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1.发明授权Ionic liquids processing of biomass to reducing sugars and other dehydration products 有权离子液体处理生物质还原糖和其他脱水产品公开(公告)号：US08575374B1
公开(公告)日：2013-11-05
申请号：US12908986
申请日：2010-10-21
IPC分类号： C07D303/02
CPC分类号： C07D233/60
摘要： The present invention describes the use of an ionic liquid acid catalyst for the hydrolysis of cellulose into reducing sugars and other degradation products. The use of an ionic liquid catalyst for the hydrolysis of cellulose provides a low volatility catalyst and eliminates the hazards associated with the handling of mineral acids. Conditions such as temperature, catalyst modification, and ionic liquid solvent control the production of reducing sugars and other products. The combination of using an ionic liquid as the solvent for cellulose and ionic liquid catalyst provides an unprecedented tunability of the reaction properties giving more control over the conversion process to produce dehydration products with higher yields depending on the desired feedstock.
摘要翻译： 本发明描述了离子液体酸催化剂用于将纤维素水解成还原糖和其它降解产物的用途。 使用离子液体催化剂水解纤维素提供低挥发性催化剂，并消除与无机酸的处理有关的危害。 条件如温度，催化剂改性和离子液体溶剂控制生产还原糖等产品。 使用离子液体作为纤维素和离子液体催化剂的溶剂的组合提供了前所未有的反应性质的可调性，从而更好地控制转化过程以根据所需原料以更高的产率生产脱水产物。
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公开(公告)号：US08202379B1
公开(公告)日：2012-06-19
申请号：US12629915
申请日：2009-12-03
CPC分类号： D04H1/4266 , D04H1/425 , D04H1/587 , D04H1/64 , D04H1/645 , D04H3/015 , D04H3/14 , D06M13/473 , D06M2101/06
摘要： Natural fiber welding is a process by which individual fibers are swollen by an appropriate ionic liquid-based solvent system to form a congealed network. Manipulated fibrous materials may be either composed of natural polymers such as cellulose, hemicellulose, silk, et cetera, or synthetic polymers, or mixed materials. The process is principally controlled by the composition of the solvent system which includes an ionic liquid solvent plus additives such as water, methanol, et cetera. Other conditions such as the amount and placement of solvent, as well as time, temperature, and pressure control the extent to which neighboring fibers are fused. Only the material at the outer surface of fibers need be sufficiently mobile to merge with that of neighboring fibers. Material in the fiber core may be left in the native state by controlling process variables. Fibers form a congealed network upon removal of the ionic liquid-based solvent.
摘要翻译： 天然纤维焊接是通过适当的基于离子液体的溶剂系统使单个纤维溶胀以形成凝结网络的过程。 操作的纤维材料可以由天然聚合物如纤维素，半纤维素，丝绸等或合成聚合物或混合材料组成。 该方法主要由包括离子液体溶剂和添加剂如水，甲醇等的溶剂体系的组成控制。 其它条件，例如溶剂的量和位置，以及时间，温度和压力控制相邻纤维融合的程度。 只有纤维外表面的材料需要足够的移动才能与相邻纤维的材料合并。 纤维芯中的材料可以通过控制过程变量而保持在天然状态。 在除去离子液体基溶剂后，纤维形成凝结网络。
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3.发明授权公开(公告)号：US07682539B1
公开(公告)日：2010-03-23
申请号：US11655041
申请日：2007-01-10
IPC分类号： D01F4/00
摘要： The present invention relates to a process of forming fibers of silk and silk-like proteins in a solution with a solvent consisting of a pure ionic liquid, an ionic liquid mixture, an ionic liquid mixed with one or more cosolvents, or an ionic liquid mixture mixed with one or more cosolvents. A solution is extruded through a spinneret orifice to form a fiber. The spinneret is either directly immersed in the coagulation bath or the spinneret is surrounded by a noncoagulating medium (i.e., air or other inert fluid) and the extruded fiber is subsequently immersed in a coagulation bath. Fibers may also be formed by extruding a fiber directly from a reservoir of solution into a noncoagulating, inert medium and then immersing the extruded fibers into a coagulation bath to rinse the fiber of ionic liquid.
摘要翻译： 本发明涉及在具有由纯离子液体，离子液体混合物，与一种或多种助溶剂混合的离子液体或离子液体混合物的溶剂的溶液中形成丝和丝状蛋白质纤维的方法 与一种或多种助溶剂混合。 通过喷丝孔挤出溶液以形成纤维。 将喷丝头直接浸入凝固浴中，或者喷丝头被非凝固介质（即空气或其它惰性流体）包围，随后将挤出的纤维浸入凝固浴中。 纤维也可以通过将纤维直接从溶液储存器挤出到非凝固的惰性介质中，然后将挤出的纤维浸入凝结浴中以漂洗离子液体的纤维而形成。
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公开(公告)号：US07671178B1
公开(公告)日：2010-03-02
申请号：US11326678
申请日：2005-12-29
IPC分类号： C07K14/00
CPC分类号： C07K1/145 , C07K14/43586
摘要： Silk is dissolved in an ionic liquid and is regenerated in a range of structural forms without requiring the use of harmful solvents. Silk solubility can be controlled by the selection of the ionic liquid constituents, with small cations and halide or pseudohalide anions favoring solution. The rinse solvent exercises a significant influence over the final properties of the regenerated silk.
摘要翻译： 丝绸溶解在离子液体中，并且在一定范围的结构形式中再生，而不需要使用有害溶剂。 可以通过选择离子液体成分来控制丝溶性，小型阳离子和卤化物或拟卤化物阴离子有利于溶液。 冲洗溶剂对再生丝绸的最终性能产生重大影响。
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