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    Phase change inks containing photoinitiator with phase change properties and gellant affinity
    2.
    发明授权
    Phase change inks containing photoinitiator with phase change properties and gellant affinity 失效
    含有相变性能和胶凝剂亲和力的光引发剂的相变油墨

    公开(公告)号：US07625956B2

    公开(公告)日：2009-12-01

    申请号：US11290202

    申请日：2005-11-30

    申请人： Peter G. Odell ,  Eniko Toma ,  Jennifer L. Belelie

    发明人： Peter G. Odell ,  Eniko Toma ,  Jennifer L. Belelie

    IPC分类号： B01F3/04

    CPC分类号： C09D11/101 ,  C08G69/26 ,  C09D11/34

    摘要： Disclosed is a phase change ink comprising a colorant, an initiator, and an ink vehicle, said ink vehicle comprising (a) at least one radically curable monomer compound, and (b) a compound of the formula wherein R1 is an alkylene, arylalkylene, or alkylarylene group, R2 and R2′ each, independently of the other, are alkylene, arylene, arylalkylene, or alkylarylene groups, R3 and R3′ each, independently of the other, are either (a) photoinitiating groups, or (b) groups which are alkyl, aryl, arylalkyl, or alkylaryl groups, provided that at least one of R3 and R3′ is a photoinitiating group, and X and X′ each, independently of the other, is an oxygen atom or a group of the formula —NR4—, wherein R4 is a hydrogen atom, an alkyl group, an aryl group, an arylalkyl group, or an alkylaryl group.

    摘要翻译： 公开了包含着色剂，引发剂和油墨载体的相变油墨，所述油墨载体包含（a）至少一种可自由基固化的单体化合物，和（b）下式化合物其中R 1是亚烷基，芳基亚烷基， 或烷基亚芳基，R 2和R 2'各自独立地为亚烷基，亚芳基，芳基亚烷基或烷基亚芳基，R 3和R 3'各自独立地为（a）光引发基团，或（b）基团 它们是烷基，芳基，芳基烷基或烷基芳基，条件是R 3和R 3'中的至少一个是光引发基团，X和X'各自独立地是氧原子或式 - NR4-，其中R4是氢原子，烷基，芳基，芳基烷基或烷基芳基。

    Processes for preparing bis(urea-urethane) compounds
    3.
    发明授权
    Processes for preparing bis(urea-urethane) compounds 有权
    制备双（脲 - 氨基甲酸酯）化合物的方法

    公开(公告)号：US07576235B2

    公开(公告)日：2009-08-18

    申请号：US11097758

    申请日：2005-04-01

    申请人： Rina Carlini ,  Adela Goredema ,  Eniko Toma ,  Christine E. Bedford

    发明人： Rina Carlini ,  Adela Goredema ,  Eniko Toma ,  Christine E. Bedford

    IPC分类号： C07C261/00 ,  C07C269/00

    CPC分类号： C07C273/1854 ,  C07C2601/14 ,  C07C275/26

    摘要： Processes for preparing bis(urea-urethane) compounds wherein R1 is alkyl, aryl, arylalkyl, or alkylaryl, R2 is alkylene, arylene, arylalkylene, or alkylarylene, R3 is alkylene, arylene, arylalkylene, or alkylarylene, and R4 is hydrogen or alkyl, comprising: (1) first bring to a reaction temperature of about 20-125° C. a reaction mixture comprising monoalcohol reactant R1—OH and diisocyanate reactant OCN—R2—NCO, the monoalcohol being present in an amount of about 0.8-1.2 moles monoalcohol per mole diisocyanate, the monoalcohol and diisocyanate reactants being admixed in a solvent, the reactants and solvent being present in relative amounts of at least about 1 milliliter solvent per millimole diisocyanate, the reaction temperature continuing until reaction between the monoalcohol and the diisocyanate is complete; and (2) subsequent to step (1), adding to the reaction mixture diamine without isolating the reaction product of step (1), thereby forming compound of the formula in desirably high yield and purity.

    摘要翻译： 制备双（脲 - 氨基甲酸酯）化合物的方法，其中R 1是烷基，芳基，芳基烷基或烷基芳基，R 2是亚烷基，亚芳基，芳基亚烷基或烷基亚芳基，R 3是亚烷基，亚芳基，芳基亚烷基或烷基亚芳基，R 4是氢或烷基 包括：（1）首先使约20-125℃的反应温度，包含一元醇反应物R1-OH和二异氰酸酯反应物OCN-R2-NCO的反应混合物，一元醇的存在量为约0.8-1.2 摩尔一元醇/摩尔二异氰酸酯，一元醇和二异氰酸酯反应物在溶剂中混合，反应物和溶剂以至少约1毫升溶剂/毫摩尔二异氰酸酯的相对量存在，直到一元醇与二异氰酸酯反应的反应温度为 完成; 和（2）在步骤（1）之后，在不分离步骤（1）的反应产物的情况下向反应混合物二胺中加入，从而以期望的高产率和纯度形成式的化合物。

    Phase change inks containing compounds derived from isocyanate, unsaturated alcohol, and polyol
    7.
    发明申请
    Phase change inks containing compounds derived from isocyanate, unsaturated alcohol, and polyol 有权
    相变油墨含有衍生自异氰酸酯，不饱和醇和多元醇的化合物

    公开(公告)号：US20070123641A1

    公开(公告)日：2007-05-31

    申请号：US11289883

    申请日：2005-11-30

    申请人： Jennifer Belelie ,  Rina Carlini ,  Eniko Toma

    发明人： Jennifer Belelie ,  Rina Carlini ,  Eniko Toma

    IPC分类号： C08G18/08

    CPC分类号： C08G18/755 ,  C08G18/2865 ,  C08G18/3206 ,  C08G18/6715 ,  C08G18/6735 ,  C09D175/16

    摘要： Disclosed is a phase change ink comprising a colorant, an initiator, and a phase change ink carrier, said carrier comprising (A) a first isocyanate-derived compound which is the reaction product of a mixture comprising (1) an isocyanate; and (2) a component comprising (a) an alcohol having at least one ethylenic unsaturation; (b) an amine having at least one ethylenic unsaturation; (c) an acid having at least one ethylenic unsaturation; or (d) mixtures thereof, (B) a second isocyanate-derived compound which is the reaction product of (1) a diisocyanate; (2) a monoalcohol having exactly one hydroxyl group and having at least one ethylenic unsaturation; and (3) a polyol having two or more hydroxyl groups, (C) an optional phase change inducing component, said phase change inducing component containing at least one hydroxyl group, said phase change inducing component having a melting point of about 40° C. or higher, and (D) an optional curable viscosity modifying ester, said ink being curable upon exposure to ultraviolet radiation.

    摘要翻译： 公开了一种相变油墨，其包含着色剂，引发剂和相变油墨载体，所述载体包含（A）第一异氰酸酯衍生化合物，其为包含（1）异氰酸酯的混合物的反应产物; 和（2）包含（a）具有至少一个烯属不饱和度的醇的组分; （b）具有至少一个烯属不饱和度的胺; （c）具有至少一个烯属不饱和度的酸; 或（d）其混合物，（B）第二异氰酸酯衍生化合物，其为（1）二异氰酸酯的反应产物; （2）具有正好一个羟基并具有至少一个烯属不饱和度的一元醇; 和（3）具有两个或多个羟基的多元醇，（C）任选的相变诱导组分，所述相变诱导组分含有至少一个羟基，所述相变诱导组分的熔点约为40℃。 或更高，和（D）任选的可固化粘度改性酯，所述油墨在暴露于紫外线辐射下是可固化的。

    Phase change inks containing curable amide gellant compounds
    8.
    发明申请
    Phase change inks containing curable amide gellant compounds 有权
    含有可固化酰胺胶凝剂化合物的相变油墨

    公开(公告)号：US20070123606A1

    公开(公告)日：2007-05-31

    申请号：US11290121

    申请日：2005-11-30

    申请人： Eniko Toma ,  Jennifer Belelie ,  Peter Odell

    发明人： Eniko Toma ,  Jennifer Belelie ,  Peter Odell

    IPC分类号： C09D11/00

    CPC分类号： C09D11/101 ,  C09D11/34

    摘要： Disclosed is a phase change ink comprising a colorant, an initiator, and a phase change ink carrier, said carrier comprising at least one radically curable monomer compound and a compound of the formula wherein R1 and R1′ each, independently of the other, is an alkyl group having at least one ethylenic unsaturation, an arylalkyl group having at least one ethylenic unsaturation, or an alkylaryl group having at least one ethylenic unsaturation, R2, R2′, and R3 each, independently of the others, are alkylene groups, arylene groups, arylalkylene groups, or alkylarylene groups, and n is an integer representing the number of repeat amide units and is at least 1. Also disclosed herein is a method of printing with the phase change ink.

    摘要翻译： 公开了一种相变油墨，其包含着色剂，引发剂和相变油墨载体，所述载体包含至少一种可自由基固化的单体化合物和下式化合物其中R 1和R 2 各自独立地是具有至少一个烯属不饱和度的烷基，具有至少一个烯属不饱和键的芳基烷基或具有至少一个烯属不饱和键的烷基芳基，R“ R 2，R 2，R 3和R 3各自独立地为亚烷基，亚芳基，芳基亚烷基或烷基亚芳基，n 是表示重复酰胺单元数的整数，并且至少为1.本文还公开了用相变油墨印刷的方法。

    Radiation curable ink containing gellant and radiation curable wax
    9.
    发明授权
    Radiation curable ink containing gellant and radiation curable wax 有权
    含有胶凝剂和可辐射固化蜡的可辐射固化油墨

    公开(公告)号：US08142557B2

    公开(公告)日：2012-03-27

    申请号：US11427172

    申请日：2006-06-28

    申请人： Jennifer L. Belelie ,  Peter G. Odell ,  Eniko Toma ,  Christopher A. Wagner ,  C. Geoffrey Allen ,  Stephan V. Drappel

    发明人： Jennifer L. Belelie ,  Peter G. Odell ,  Eniko Toma ,  Christopher A. Wagner ,  C. Geoffrey Allen ,  Stephan V. Drappel

    IPC分类号： C09D11/00 ,  B01F3/04

    CPC分类号： C09D11/101 ,  C09D11/34

    摘要： Radiation curable phase change ink comprising an ink vehicle that includes at least one curable carrier, at least one gellant, at least one curable wax and at least one photoinitiator. In a method of forming an image with the ink, the radiation curable phase change ink is melted, then jetted onto an image receiving substrate, wherein the radiation curable phase change ink forms a gel state, and exposed to ultraviolet light to cure the curable components of the radiation curable phase change ink. The wax cures into the structure of the ink, thereby generating a robust image of excellent gloss.

    摘要翻译： 包含油墨载体的可辐射固化相变油墨，其包含至少一种可固化载体，至少一种胶凝剂，至少一种可固化蜡和至少一种光引发剂。 在用油墨形成图像的方法中，将可辐射固化相变油墨熔化，然后喷射到图像接收基板上，其中可辐射固化相变油墨形成凝胶状态，并暴露于紫外光以固化可固化组分 的可辐射固化相变油墨。 蜡固化成油墨的结构，从而产生具有优异光泽的坚固的图像。

    Phase change inks containing curable amide gellant compounds
    10.
    发明授权
    Phase change inks containing curable amide gellant compounds 有权
    含有可固化酰胺胶凝剂化合物的相变油墨

    公开(公告)号：US07714040B2

    公开(公告)日：2010-05-11

    申请号：US11290121

    申请日：2005-11-30

    申请人： Eniko Toma ,  Jennifer L. Belelie ,  Peter G. Odell

    发明人： Eniko Toma ,  Jennifer L. Belelie ,  Peter G. Odell

    IPC分类号： C09D11/00 ,  G01D11/00

    CPC分类号： C09D11/101 ,  C09D11/34

    摘要： Disclosed is a phase change ink comprising a colorant, an initiator, and a phase change ink carrier, said carrier comprising at least one radically curable monomer compound and a compound of the formula wherein R1 and R1′ each, independently of the other, is an alkyl group having at least one ethylenic unsaturation, an arylalkyl group having at least one ethylenic unsaturation, or an alkylaryl group having at least one ethylenic unsaturation, R2, R2′, and R3 each, independently of the others, are alkylene groups, arylene groups, arylalkylene groups, or alkylarylene groups, and n is an integer representing the number of repeat amide units and is at least 1. Also disclosed herein is a method of printing with the phase change ink.

    摘要翻译： 公开了一种相变油墨，其包含着色剂，引发剂和相变油墨载体，所述载体包含至少一种可自由基固化的单体化合物和下式化合物：其中R 1和R 1'各自独立地为 具有至少一个烯属不饱和基团的烷基，具有至少一个烯属不饱和基团的芳基烷基或具有至少一个烯属不饱和键的烷基芳基，R 2，R 2'和R 3各自独立地为亚烷基，亚芳基 ，芳基亚烷基或烷基亚芳基，n是表示重复酰胺单元数的整数，并且至少为1.本文还公开了用相变油墨印刷的方法。