Method for producing acyloxy benzoic acids
    1.
    发明授权
    Method for producing acyloxy benzoic acids 有权
    酰氧基苯甲酸的制备方法

    公开(公告)号:US08907118B2

    公开(公告)日:2014-12-09

    申请号:US13816686

    申请日:2011-08-06

    IPC分类号: C07C67/14

    摘要: The invention relates to a method for producing acyloxy benzoic acids of the formula (I), in which R1 is a linear or branched saturated alkyl group with 6 to 30 carbon atoms, a linear or branched mono- or polyunsaturated alkenyl group with 6 to 30 carbon atoms, or an aryl group with 6 to 30 carbon atoms. The acyloxy benzoic acids of the formula (I) are produced from para-hydroxy benzoic acid and a corresponding carboxylic acid halide in the presence of an alkali hydroxide.

    摘要翻译: 本发明涉及一种制备式(I)的酰氧基苯甲酸的方法,其中R 1为具有6至30个碳原子的直链或支链饱和烷基,具有6至30个直链或支链单或多不饱和链烯基 碳原子或具有6至30个碳原子的芳基。 式(I)的酰氧基苯甲酸由对羟基苯甲酸和相应的羧酸卤化物在碱金属氢氧化物存在下制备。

    Method for producing acyloxy benzoic acids
    2.
    发明授权
    Method for producing acyloxy benzoic acids 有权
    酰氧基苯甲酸的制备方法

    公开(公告)号:US08901342B2

    公开(公告)日:2014-12-02

    申请号:US13816650

    申请日:2011-08-06

    IPC分类号: C07C67/14 C11D3/39

    摘要: The invention relates to a method for producing acyloxy benzoic acids of the formula (I), in which R1 is a linear or branched saturated alkyl group with 6 to 30 carbon atoms, a linear or branched mono- or polyunsaturated alkenyl group with 6 to 30 carbon atoms, or an aryl group with 6 to 30 carbon atoms. The acyloxy benzoic acids of the formula (I) are produced from para-hydroxy benzoic acid and a corresponding carboxylic acid halogenide in the presence of a base and are advantageously suitable for use as activators for hydrogen peroxide.

    摘要翻译: 本发明涉及一种制备式(I)的酰氧基苯甲酸的方法,其中R 1为具有6至30个碳原子的直链或支链饱和烷基,具有6至30个直链或支链单或多不饱和链烯基 碳原子或具有6至30个碳原子的芳基。 式(I)的酰氧基苯甲酸由对羟基苯甲酸和相应的羧酸卤化物在碱的存在下制备,并且有利地适合用作过氧化氢的活化剂。

    Method For Producing Acyloxy Benzoic Acids
    3.
    发明申请
    Method For Producing Acyloxy Benzoic Acids 有权
    生产甲氧基苯甲酸的方法

    公开(公告)号:US20130217911A1

    公开(公告)日:2013-08-22

    申请号:US13816686

    申请日:2011-08-06

    IPC分类号: C07C67/14

    摘要: The invention relates to a method for producing acyloxy benzoic acids of the formula (I), in which R1 is a linear or branched saturated alkyl group with 6 to 30 carbon atoms, a linear or branched mono- or polyunsaturated alkenyl group with 6 to 30 carbon atoms, or an aryl group with 6 to 30 carbon atoms. The acyloxy benzoic acids of the formula (I) are produced from para-hydroxy benzoic acid and a corresponding carboxylic acid halide in the presence of an alkali hydroxide.

    摘要翻译: 本发明涉及一种制备式(I)的酰氧基苯甲酸的方法,其中R 1为具有6至30个碳原子的直链或支链饱和烷基,具有6至30个直链或支链单或多不饱和链烯基 碳原子或具有6至30个碳原子的芳基。 式(I)的酰氧基苯甲酸由对羟基苯甲酸和相应的羧酸卤化物在碱金属氢氧化物存在下制备。

    Method For Producing Acyloxy Benzoic Acids
    4.
    发明申请
    Method For Producing Acyloxy Benzoic Acids 有权
    生产甲氧基苯甲酸的方法

    公开(公告)号:US20130211131A1

    公开(公告)日:2013-08-15

    申请号:US13816650

    申请日:2011-08-06

    IPC分类号: C07C67/14

    摘要: The invention relates to a method for producing acyloxy benzoic acids of the formula (I), in which R1 is a linear or branched saturated alkyl group with 6 to 30 carbon atoms, a linear or branched mono- or polyunsaturated alkenyl group with 6 to 30 carbon atoms, or an aryl group with 6 to 30 carbon atoms. The acyloxy benzoic acids of the formula (I) are produced from para-hydroxy benzoic acid and a corresponding carboxylic acid halogenide in the presence of a base and are advantageously suitable for use as activators for hydrogen peroxide.

    摘要翻译: 本发明涉及一种制备式(I)的酰氧基苯甲酸的方法,其中R 1为具有6至30个碳原子的直链或支链饱和烷基,具有6至30个直链或支链单或多不饱和链烯基 碳原子或具有6至30个碳原子的芳基。 式(I)的酰氧基苯甲酸由对羟基苯甲酸和相应的羧酸卤化物在碱的存在下制备,并且有利地适合用作过氧化氢的活化剂。

    Method for producing 3,7-diaza-bicyclo[3.3.1]nonane compounds
    5.
    发明授权
    Method for producing 3,7-diaza-bicyclo[3.3.1]nonane compounds 有权
    制备3,7-二氮杂双环[3.3.1]壬烷化合物的方法

    公开(公告)号:US08293910B2

    公开(公告)日:2012-10-23

    申请号:US13059470

    申请日:2009-08-17

    IPC分类号: C07D471/08

    CPC分类号: C07D471/08

    摘要: The invention relates to a one-pot reaction for the production of 3,7-diaza-bicyclo[3.3.1]nonane compounds, wherein in a first step a dicarboxylic acid ester is reacted with a pyridine aldehyde and a primary amine. The piperidone created in this manner is reacted with formaldehyde and a further primary amine in a second step. It is essential to the invention that both reaction steps are carried out in a one-pot variation in a C1-C4 alcohol as the solvent, and that the reaction water created is removed by means of distillation.

    摘要翻译: 本发明涉及一种用于制备3,7-二氮杂双环[3.3.1]壬烷化合物的一锅反应,其中在第一步中,二羧酸酯与吡啶醛和伯胺反应。 在第二步骤中以这种方式产生的哌啶酮与甲醛和另外的伯胺反应。 本发明重要的是,两个反应步骤都是以C1-C4醇作为溶剂的一锅变化进行的,所产生的反应水通过蒸馏除去。

    Method for producing 3,7-diaza-bicyclo[3.3.1]nonane metal complexes
    6.
    发明授权
    Method for producing 3,7-diaza-bicyclo[3.3.1]nonane metal complexes 有权
    制备3,7-二氮杂双环[3.3.1]壬烷金属络合物的方法

    公开(公告)号:US08536334B2

    公开(公告)日:2013-09-17

    申请号:US13140589

    申请日:2009-12-12

    IPC分类号: C07F15/02 C07F15/00

    CPC分类号: C07F15/025

    摘要: The invention relates to a method for producing 3,7-diaza-bicyclo[3.3.1]nonane metal complexes, wherein the ligand, a 3,7-diaza-bicyclo[3.3.1]nonane compound, is reacted with an aqueous metal(II)salt solution in one step. According to the invention, the reaction stage is carried out with water as solvent.

    摘要翻译: 本发明涉及制备3,7-二氮杂双环[3.3.1]壬烷金属络合物的方法,其中配体,3,7-二氮杂 - 双环[3.3.1]壬烷化合物与含水金属 (II)盐溶液。 根据本发明,反应阶段用水作为溶剂进行。

    Method For Producing 3,7-Diaza-Bicyclo[3.3.1]Nonane Metal Complexes
    7.
    发明申请
    Method For Producing 3,7-Diaza-Bicyclo[3.3.1]Nonane Metal Complexes 有权
    制备3,7-二氮杂双环[3.3.1]壬烷金属络合物的方法

    公开(公告)号:US20110263857A1

    公开(公告)日:2011-10-27

    申请号:US13140589

    申请日:2009-12-12

    IPC分类号: C07F15/02

    CPC分类号: C07F15/025

    摘要: The invention relates to a method for producing 3,7-diaza-bicyclo[3.3.1]nonane metal complexes, wherein the ligand, a 3,7-diaza-bicyclo[3.3.1] nonane compound, is reacted with an aqueous metal(II)salt solution in one step. According to the invention, the reaction stage is carried out with water as solvent.

    摘要翻译: 本发明涉及制备3,7-二氮杂双环[3.3.1]壬烷金属络合物的方法,其中配体,3,7-二氮杂 - 双环[3.3.1]壬烷化合物与含水金属 (II)盐溶液。 根据本发明,反应阶段用水作为溶剂进行。

    Method For Producing 3,7-Diaza-Bicyclo[3.3.1] Nonane Compounds
    8.
    发明申请
    Method For Producing 3,7-Diaza-Bicyclo[3.3.1] Nonane Compounds 有权
    制备3,7-二氮杂双环[3.3.1]壬烷化合物的方法

    公开(公告)号:US20110152528A1

    公开(公告)日:2011-06-23

    申请号:US13059470

    申请日:2009-08-17

    IPC分类号: C07D471/08

    CPC分类号: C07D471/08

    摘要: The invention relates to a one-pot reaction for the production of 3,7-diaza-bicyclo[3.3.1]nonane compounds, wherein in a first step a dicarboxylic acid ester is reacted with a pyridine aldehyde and a primary amine. The piperidone created in this manner is reacted with formaldehyde and a further primary amine in a second step. It is essential to the invention that both reaction steps are carried out in a one-pot variation in a C1-C4 alcohol as the solvent, and that the reaction water created is removed by means of distillation.

    摘要翻译: 本发明涉及一种用于制备3,7-二氮杂双环[3.3.1]壬烷化合物的一锅反应,其中在第一步中,二羧酸酯与吡啶醛和伯胺反应。 在第二步骤中以这种方式产生的哌啶酮与甲醛和另外的伯胺反应。 本发明重要的是,两个反应步骤都是以C1-C4醇作为溶剂的一锅变化进行的,所产生的反应水通过蒸馏除去。