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1.发明授权
公开(公告)号：US4169107A
公开(公告)日：1979-09-25
申请号：US838368
申请日：1977-09-30
申请人： Shiro Asano , Kiyotaka Yoshimura , Masao Hashimoto
发明人： Shiro Asano , Kiyotaka Yoshimura , Masao Hashimoto
IPC分类号： C07D213/82 , B01J23/00 , B01J23/72 , B01J25/00 , B01J27/00 , B01J27/24 , C07B61/00 , C07C67/00 , C07C231/00 , C07C231/06 , C07C233/09 , C07D213/81 , C07C102/08
CPC分类号： C07D213/81 , B01J23/72 , B01J27/24
摘要： An improved process for converting acrylonitrile to the corresponding amide by hydrating said nitrile in the presence of a metallic copper catalyst and aluminum nitrate as promoter for said catalyst.
摘要翻译： 通过在金属铜催化剂和硝酸铝作为催化剂的助催化剂存在下使所述腈水合而将丙烯腈转化成相应的酰胺的改进方法。
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公开(公告)号：US3962333A
公开(公告)日：1976-06-08
申请号：US617973
申请日：1975-09-25
申请人： Kiyotaka Yoshimura , Shiro Asano , Tadatoshi Honda
发明人： Kiyotaka Yoshimura , Shiro Asano , Tadatoshi Honda
IPC分类号： C07C233/09 , C07C103/08
CPC分类号： C07C233/09
摘要： An improved process for preparing acrylamide or methacrylamide which process comprises the step of reacting acrylonitrile or methacrylonitrile with water in the presence of a catalyst system consisting of a metallic copper containing catalyst and a copper salt promoter, said copper salt being copper sulfate, copper nitrate, copper halide, or a copper salt of a lower fatty acid.
摘要翻译： 一种制备丙烯酰胺或甲基丙烯酰胺的改进方法，该方法包括在由含金属铜催化剂和铜盐促进剂组成的催化剂体系存在下使丙烯腈或甲基丙烯腈与水反应的步骤，所述铜盐是硫酸铜，硝酸铜， 卤化铜或低级脂肪酸的铜盐。
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公开(公告)号：US3951600A
公开(公告)日：1976-04-20
申请号：US311900
申请日：1972-12-04
IPC分类号： C07C231/22 , C07C67/00 , C07C231/00 , C07C231/06 , C07C233/09 , A61L13/00 , C07C103/08
CPC分类号： C07C233/09
摘要： There is disclosed a method for handling acrylamide aqueous solutions with safety wherein acrylamide aqueous solutions obtained through catalytic hydration reaction of acrylonitrile are handled using utensils made from phenol resin, polyethylene, polypropylene, polyvinylchloride resin or fluorine-containing resin or glass or using such utensils that are provided with linings formed by these materials.
摘要翻译： 公开了一种安全处理丙烯酰胺水溶液的方法，其中通过丙烯腈的催化水合反应获得的丙烯酰胺水溶液是使用由酚醛树脂，聚乙烯，聚丙烯，聚氯乙烯树脂或含氟树脂或玻璃制成的器具处理的，或者使用这样的器具 设置有由这些材料形成的衬里。
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公开(公告)号：US3985806A
公开(公告)日：1976-10-12
申请号：US279309
申请日：1972-08-10
IPC分类号： B01J8/20 , B01J8/22 , C07C20060101 , C07C67/00 , C07C231/00 , C07C231/06 , C07C233/09 , C07C103/133
CPC分类号： B01J23/72
摘要： A process for continuously manufacturing acrylamide by hydrating acrylonitrile in the presence of a free metallic copper catalyst, characterized in that a reactor is employed, which is internally partitioned into a catalyst slurry circulating section and a catalyst precipitating section, and that raw materials and supplementary catalyst are supplied continuously into the reactor and at the same time the clear reaction liquid and a portion of the catalyst are continuously taken out of the reactor so that the properties of the catalyst are maintained constant.
摘要翻译： 一种在游离金属铜催化剂存在下通过水合丙烯腈连续制造丙烯酰胺的方法，其特征在于使用反应器，其内部分隔成催化剂淤浆循环段和催化剂沉淀段，原料和辅助催化剂 连续供入反应器，同时将澄清反应液和一部分催化剂连续地从反应器中取出，使得催化剂的性质保持恒定。
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公开(公告)号：US3941837A
公开(公告)日：1976-03-02
申请号：US473551
申请日：1974-05-28
申请人： Shiro Asano , Kiyotaka Yoshimura , Masao Hashimoto
发明人： Shiro Asano , Kiyotaka Yoshimura , Masao Hashimoto
IPC分类号： C07C231/06 , C07C20060101 , C07C67/00 , C07C231/00 , C07C231/22 , C07C231/24 , C07C233/09 , C07C103/08
CPC分类号： B01J23/72
摘要： A method of purifying an aqueous solution of acrylamide, which has been formed by reacting acrylonitrile with water in the presences of the metallic copper catalyst, and which contains cuprous ions, comprising treating said aqueous solution in a reaction zone which is substantially free of an oxygen containing gas or liquid.
摘要翻译： 一种净化丙烯酰胺水溶液的方法，该方法是在金属铜催化剂的存在下，使丙烯腈与水反应形成的并含有亚铜离子的方法，包括在基本上不含氧的反应区中处理所述水溶液 含气体或液体。
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公开(公告)号：US4032572A
公开(公告)日：1977-06-28
申请号：US637416
申请日：1975-12-03
IPC分类号： C07C233/09 , C07C103/08
CPC分类号： C07C233/09 , Y10S159/10
摘要： A method for economically concentrating an acrylamide aqueous solution by catalytic hydration without substantial deterioration in the product. According to the method, an acrylamide aqueous solution obtained from catalytic hydration, is concentrated by distillation while maintaining the solution in good contact with at least 0.1 mole. or more of air per mole of water distilled from the acrylamide aqueous solution.
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