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1.发明申请Liquid-Liquid Extraction Composition Useful In Processing Water-Soluble Surfactants 审中-公开液体 - 液体萃取组合物可用于加工水溶性表面活性剂公开(公告)号：US20130032748A1
公开(公告)日：2013-02-07
申请号：US13564841
申请日：2012-08-02
IPC分类号： C09K3/00
摘要： Compositions useful in liquid-liquid extraction processes for improving the taste of water-soluble surfactants, said composition comprising: from about 5% to about 60%, by weight of the composition, of water soluble surfactant; from about 10% to about 90%, by weight of the composition, of water; from about 10% to about 90%, by weight of the composition, of extraction solvent; at least 0.01%, by weight of the composition, of undesirable non-polar materials; wherein the extraction solvent is selected from solvents having individual Hansen solubility parameters of a dispersion force component (δD) ranging from about 15 to about 17 (MPa)0.5, a polar component (δP) ranging from 0 to about 9 (MPa)0.5 and a hydrogen bonding component (δH) ranging from 0 to about 11 (MPa)0.5.
摘要翻译： 用于提高水溶性表面活性剂的味道的液体 - 液体萃取方法中的组合物，所述组合物包含：组合物重量的约5％至约60％的水溶性表面活性剂; 约10重量％至约90重量％的水; 约10重量％至约90重量％的提取溶剂; 至少0.01重量％的组合物，不期望的非极性材料; 其中所述提取溶剂选自具有约15至约17（MPa）0.5范围内的分散力分量（δD）和0至约9（MPa）0.5范围内的极性组分（δP）的各个Hansen溶解度参数的溶剂和 0〜11（MPa）的氢键成分（δH）为0.5。
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公开(公告)号：US20110280814A1
公开(公告)日：2011-11-17
申请号：US13105181
申请日：2011-05-11
摘要： Processes for preparing an oral care composition having improved taste, color, odor and/or clarity, wherein said processes comprise the steps of: providing an unfiltered dentifrice component selected from unfiltered alkyl phosphate surfactants, alkyl phosphate ethoxylated surfactants, lauryl sulfate surfactants, betaine surfactants, antibacterial agents, cetyl pyridinium chloride, metal Salts, phytic acids, or mixtures thereof; filtering the unfiltered dentifrice component with an adsorbent to form a filtered dentifrice component; and incorporating the filtered dentifrice component into the oral care composition. In one such process, activated carbon with a median particle size of less than or equal to about 30 μm, optionally a macro-mesoporous:microporous ratio about 0.9 or higher and optionally a BET per Total Volume of equal to or less than about 1600 m̂2/g, has been found to remove undesirable contaminants from oral care dentifrice components, such as alkyl phosphate surfactant, alkyl phosphate ethoxylated surfactant, lauryl sulfate surfactant, betaine surfactants, antibacterial agents, cetyl pyridinium chloride, metal salts, or phytic acid.
摘要翻译： 制备具有改善的味道，颜色，气味和/或透明度的口腔护理组合物的方法，其中所述方法包括以下步骤：提供未过滤的洁齿剂组分，其选自未过滤的烷基磷酸盐表面活性剂，烷基磷酸盐乙氧基化表面活性剂，月桂基硫酸盐表面活性剂，甜菜碱表面活性剂 ，抗菌剂，氯化十六烷基吡啶，金属盐，植酸或其混合物; 用吸附剂过滤未过滤的洁牙剂组分以形成过滤的洁牙剂组分; 并将经过滤的洁牙剂组分并入口腔护理组合物中。 在一种这样的方法中，中值粒度小于或等于约30μm的活性炭，任选的大孔介孔：微孔比为约0.9或更高，任选的BET总体积等于或小于约1600m 2 已经发现，从口腔护理洁齿剂组分如磷酸烷基酯表面活性剂，烷基磷酸乙氧基化表面活性剂，月桂基硫酸盐表面活性剂，甜菜碱表面活性剂，抗菌剂，十六烷基吡啶鎓氯化物，金属盐或植酸中除去不需要的污染物。
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公开(公告)号：US08609070B2
公开(公告)日：2013-12-17
申请号：US13105181
申请日：2011-05-11
摘要： Processes for preparing an oral care composition having improved taste, color, odor and/or clarity, wherein said processes comprise the steps of: providing an unfiltered dentifrice component selected from unfiltered alkyl phosphate surfactants, alkyl phosphate ethoxylated surfactants, lauryl sulfate surfactants, betaine surfactants, antibacterial agents, cetyl pyridinium chloride, metal Salts, phytic acids, or mixtures thereof; filtering the unfiltered dentifrice component with an adsorbent to form a filtered dentifrice component; and incorporating the filtered dentifrice component into the oral care composition. In one such process, activated carbon with a median particle size of less than or equal to about 30 μm, optionally a macro-mesoporous:microporous ratio about 0.9 or higher and optionally a BET per Total Volume of equal to or less than about 1600 m^2/g, has been found to remove undesirable contaminants from oral care dentifrice components, such as alkyl phosphate surfactant, alkyl phosphate ethoxylated surfactant, lauryl sulfate surfactant, betaine surfactants, antibacterial agents, cetyl pyridinium chloride, metal salts, or phytic acid.
摘要翻译： 制备具有改善的味道，颜色，气味和/或透明度的口腔护理组合物的方法，其中所述方法包括以下步骤：提供未过滤的洁齿剂组分，其选自未过滤的烷基磷酸盐表面活性剂，烷基磷酸盐乙氧基化表面活性剂，月桂基硫酸盐表面活性剂，甜菜碱表面活性剂 ，抗菌剂，氯化十六烷基吡啶，金属盐，植酸或其混合物; 用吸附剂过滤未过滤的洁牙剂组分以形成过滤的洁牙剂组分; 并将经过滤的洁牙剂组分并入口腔护理组合物中。 在一种这样的方法中，中值粒度小于或等于约30μm的活性炭，任选的大孔介孔：微孔比为约0.9或更高，任选的BET总体积等于或小于约1600μm 已经发现，从口腔护理洁齿剂组分如磷酸烷基酯表面活性剂，烷基磷酸乙氧基化表面活性剂，月桂基硫酸盐表面活性剂，甜菜碱表面活性剂，抗菌剂，十六烷基吡啶鎓氯化物，金属盐或植酸中除去不期望的污染物。
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公开(公告)号：US09078826B2
公开(公告)日：2015-07-14
申请号：US13564853
申请日：2012-08-02
摘要： Treated surfactant composition containing a water-soluble surfactant and exhibiting improved taste, said composition comprising: a water-soluble surfactant selected from alkyl phosphate surfactants, alkyl phosphate ethoxylated surfactants, betaine surfactants, betaine ethoxylated surfactants, amine oxide surfactants, and mixtures thereof and water; wherein the composition further comprises: less than about 4%, by weight of the water-soluble surfactant, of total undesirable non-polar materials; less than about 2.5%, by weight of the water-soluble surfactant, of alcohols having a carbon chain length of greater than 4; less than about 1%, by weight of the water-soluble surfactant, of amine and amide materials; and less than about 1%, by weight of the water-soluble surfactant, undesirable non-polar materials selected from aldehydes, esters, ketones, and organic acids. Such compositions wherein the compositions have been subjected to liquid-liquid extraction processes.
摘要翻译： 所述组合物包含：选自烷基磷酸酯表面活性剂，烷基磷酸乙氧基化表面活性剂，甜菜碱表面活性剂，甜菜碱乙氧基化表面活性剂，氧化胺表面活性剂及其混合物和水的表面活性剂组合物，所述表面活性剂组合物含有水溶性表面活性剂， ; 其中所述组合物还包含：小于约4重量％的所述水溶性表面活性剂;总不需要的非极性材料; 小于2.5重量％的水溶性表面活性剂，碳链长度大于4的醇; 小于约1重量％的水溶性表面活性剂的胺和酰胺材料; 和小于约1重量％的水溶性表面活性剂，选自醛，酯，酮和有机酸的不期望的非极性材料。 这种组合物，其中组合物已经经过液 - 液萃取方法。
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公开(公告)号：US08697036B2
公开(公告)日：2014-04-15
申请号：US13564823
申请日：2012-08-02
CPC分类号： A61K8/55 , A61K8/37 , A61K2800/805 , A61Q11/00 , B01D11/0492
摘要： Processes for improving the taste of water-soluble surfactants using liquid-liquid solvent extraction, said process comprising the steps of: providing a water-soluble surfactant composition in need of treatment wherein said water-soluble surfactant composition comprises a water-soluble surfactant and one or more undesirable non-polar materials; contacting said water-soluble surfactant composition with an extraction solvent and water to form an extraction mixture comprising an aqueous phase and a solvent phase; and separating the aqueous phase from the solvent phase; wherein the extraction solvent is selected from solvents having individual Hansen solubility parameters of a dispersion force component (δD) ranging from about 15 to about 17 (MPa)0.5, a polar component (δP) ranging from 0 to about 9 (MPa)0.5 and a hydrogen bonding component (δH) ranging from 0 to about 11 (MPa)0.5. Treated water-soluble surfactant compositions produced by such processes and oral care compositions containing such treated water-soluble surfactant compositions.
摘要翻译： 使用液 - 液溶剂萃取来改善水溶性表面活性剂的味道的方法，所述方法包括以下步骤：提供需要处理的水溶性表面活性剂组合物，其中所述水溶性表面活性剂组合物包含水溶性表面活性剂和一种 或更不希望的非极性材料; 使所述水溶性表面活性剂组合物与提取溶剂和水接触以形成包含水相和溶剂相的萃取混合物; 并将水相与溶剂相分离; 其中提取溶剂选自具有范围为约15至约17（MPa）0.5，极性组分（δP）为0至约9（MPa）0.5的分散力组分（δD）的单独Hansen溶解度参数的溶剂和0至约9（MPa） 0〜11（MPa）的氢键成分（δH）为0.5。 通过这些方法制备的经处理的水溶性表面活性剂组合物和含有这种经处理的水溶性表面活性剂组合物的口腔护理组合物。
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公开(公告)号：US20130034506A1
公开(公告)日：2013-02-07
申请号：US13564853
申请日：2012-08-02
摘要： Treated surfactant composition containing a water-soluble surfactant and exhibiting improved taste, said composition comprising: a water-soluble surfactant selected from alkyl phosphate surfactants, alkyl phosphate ethoxylated surfactants, betaine surfactants, betaine ethoxylated surfactants, amine oxide surfactants, and mixtures thereof and water; wherein the composition further comprises: less than about 4%, by weight of the water-soluble surfactant, of total undesirable non-polar materials; less than about 2.5%, by weight of the water-soluble surfactant, of alcohols having a carbon chain length of greater than 4; less than about 1%, by weight of the water-soluble surfactant, of amine and amide materials; and less than about 1%, by weight of the water-soluble surfactant, undesirable non-polar materials selected from aldehydes, esters, ketones, and organic acids. Such compositions wherein the compositions have been subjected to liquid-liquid extraction processes.
摘要翻译： 所述组合物包含：选自烷基磷酸酯表面活性剂，烷基磷酸乙氧基化表面活性剂，甜菜碱表面活性剂，甜菜碱乙氧基化表面活性剂，氧化胺表面活性剂及其混合物和水的表面活性剂组合物，所述表面活性剂组合物含有水溶性表面活性剂， ; 其中所述组合物还包含：小于约4重量％的所述水溶性表面活性剂;总不需要的非极性材料; 小于2.5重量％的水溶性表面活性剂，碳链长度大于4的醇; 小于约1重量％的水溶性表面活性剂的胺和酰胺材料; 和小于约1重量％的水溶性表面活性剂，选自醛，酯，酮和有机酸的不期望的非极性材料。 这种组合物，其中组合物已经经过液 - 液萃取方法。
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公开(公告)号：US10413844B2
公开(公告)日：2019-09-17
申请号：US13564841
申请日：2012-08-02
摘要： Compositions useful in liquid-liquid extraction processes for improving the taste of water-soluble surfactants, said composition comprising: from about 5% to about 60%, by weight of the composition, of water soluble surfactant; from about 10% to about 90%, by weight of the composition, of water; from about 10% to about 90%, by weight of the composition, of extraction solvent; at least 0.01%, by weight of the composition, of undesirable non-polar materials; wherein the extraction solvent is selected from solvents having individual Hansen solubility parameters of a dispersion force component (δD) ranging from about 15 to about 17 (MPa)0.5, a polar component (δP) ranging from 0 to about 9 (MPa)0.5 and a hydrogen bonding component (δH) ranging from 0 to about 11 (MPa)0.5.
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公开(公告)号：US20130034508A1
公开(公告)日：2013-02-07
申请号：US13564823
申请日：2012-08-02
CPC分类号： A61K8/55 , A61K8/37 , A61K2800/805 , A61Q11/00 , B01D11/0492
摘要： Processes for improving the taste of water-soluble surfactants using liquid-liquid solvent extraction, said process comprising the steps of: providing a water-soluble surfactant composition in need of treatment wherein said water-soluble surfactant composition comprises a water-soluble surfactant and one or more undesirable non-polar materials; contacting said water-soluble surfactant composition with an extraction solvent and water to form an extraction mixture comprising an aqueous phase and a solvent phase; and separating the aqueous phase from the solvent phase; wherein the extraction solvent is selected from solvents having individual Hansen solubility parameters of a dispersion force component (δD) ranging from about 15 to about 17 (MPa)0.5, a polar component (δP) ranging from 0 to about 9 (MPa)0.5 and a hydrogen bonding component (δH) ranging from 0 to about 11 (MPa)0.5. Treated water-soluble surfactant compositions produced by such processes and oral care compositions containing such treated water-soluble surfactant compositions.
摘要翻译： 使用液 - 液溶剂萃取来改善水溶性表面活性剂的味道的方法，所述方法包括以下步骤：提供需要处理的水溶性表面活性剂组合物，其中所述水溶性表面活性剂组合物包含水溶性表面活性剂和一种 或更不希望的非极性材料; 使所述水溶性表面活性剂组合物与提取溶剂和水接触以形成包含水相和溶剂相的萃取混合物; 并将水相与溶剂相分离; 其中所述提取溶剂选自具有约15至约17（MPa）0.5范围内的分散力分量（δD）和0至约9（MPa）0.5范围内的极性组分（δP）的各个Hansen溶解度参数的溶剂和 0〜11（MPa）的氢键成分（δH）为0.5。 通过这些方法制备的经处理的水溶性表面活性剂组合物和含有这种经处理的水溶性表面活性剂组合物的口腔护理组合物。
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