公开(公告)号：US11116745B2

公开(公告)日：2021-09-14

申请号：US15929099

申请日：2019-01-31

申请人： Deep Cell Industries, Inc.

发明人： James Gerstenberger ,  Kelly Ogilvie

IPC分类号： A61K31/352 ,  A61K9/16 ,  B01D9/00 ,  C07C51/43 ,  B01D21/00 ,  B01D11/02 ,  A61K9/14 ,  C07C37/00

摘要： A method of generating an oligosaccharide encapsulated cannabidiol (CBD) formulation includes forming a cannabidiol ethanol mixture comprising ethanol and cannabidiol, forming an oligosaccharide CBD slurry by mixing the oligosaccharide with the cannabidiol ethanol mixture. The slurry is heated and mixed in a pressurized chamber to form a colloidal mixture, which is distributed into a tray as a layer. A cover is added to the tray to form an evaporation vessel, which is heated in a heating chamber. A rapid cooling process is performed on the colloidal mixture layer by removing the cover and spraying pulverized dry ice on the layer. The rapid cooling process is repeated until crystal formation is detected within the layer, the crystals including oligosaccharide encapsulated cannabidiol. An oligosaccharide encapsulated cannabidiol formulation includes cannabidiol and at least one oligosaccharide in a ratio in the range between about 1000:1 to 2200:1 (w/w) of CBD.

公开(公告)号：US20190231736A1

公开(公告)日：2019-08-01

申请号：US15929099

申请日：2019-01-31

申请人： Deep Cell Industries, Inc.

发明人： James Gerstenberger ,  Kelly Ogilvie

IPC分类号： A61K31/352 ,  A61K9/16 ,  B01D9/00 ,  B01D11/02 ,  B01D21/00 ,  C07C51/43

CPC分类号： A61K31/352 ,  A61K9/1652 ,  B01D9/0009 ,  B01D11/0288 ,  B01D11/0292 ,  B01D21/009 ,  C07C51/43

摘要： A method of generating an oligosaccharide encapsulated cannabidiol (CBD) formulation includes forming a cannabidiol ethanol mixture comprising ethanol and cannabidiol, forming an oligosaccharide CBD slurry by mixing the oligosaccharide with the cannabidiol ethanol mixture. The slurry is heated and mixed in a pressurized chamber to form a colloidal mixture, which is distributed into a tray as a layer. A cover is added to the tray to form an evaporation vessel, which is heated in a heating chamber. A rapid cooling process is performed on the colloidal mixture layer by removing the cover and spraying pulverized dry ice on the layer. The rapid cooling process is repeated until crystal formation is detected within the layer, the crystals including oligosaccharide encapsulated cannabidiol. An oligosaccharide encapsulated cannabidiol formulation includes cannabidiol and at least one oligosaccharide in a ratio in the range between about 1000:1 to 2200:1 (w/w) of CBD.

公开(公告)号：US09815810B1

公开(公告)日：2017-11-14

申请号：US15287615

申请日：2016-10-06

申请人： Deep Cell Industries Inc.

发明人： Kelly Ogilvie ,  Gary Bonilla

IPC分类号： C07D311/80 ,  C07D311/64 ,  B01D9/00 ,  C07C51/43

CPC分类号： C07D311/80 ,  B01D9/0009 ,  B01D9/0031 ,  B01D9/0036 ,  C07B2200/13 ,  C07C37/88 ,  C07C51/43 ,  C07D311/64 ,  C07C39/19 ,  C07C39/23

摘要： A method of cannabinoid preservation includes separating a cannabinoid ethanol (EtOH) mixture from a cannabis extract through a filtration process; forming a slurry by combining a crystalline compound with the cannabinoid EtOH mixture; heating and agitating the slurry in a pressurized chamber to form a colloidal cannabinoid EtOH mixture; distributing the colloidal cannabinoid EtOH mixture into a tray to form an evenly distributed mixture layer; forming an evaporation vessel for the evenly distributed mixture layer through the attachment of a detachable cover to the tray; positioning and heating the evaporation vessel within a heating chamber; performing a rapid cools process as the evenly distributed mixture layer approaches approaches saturation temperature; repeating the rapid cooling process until crystal formation is detected within the evenly distributed mixture layer; and/or removing the evaporation vessel from the heating chamber upon detection of crystal formation.