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公开(公告)号：US11433697B2
公开(公告)日：2022-09-06
申请号：US17264851
申请日：2019-08-22
申请人： Hirotoshi Ishida
发明人： Hirotoshi Ishida
IPC分类号： B42F1/12
摘要： A clip includes an insertion piece insertable into a valley formed by folding a corner of a stack of a plurality of paper pieces, a front-side clamping piece contactable with a paper piece portion on a front side of the valley, and a back-side clamping piece contactable with a paper piece portion on a back side of the valley. The insertion piece, front-side clamping piece, and back-side clamping piece are elastically and integrally formed so that the paper piece portion on the front side and the paper piece portion on the back side of the valley are clamped between the front-side clamping piece and the insertion piece and between the insertion piece and the back-side clamping piece, respectively, and both of the paper piece portion on the front side and the paper piece portion on the back side of the valley are clamped between the front-side and back-side clamping pieces.
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公开(公告)号：US06790470B1
公开(公告)日：2004-09-14
申请号：US09708006
申请日：2000-11-08
IPC分类号： A23L1236
CPC分类号： C07K5/06113
摘要： For example, N-[N-(3,3-dimethylbutyl)-L-&agr;-aspartyl]-L-phenylalanine methyl ester (A-type crystal) showing characteristic peaks in diffractive X-ray at diffraction angles (2&thgr;, CuK&agr; ray) of at least 6.0°, 24.8°, 8.2° and 16.5° is dried to its water content below 3% by weight. The crystal thus dried is a novel crystal (C-type crystal) of N-[N-(3,3-dimethylbutyl)-L-&agr;-aspartyl]-L-phenylalanine methyl ester excellent in dissolution rate, and when measured by powder X-ray diffractometry, this crystal shows characteristic peaks in diffractive X-ray at diffraction angles (2&thgr;, CuK&agr; ray) of at least 7.1°, 19.8°, 17.3° and 17.7°. The dissolution rate (solubility) of the C-type crystals is further improved by converting the crystals into granules.
摘要翻译： 例如，在衍射角衍射X射线（2θ，CuKalpha射线）中显示特征峰的N- [N-（3,3-二甲基丁基）-L-α-天冬氨酰基] -L-苯丙氨酸甲酯（A型晶体） ）至少为6.0°，24.8°，8.2°和16.5°，其水分含量低于3重量％。 这样干燥的晶体是溶解速度优异的N- [N-（3,3-二甲基丁基）-L-α-天冬氨酰基] -L-苯丙氨酸甲酯的新晶体（C型晶体），当用粉末 X射线衍射法，该晶体在衍射角（2θ，CuKalpha射线）的衍射X射线中显示出至少7.1°，19.8°，17.3°和17.7°的特征峰。 通过将晶体转化为颗粒，进一步提高了C型晶体的溶解速率（溶解度）。
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公开(公告)号：US06399132B1
公开(公告)日：2002-06-04
申请号：US09581181
申请日：2000-08-14
IPC分类号： A23L1236
CPC分类号： A23L27/32
摘要： Herein is disclosed a sweetener composition containing Aspartame and Acesulfame-K as active ingredients, wherein the amount of Acesulfame-K is 5 to 90% by weight based on the total amount of both the components and wherein the particle sizes of the both the components are respectively selected from within the range of the particle size which allows the dissolution rate of the mixture to be higher than that of Aspartame alone, in which sweetener composition the poorly dissoluble, high intense synthetic sweetener Aspartame (APM) is improved in solubility.
摘要翻译： 本文公开了含有天冬甜素和乙酰磺胺酸钾作为活性成分的甜味剂组合物，其中基于两种组分的总量，乙酰磺胺酸钾的量为5至90重量％，并且其中两种组分的颗粒尺寸为 分别选自允许混合物的溶解速率高于天冬甜素单独的粒度的范围内，其中甜味剂组合物不易溶解的高强度合成甜味剂阿斯巴甜（APM）的溶解度提高。
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公开(公告)号：US06372278B1
公开(公告)日：2002-04-16
申请号：US09707953
申请日：2000-11-08
IPC分类号： A23L1236
CPC分类号： C07K5/06113 , A23L27/32
摘要： One embodiment of the present invention provides a sweetener composition, which includes N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl}-L-phenylalanine 1-methyl ester, and Aspartame, wherein a ratio of the Aspartame to a total amount of the Aspartame and the N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl}-L-phenylalanine 1-methyl ester is in the range of 10 to 99.5% by weight, methods of making and of using. Another embodiment of the present invention provides a method for preparing a sweetener composition, which includes drying an A-type crystal of N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl }-L-phenylalanine 1-methyl ester to obtain a C-type crystal of N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl }-L-phenylalanine 1-methyl ester. Another embodiment of the present invention provides a method for producing a sweetener, which includes admixing N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl }-L-phenylalanine 1-methyl ester with Aspartame, wherein a ratio of the Aspartame to a total amount of the N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl }-L-phenylalanine 1-methyl ester and the Aspartame is in the range of 10 to 99.5% by weight. Another embodiment of the present invention provides a method for improving the dissolution rate of N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl }-L-phenylalanine 1-methyl ester, which includes, prior to dissolving the N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl }-L-phenylalanine 1-methyl ester, admixing the N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl }-L-phenylalanine 1-methyl ester with Aspartame, wherein a ratio of the Aspartame to a total amount of the N-{N-(3,3-dimethylbutyl)-L&agr;-aspartyl}-L-phenylalanine 1-methyl ester and the Aspartame is in the range of 10 to 99.5% by weight.
摘要翻译： 本发明的一个实施方案提供了一种甜味剂组合物，其包括N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯和天冬甜素，其中天冬甜素 至总量的天冬甜素和N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯的重量百分比为10〜99.5重量％ 制作和使用。 本发明的另一个实施方案提供了一种制备甜味剂组合物的方法，其包括将N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲基 得到N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯的C型结晶。 本发明的另一个实施方案提供一种生产甜味剂的方法，其包括将N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯与天冬甜素混合，其中比例 的天冬甜素与总量的N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯和天冬甜素的比例在10至99.5重量％的范围内 。 本发明的另一个实施方案提供了一种改善N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯的溶解速率的方法，其包括在将 N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯，将N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} 具有天冬甜素的L-苯丙氨酸1-甲酯，其中天冬甜素与N- {N-（3,3-二甲基丁基）-Lα-天冬氨酰基} -L-苯丙氨酸1-甲酯和天冬甜精的总量的比例 在10至99.5重量％的范围内。
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公开(公告)号：US20210229485A1
公开(公告)日：2021-07-29
申请号：US17264851
申请日：2019-08-22
申请人： Hirotoshi ISHIDA
发明人： Hirotoshi ISHIDA
IPC分类号： B42F1/12
摘要： A clip includes an insertion piece insertable into a valley formed by folding a corner of a stack of a plurality of paper pieces, a front-side clamping piece contactable with a paper piece portion on a front side of the valley, and a back-side clamping piece contactable with a paper piece portion on a back side of the valley. The insertion piece, front-side clamping piece, and back-side clamping piece are elastically and integrally formed so that the paper piece portion on the front side and the paper piece portion on the back side of the valley are clamped between the front-side clamping piece and the insertion piece and between the insertion piece and the back-side clamping piece, respectively, and both of the paper piece portion on the front side and the paper piece portion on the back side of the valley are clamped between the front-side and back-side clamping pieces.
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公开(公告)号：US20190128723A1
公开(公告)日：2019-05-02
申请号：US16151687
申请日：2018-10-04
发明人： Hirotoshi ISHIDA , Akio NAKAMURA , Katsuya FUNAKOSHI , Tatsushi SHIBUYA , Maiko KIKUCHI , Takashi ARITA , Eiji YUMOTO , Mitsuhiro SEKIZAWA
IPC分类号： G01F22/00 , G01G23/48 , G01G19/415 , G08B21/18 , B65D25/20
摘要： A measuring device includes: a holding device that holds a container containing a measured object detachably; a measuring unit that measures a weight of the container or a volume of the measured object; a calculation unit configured to calculate an amount of use of the measured object based on the weight or the volume measured by the measuring unit and a last measurement result by the measuring unit; and a communication device that transmits the amount of use of the measured object to an external terminal.
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公开(公告)号：US06706304B1
公开(公告)日：2004-03-16
申请号：US09581180
申请日：2000-07-14
IPC分类号： A23L1236
CPC分类号： A23L27/32
摘要： Herein is disclosed a granulated sweetener comprising Aspartame and Acesulfame-K as active ingredients, wherein the amount of the Acesulfame-K is 5 to 90% by weight based on the total amount of both the components and wherein the maximum particle size of the granules is about 1,400 &mgr;m or less, in which granulated sweetener the poorly dissoluble, high intense synthetic sweetener Aspartame (APM) is improved in solubility.
摘要翻译： 本文公开了包含天冬甜素和乙酰磺胺酸K作为活性成分的颗粒状甜味剂，其中基于两种成分的总量，所述乙酰磺胺酸钾的量为5-90重量％，并且其中所述颗粒的最大粒径为 约1400毫克或更少，其中颗粒状甜味剂不易溶解，高强度合成甜味剂天冬甜精（APM）的溶解度提高。
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公开(公告)号：US06372279B1
公开(公告)日：2002-04-16
申请号：US09707954
申请日：2000-11-08
IPC分类号： A23L1236
CPC分类号： A23L27/32
摘要： One embodiment of the present invention provides a sweetener composition, which includes a mixture of N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl}-L-phenylalanine 1-methyl ester, and Acesulfame K, wherein a ratio of the Acesulfame K to a total amount of the N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl}-L-phenylalanine 1-methyl ester and the Acesulfame K is in the range of 10 to 97% by weight, methods of making and of using. Another embodiment of the present invention provides a method for preparing a sweetener composition, which includes drying an A-type crystal of N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl}-L-phenylalanine 1-methyl ester to obtain a C-type crystal of N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl}-L-phenylalanine 1-methyl ester. Another embodiment of the present invention provides a method for producing a sweetener, which includes admixing N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl}-L-phenylalanine 1-methyl ester with Acesulfame K, wherein a ratio of the Acesulfame K to a total amount of the N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl}-L-phenylalanine 1-methyl ester and the Acesulfame K is in the range of 10 to 97% by weight. Another embodiment of the present invention provides a method for improving the dissolution rate of N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl}-L-phenylalanine 1-methyl ester, which includes, prior to dissolving the N-{N-(3,3 -dimethylbutyl)-L-&agr;-aspartyl}-L-phenylalanine 1-methyl ester, admixing the N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl}-L-phenylalanine 1-methyl ester with Acesulfame K, wherein a ratio of the Acesulfame K to a total amount of the N-{N-(3,3-dimethylbutyl)-L-&agr;-aspartyl}-L-phenylalanine 1-methyl ester and the Acesulfame K is in the range of 10 to 97% by weight.
摘要翻译： 本发明的一个实施方案提供一种甜味剂组合物，其包括N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯和乙酰磺胺酸K的混合物，其中a 乙酰磺胺酸钾与N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯和乙酰磺胺酸钾的总量的比例在10至97的范围内 重量％，制造方法和使用方法。 本发明的另一个实施方案提供了一种制备甜味剂组合物的方法，其包括将N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲基 得到N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯的C型晶体。 本发明的另一个实施方案提供了一种生产甜味剂的方法，其包括将N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯与乙酰磺胺酸K混合，其中 乙酰磺胺酸钾与N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯和乙酰磺胺酸钾的总量的比例在10至97的范围内 重量％。 本发明的另一个实施方案提供了一种改善N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯的溶解速率的方法，其包括在溶解 N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲酯，混合N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} L-苯丙氨酸1-甲酯与乙酰磺胺酸K，其中乙酰磺胺酸钾与N- {N-（3,3-二甲基丁基）-L-α-天冬氨酰基} -L-苯丙氨酸1-甲基酯的总量的比例 酯和丁磺克烷K的重量百分比在10至97％的范围内。
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