公开(公告)号：US08764886B2

公开(公告)日：2014-07-01

申请号：US13515180

申请日：2010-12-13

申请人： Joerg Halpap ,  Andreas Bode ,  Eberhard Herrmann ,  Markus Linsenbuehler ,  Bernd Sachweh ,  Michael Pilz ,  Michael Mertler ,  Matthias Wilhelm Meier

发明人： Joerg Halpap ,  Andreas Bode ,  Eberhard Herrmann ,  Markus Linsenbuehler ,  Bernd Sachweh ,  Michael Pilz ,  Michael Mertler ,  Matthias Wilhelm Meier

IPC分类号： B01D45/12

CPC分类号： B01D45/12 ,  B04C5/04 ,  B04C5/13 ,  B04C5/181 ,  B04C9/00

摘要： An apparatus, for separating liquid droplets out of a feed gas stream, includes a delay vessel for preliminary separation of some of the liquid droplets out of the feed gas stream under gravity, with an inlet line for the feed gas stream and an outlet line for the gas stream which has been depleted of liquid droplets and which flows out of the delay vessel and a tangential supply thereof into a centrifugal droplet separator. The outlet line is arranged in the upper region of the delay vessel and spaced apart from the inlet line to such an extent that the delay time of the gas stream in the delay vessel is at a maximum, and with an outlet line for the liquid separated in the delay vessel at the base thereof.

摘要翻译： 用于从进料气流中分离液滴的装置包括延迟容器，用于在重力作用下将一些液滴从进料气流中预先分离出来，其中进料气流的入口管线和用于 已经耗尽液滴并且从延迟容器流出并且切向供应的气流进入离心液滴分离器。 出口管线布置在延迟容器的上部区域中并与入口管线间隔开，使得延迟容器中的气体流的延迟时间处于最大值，并且用于液体分离的出口管线 在其基部的延迟容器中。

公开(公告)号：US20080014128A1

公开(公告)日：2008-01-17

申请号：US11667417

申请日：2005-11-08

申请人： Eberhard Herrmann ,  Manfred Hecker ,  Rainer Karer ,  Klaus Berhalter ,  Paulus de Lange ,  Jorg Halpap ,  Cyrus Ahmadzade-Youssefi

发明人： Eberhard Herrmann ,  Manfred Hecker ,  Rainer Karer ,  Klaus Berhalter ,  Paulus de Lange ,  Jorg Halpap ,  Cyrus Ahmadzade-Youssefi

IPC分类号： C08F10/00 ,  B01J19/18

CPC分类号： B01J8/003 ,  B01J8/006 ,  B01J8/1872 ,  B01J2208/00256 ,  B01J2208/00274 ,  B01J2208/00761 ,  C08F10/00 ,  C08F110/02 ,  C08F2/34

摘要： Apparatus for the polymerization of olefins, in particular ethylene, comprising a gas-phase fluidized-bed reactor (1), a product offtake line (15) for taking polymer particles either continuously or discontinuously from the reactor (1), which line (15) is connected to a depressurization vessel (2) for separating polymer particles and gas, a recycle gas filter (3) for freeing the gas of entrained fine particles connected to the depressurization vessel (2), a compressor which compresses the gas which has been freed of fine particles and recirculates it into the reactor (1), with the recycle gas filter (3) having an inlet chamber (4) provided with a gas inlet (6), an outlet chamber (5) provided with a gas outlet (7), an essentially vertical sheet-like filter medium (9) for retaining the fine particles which separates the inlet chamber (4) from the outlet chamber (5) and a particle outlet (8). The inlet chamber (4) has a dividing wall (10) which is arranged essentially parallel to the filter medium (9) and separates the inlet chamber (4) into an inflow region (4a), which is connected to the gas inlet (6), and a filter region (4b) in which the filter medium is located and has an upper opening and a lower opening which are dimensioned so that from 60 to 90% of the volume flow flows through the upper opening so that flow along the filter medium (9) from the top downward results.

摘要翻译： 用于烯烃聚合的设备，特别是乙烯，包括气相流化床反应器（1），用于从反应器（1）连续或不连续地获取聚合物颗粒的出口管线（15），该管线（15） ）连接到用于分离聚合物颗粒和气体的减压容器（2），用于释放连接到减压容器（2）的夹带的细颗粒的气体的循环气体过滤器（3），压缩已经被 释放细颗粒并将其再循环到反应器（1）中，循环气体过滤器（3）具有设置有气体入口（6）的入口室（4），设置有气体出口的出口室（5） 7），用于保持将入口室（4）与出口室（5）分离的细颗粒和颗粒出口（8）的基本垂直的片状过滤介质（9）。 入口室（4）具有基本上与过滤介质（9）平行布置的分隔壁（10），并将入口室（4）分离成入口区域（4a），该入口区域连接到气体入口 6）和过滤器区域（4b），其中过滤介质位于并具有上开口和下开口，其尺寸使得体积流量的60％至90％流过上开口，使得沿着 过滤介质（9）从顶部向下的结果。

公开(公告)号：US20070264171A1

公开(公告)日：2007-11-15

申请号：US11667349

申请日：2005-11-09

申请人： Eberhard Herrmann ,  Axel Sperber ,  Manfred Hecker ,  Rainer Karer ,  Klaus Berhalter ,  Paulus de Lange ,  Jorg Halpap ,  Cyrus Ahmadzade-Youssefi

发明人： Eberhard Herrmann ,  Axel Sperber ,  Manfred Hecker ,  Rainer Karer ,  Klaus Berhalter ,  Paulus de Lange ,  Jorg Halpap ,  Cyrus Ahmadzade-Youssefi

IPC分类号： C08F2/34

CPC分类号： B01J8/1872 ,  B01J8/0055 ,  B01J8/24 ,  B01J2208/00256 ,  B01J2208/00274 ,  B04C5/081 ,  C08F6/02 ,  C08F10/00 ,  C08F10/02 ,  C08F110/02 ,  C08L23/04 ,  C08F2/34

摘要： An apparatus for the polymerization of olefins, in particular ethylene, comprising a gas-phase fluidized-bed reactor (1), a recycle gas line (2) connected to the reactor for discharging and recirculating the recycle gas stream comprising the unpolymerized olefin and a cyclone (3) located in the recycle gas line for the reduction and precipitation of the solid particles entrained in the recycle gas from the reactor, with the cyclone comprising an upper section (3a) which has an essentially vertical central axis, whose wall extends along a rotationally symmetric body and which is provided with a cyclone inlet (4) arranged eccentrically relative to the central axis, a middle section (3b) which adjoins the upper section (3a) and whose wall extends along a rotationally symmetric body which tapers in a downward direction, a lower section (3c) for discharging the solid particles precipitated from the recycle gas which adjoins the middle section (3b) and whose wall extends along a rotationally symmetric body and a tube (5) extending essentially axially symmetrically down into the upper section and, if appropriate, the middle section for discharging the recycle gas which has been freed of the particles. According to the invention the ratio Hi of the distance hi from the lower end of the tube (5) extending downward into the cyclone to the intersection (6) of an imaginary extension of the wall of the downward-extending tube (5) with the wall of the middle section (3b) to the diameter di of the downward-extending tube (5) is from 3 to 8, in particular from 4 to 7.

摘要翻译： 用于烯烃聚合的装置，特别是乙烯，包括气相流化床反应器（1），连接到反应器的再循环气体管线（2），用于排出和再循环包含未聚合烯烃的循环气流和 旋流器（3），其位于循环气体管线中，用于还原和沉淀夹带在来自反应器的再循环气体中的固体颗粒，旋风分离器包括具有基本上垂直的中心轴线的上部分（3a），其上壁延伸 沿着旋转对称体并且设置有相对于中心轴线偏心布置的旋风入口（4），邻近上部（3a）并且其壁沿旋转对称体延伸的中间部分（3b） 用于排出邻近中间部分（3b）并且其壁延伸的再循环气体沉淀的固体颗粒的下部分（3c） 旋转对称体和基本上轴向对称地延伸到上部的管（5）以及适当的中间部分用于排出已经没有颗粒的循环气体。 根据本发明，与从下游进入旋风分离器的管（5）的下端距离h i i的距离h i i的比例H i 向下延伸的管（5）的壁与中间部分（3b）的壁与向下延伸的管（5）的直径d iI i的假想延伸为3至 8，特别是4到7。

公开(公告)号：US20120285322A1

公开(公告)日：2012-11-15

申请号：US13515180

申请日：2010-12-13

申请人： Joerg Halpap ,  Andreas Bode ,  Eberhard Herrmann ,  Markus Linsenbuehler ,  Bernd Sachweh ,  Michael Pilz ,  Michael Mertler ,  Matthias Wilhelm Meier

发明人： Joerg Halpap ,  Andreas Bode ,  Eberhard Herrmann ,  Markus Linsenbuehler ,  Bernd Sachweh ,  Michael Pilz ,  Michael Mertler ,  Matthias Wilhelm Meier

IPC分类号： B01D45/16

CPC分类号： B01D45/12 ,  B04C5/04 ,  B04C5/13 ,  B04C5/181 ,  B04C9/00

摘要： What is proposed is an apparatus for separating liquid droplets out of a feed gas stream comprising them comprising a delay vessel (1) for preliminary separation of some of the liquid droplets out of the feed gas stream under the action of gravity, with an inlet line (2) for the feed gas stream into the delay vessel (1) and an outlet line (3) for the gas stream which has been depleted of liquid droplets and flows out of the delay vessel (1), and tangential supply thereof into a centrifugal droplet separator (4), the outlet line (3) being arranged in the upper region of the delay vessel (1) and being spaced apart from the inlet line (2) to such an extent that the delay time of the gas stream in the delay vessel (1) is at a maximum, and with an outlet line (5) for the liquid separated in the delay vessel (1) at the base thereof,and wherein the centrifugal droplet separator (4) used is an axially symmetric apparatus with a vertical longitudinal axis and circular cross section, with a jacket and hoods at the upper and lower ends of the jacket, and wherein an outlet stub (6) for the liquid separated in the centrifugal droplet separator (4) is arranged in the region of the lower hood of the centrifugal droplet separator (4) and has such dimensions that it is immersed into the liquid standing at the base of the delay vessel (1) or into a liquid standing in a cup in the interior of the delay vessel (1), and with a gas outlet stub (7) at the upper end of the centrifugal droplet separator (4) for the gas stream purified further in the centrifugal droplet separator (4), and wherein both the supply of the gas stream depleted of liquid droplets from the delay vessel (1) via the outlet line (3) and the removal of the liquid separated in the centrifugal droplet separator (4) via line (6) into the delay vessel (1) are effected without the use of pumps and shutoff devices.

公开(公告)号：US07781544B2

公开(公告)日：2010-08-24

申请号：US11667349

申请日：2005-11-09

申请人： Eberhard Herrmann ,  Axel Sperber ,  Manfred Hecker ,  Rainer Karer ,  Klaus Berhalter ,  Paulus De Lange ,  Jörg Halpap ,  Cyrus Ahmadzade-Youssefi

发明人： Eberhard Herrmann ,  Axel Sperber ,  Manfred Hecker ,  Rainer Karer ,  Klaus Berhalter ,  Paulus De Lange ,  Jörg Halpap ,  Cyrus Ahmadzade-Youssefi

IPC分类号： C08F2/00 ,  F27B15/08

CPC分类号： B01J8/1872 ,  B01J8/0055 ,  B01J8/24 ,  B01J2208/00256 ,  B01J2208/00274 ,  B04C5/081 ,  C08F6/02 ,  C08F10/00 ,  C08F10/02 ,  C08F110/02 ,  C08L23/04 ,  C08F2/34

摘要： An apparatus for the polymerization of olefins, in particular ethylene, comprising a gas-phase fluidized-bed reactor (1), a recycle gas line (2) connected to the reactor for discharging and recirculating the recycle gas stream comprising the unpolymerized olefin and a cyclone (3) located in the recycle gas line for the reduction and precipitation of the solid particles entrained in the recycle gas from the reactor, with the cyclone comprising an upper section (3a) which has an essentially vertical central axis, whose wall extends along a rotationally symmetric body and which is provided with a cyclone inlet (4) arranged eccentrically relative to the central axis, a middle section (3b) which adjoins the upper section (3a) and whose wall extends along a rotationally symmetric body which tapers in a downward direction, a lower section (3c) for discharging the solid particles precipitated from the recycle gas which adjoins the middle section (3b) and whose wall extends along a rotationally symmetric body and a tube (5) extending essentially axially symmetrically down into the upper section and, if appropriate, the middle section for discharging the recycle gas which has been freed of the particles. According to the invention the ratio Hi of the distance hi from the lower end of the tube (5) extending downward into the cyclone to the intersection (6) of an imaginary extension of the wall of the downward-extending tube (5) with the wall of the middle section (3b) to the diameter di of the downward-extending tube (5) is from 3 to 8, in particular from 4 to 7.

摘要翻译： 用于烯烃聚合的装置，特别是乙烯，包括气相流化床反应器（1），连接到反应器的再循环气体管线（2），用于排出和再循环包含未聚合烯烃的循环气流和 旋风分离器（3）位于循环气体管线中，用于还原和沉淀夹带在来自反应器的再循环气体中的固体颗粒，其中旋风分离器包括具有基本垂直的中心轴线的上部分（3a），其上壁沿着 旋转对称体，并且设置有相对于中心轴偏心布置的旋风入口（4），邻接上部（3a）的中间部分（3b），并且其壁沿着旋转对称的体 用于排出邻近中间部分（3b）的循环气体沉淀的固体颗粒的下部（3c），并且其壁沿旋转方向延伸 对称体和管（5），其基本上轴向对称地延伸到上部，并且如果适当的话，中间部分用于排出已经没有颗粒的循环气体。 根据本发明，从管（5）的下端向下延伸到旋风分离器中的距离hi的距离hi与向下延伸的管（5）的壁的假想延伸部的交点（6） 中间部分（3b）的壁向下延伸管（5）的直径di为3至8，特别是4至7。

公开(公告)号：US07776278B2

公开(公告)日：2010-08-17

申请号：US11667417

申请日：2005-11-08

申请人： Eberhard Herrmann ,  Manfred Hecker ,  Rainer Karer ,  Klaus Berhalter ,  Paulus De Lange ,  Jörg Halpap ,  Cyrus Ahmadzade-Youssefi

发明人： Eberhard Herrmann ,  Manfred Hecker ,  Rainer Karer ,  Klaus Berhalter ,  Paulus De Lange ,  Jörg Halpap ,  Cyrus Ahmadzade-Youssefi

IPC分类号： B01J19/00

CPC分类号： B01J8/003 ,  B01J8/006 ,  B01J8/1872 ,  B01J2208/00256 ,  B01J2208/00274 ,  B01J2208/00761 ,  C08F10/00 ,  C08F110/02 ,  C08F2/34

摘要： Apparatus for the polymerization of olefins, in particular ethylene, comprising a gas-phase fluidized-bed reactor (1), a product offtake line (15) for taking polymer particles either continuously or discontinuously from the reactor (1), which line (15) is connected to a depressurization vessel (2) for separating polymer particles and gas, a recycle gas filter (3) for freeing the gas of entrained fine particles connected to the depressurization vessel (2), a compressor which compresses the gas which has been freed of fine particles and recirculates it into the reactor (1), with the recycle gas filter (3) having an inlet chamber (4) provided with a gas inlet (6), an outlet chamber (5) provided with a gas outlet (7), an essentially vertical sheet-like filter medium (9) for retaining the fine particles which separates the inlet chamber (4) from the outlet chamber (5) and a particle outlet (8). The inlet chamber (4) has a dividing wall (10) which is arranged essentially parallel to the filter medium (9) and separates the inlet chamber (4) into an inflow region (4a), which is connected to the gas inlet (6), and a filter region (4b) in which the filter medium is located and has an upper opening and a lower opening which are dimensioned so that from 60 to 90% of the volume flow flows through the upper opening so that flow along the filter medium (9) from the top downward results.

摘要翻译： 用于烯烃聚合的设备，特别是乙烯，包括气相流化床反应器（1），用于从反应器（1）连续或不连续地获取聚合物颗粒的出口管线（15），该管线（15） ）连接到用于分离聚合物颗粒和气体的减压容器（2），用于释放连接到减压容器（2）的夹带的细颗粒的气体的循环气体过滤器（3），压缩已经被 释放细颗粒并将其再循环到反应器（1）中，循环气体过滤器（3）具有设置有气体入口（6）的入口室（4），设置有气体出口的出口室（5） 7），用于保持将入口室（4）与出口室（5）分离的细颗粒和颗粒出口（8）的基本垂直的片状过滤介质（9）。 入口室（4）具有基本上与过滤介质（9）平行布置的分隔壁（10），并将入口室（4）分离成入口区域（4a），该入口区域连接到气体入口 ）和过滤器区域（4b），其中所述过滤介质定位并具有上开口和下开口，所述上开口和下开口的尺寸使得所述体积流的60至90％流过所述上开口，使得沿着所述过滤器的流动 中等（9）从上方下降。