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公开(公告)号：US09284657B2
公开(公告)日：2016-03-15
申请号：US14361143
申请日：2011-11-30
摘要： A replenisher which is capable of supplying Zr ions to a metal surface treatment solution, while suppressing an increase in the HF concentration in the metal surface treatment solution, so that a chemical conversion coating film can be continuously formed on a steel sheet by electrolysis and contains (A) zirconium hydrofluoric acid or a salt thereof and/or (B) hydrofluoric acid or a salt thereof and (C) a fluorine-free zirconium compound. The total concentration (g/l) of zirconium ions derived from the components (A) and (C) is 20 or more, and the ratio of the total molar amount (MF) of the fluorine ions derived from the components (A) and (B) relative to the total molar amount (MZr) of the zirconium ions derived from the components (A) and (C), namely MF/MZr is 0.01 or more but less than 4.00.
摘要翻译： 能够在金属表面处理液中抑制金属表面处理液中的HF浓度上升的同时能够向金属表面处理液供给Zr离子的补充剂，能够通过电解在钢板上连续地形成化学转化膜， （A）氢氟酸锆或其盐和/或（B）氢氟酸或其盐和（C）无氟锆化合物。 从（A）成分和（C）成分得到的锆离子的总浓度（g / l）为20以上，来自（A）成分的氟离子的总摩尔量（MF） （A）和（C）衍生的锆离子的总摩尔量（MZr），即MF / MZr为0.01以上且小于4.00。
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公开(公告)号：US20150021192A1
公开(公告)日：2015-01-22
申请号：US14361143
申请日：2011-11-30
摘要： The purpose of the present invention is to provide a replenisher which is capable of supplying Zr ions to a metal surface treatment solution, while suppressing an increase in the HF concentration in the metal surface treatment solution, so that a chemical conversion coating film can be continuously formed on a steel sheet by electrolysis. A replenisher of the present invention is a replenisher which is used for the purpose of supplying zirconium ions to a metal surface treatment solution that contains zirconium ions and fluorine ions, and the replenisher contains (A) zirconium hydrofluoric acid or a salt thereof and/or (B) hydrofluoric acid or a salt thereof and (C) a fluorine-free zirconium compound. The total concentration (g/l) of zirconium ions derived from the components (A) and (C) is 20 or more, and the ratio of the total molar amount (MF) of the fluorine ions derived from the components (A) and (B) relative to the total molar amount (MZr) of the zirconium ions derived from the components (A) and (C), namely MF/MZr is 0.01 or more but less than 4.00.
摘要翻译： 本发明的目的是提供一种能够在抑制金属表面处理溶液中的HF浓度增加的同时向金属表面处理溶液供给Zr离子的补充剂，从而能够连续地进行化学转化覆膜 通过电解在钢板上形成。 本发明的补充剂是用于将锆离子供给到含有锆离子和氟离子的金属表面处理溶液中的补充剂，补充剂含有（A）氢氟酸锆或其盐和/或 （B）氢氟酸或其盐和（C）无氟锆化合物。 从（A）成分和（C）成分得到的锆离子的总浓度（g / l）为20以上，来自（A）成分的氟离子的总摩尔量（MF） （A）和（C）衍生的锆离子的总摩尔量（MZr），即MF / MZr为0.01以上且小于4.00。
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