摘要:
What is proposed is an apparatus for separating liquid droplets out of a feed gas stream comprising them comprising a delay vessel (1) for preliminary separation of some of the liquid droplets out of the feed gas stream under the action of gravity, with an inlet line (2) for the feed gas stream into the delay vessel (1) and an outlet line (3) for the gas stream which has been depleted of liquid droplets and flows out of the delay vessel (1), and tangential supply thereof into a centrifugal droplet separator (4), the outlet line (3) being arranged in the upper region of the delay vessel (1) and being spaced apart from the inlet line (2) to such an extent that the delay time of the gas stream in the delay vessel (1) is at a maximum, and with an outlet line (5) for the liquid separated in the delay vessel (1) at the base thereof,and wherein the centrifugal droplet separator (4) used is an axially symmetric apparatus with a vertical longitudinal axis and circular cross section, with a jacket and hoods at the upper and lower ends of the jacket, and wherein an outlet stub (6) for the liquid separated in the centrifugal droplet separator (4) is arranged in the region of the lower hood of the centrifugal droplet separator (4) and has such dimensions that it is immersed into the liquid standing at the base of the delay vessel (1) or into a liquid standing in a cup in the interior of the delay vessel (1), and with a gas outlet stub (7) at the upper end of the centrifugal droplet separator (4) for the gas stream purified further in the centrifugal droplet separator (4), and wherein both the supply of the gas stream depleted of liquid droplets from the delay vessel (1) via the outlet line (3) and the removal of the liquid separated in the centrifugal droplet separator (4) via line (6) into the delay vessel (1) are effected without the use of pumps and shutoff devices.
摘要:
An apparatus, for separating liquid droplets out of a feed gas stream, includes a delay vessel for preliminary separation of some of the liquid droplets out of the feed gas stream under gravity, with an inlet line for the feed gas stream and an outlet line for the gas stream which has been depleted of liquid droplets and which flows out of the delay vessel and a tangential supply thereof into a centrifugal droplet separator. The outlet line is arranged in the upper region of the delay vessel and spaced apart from the inlet line to such an extent that the delay time of the gas stream in the delay vessel is at a maximum, and with an outlet line for the liquid separated in the delay vessel at the base thereof.
摘要:
What is proposed is a centrifugal droplet separator for separating liquid droplets out of a feed gas stream comprising them, with a vertical longitudinal axis and circular cross section, with a jacket (1) and with hoods (2) at the upper and lower ends of the jacket (1), with tangential supply (3) of the feed gas stream comprising liquid droplets at the jacket (1) and with an outlet stub (4) for the liquid separated out in the centrifugal droplet separator in the region of the lower hood (2), and with a gas outlet stub (7) for the gas stream cleaned in the centrifugal droplet separator in the region of the upper hood (2), wherein two, three or more inlet orifices (9) arranged symmetrically on the circumference of the upper hood (2) for tangential supply of cleaning liquid are provided in the same direction as the supply of the feed gas stream comprising liquid droplets.
摘要:
A process for preparing chlorine by gas-phase oxidation of hydrogen chloride over a heterogeneous, particulate catalyst in a fluidized-bed reactor to give a product gas mixture which is freed of entrained catalyst particles in cyclones (1) which are arranged in the upper region of the fluidized-bed reactor, which comprises a cylindrical upper part (2) which has a tangential or spiral-shaped inlet (3) for the product gas mixture and tapers at its lower end via a conical section (4) into a cyclone downcomer tube (5) and also a central downward-extending tube (6) in the upper region of the cyclone (1) for discharging the product gas mixture which has been freed of entrained catalyst particles, whereinfrom one to seven cascades of in each case from two to five cyclones (1) connected in series are used, with the cyclones (1) of each cascade, with the exception of the first cyclone (1) through which flow occurs in each case, which is designed so that about 90 to 99% by weight of the entrained catalyst particles are precipitated, each having a trickle valve (7) comprising an angled tube end piece (8) and also a loose flap (9) suspended at an angle α to the vertical at the lower end of the cyclone downcomer tube (5), where the angle α and the weight of the flap (9) are designed so that the torque of the flap (9) divided by the diameter of the outlet opening from the angled tube end piece (8) is in the range from 2 to 300 N/m2, is proposed.