一步（a），其中丁二烯至1,7-辛二烯的双加氢二聚在催化剂存在下进行，所述催化剂基于钯络合物 含有一种或多种三取代的单齿膦，任选地含有有机碱的非质子极性溶剂; 其中进行1,7-辛二烯部分催化氢化至1-辛烯的第二步（b），上述方法的特征在于：（i）在第一步中，非质子极性溶剂选自二取代的环脲 ; （ii）在第二步中，催化剂选自具有通式（II）的非负载钌络合物：RuX m L（II）。

    Catalytic procedure for the preparation of organic carbonates
    10.
    发明授权
    Catalytic procedure for the preparation of organic carbonates 失效
    用于制备有机碳酸酯的催化方法

    公开(公告)号：US5457213A

    公开(公告)日：1995-10-10

    申请号：US73773

    申请日：1993-06-08

    申请人： Daniele Delledonne ,  Franco Rivetti ,  Ugo Romano

    发明人： Daniele Delledonne ,  Franco Rivetti ,  Ugo Romano

    IPC分类号： B01J31/12 ,  C07B61/00 ,  C07C68/00 ,  C07C69/96 ,  C07D317/36 ,  C07D317/38

    CPC分类号： C07D317/38 ,  C07C68/005 ,  C07D317/36

    摘要： Catalytic procedure for the preparation of an organic carbonate having general formula (I): ##STR1## wherein R represents a C.sub.1 -C.sub.10 alkyl radical, linear or branched, or a C.sub.5 -C.sub.8 cycloalkyl radical; or of a cyclic organic carbonate having general formula (II): ##STR2## wherein R' represents a C.sub.2 -C.sub.5 alkylene radical, linear or branched; including the reacting of an aliphatic or cyclo-aliphatic alcohol having general formula (III):R--OH (III)or an aliphatic diol having general formula (IV):HO--R'--OH (IV)wherein R and R' have the meaning described above, with carbon monoxide and oxygen, in the presence of a catalyst composed of a cobalt(II) or cobalt(III) ion and an organic binder containing at least one oxygen atom, characterized in that the process is carried out in the presence of at least one reaction coadjuvant selected from the following groups of linear or cyclic compounds: ureas, nitriles, amides, phosphoramides, sulphones, sulphoxides, carbamates.

    摘要翻译： 用于制备具有通式（I）的有机碳酸酯的催化方法：其中R表示直链或支链的C 1 -C 10烷基或C 5 -C 8环烷基; 或具有通式（II）的环状有机碳酸酯：其中R'表示直链或支链的C 2 -C 5亚烷基; 包括具有通式（III）的脂族或环脂族醇：R-OH（III）或具有通式（IV）的脂族二醇：HO-R'-OH（IV）其中R和R'具有 在由钴（II）或钴（III）离子组成的催化剂和含有至少一个氧原子的有机粘合剂存在下，用上述一氧化碳和氧气的含义，其特征在于该方法在 至少一种选自以下一组线性或环状化合物的反应助剂的存在：脲，腈，酰胺，磷酰胺，砜，亚砜，氨基甲酸酯。