公开(公告)号：US5425786A

公开(公告)日：1995-06-20

申请号：US119880

申请日：1993-09-13

申请人： Rudolf Vanheertum ,  Richard Hendricx ,  Norbert Kriebitzsch ,  Francois van de Velde ,  Ruediger Schirrmacher

发明人： Rudolf Vanheertum ,  Richard Hendricx ,  Norbert Kriebitzsch ,  Francois van de Velde ,  Ruediger Schirrmacher

IPC分类号： C04B41/48 ,  C07D251/28 ,  B01J13/00

CPC分类号： C07D251/28 ,  C04B41/4861

摘要： A process is described for the production of a suspension of cyanuric chloride in an aqueous liquid, more particularly, water. Molten cyanuric chloride is sprayed using a spray arrangement comprising a spray nozzle immersed in the aqueous liquid. Blockages in the nozzle during the critical start and stop phases are avoided by passing superheated steam through those parts of the spray arrangement which come into contact with the cyanuric chloride melt before and after the spraying process. A particularly reactive cyanuric chloride suspension is obtained by spraying a mixture of cyanuric chloride melt and superheated steam.

摘要翻译： 描述了一种制备氰尿酰氯在水性液体，特别是水中的悬浮液的方法。 使用包含浸入水性液体中的喷雾喷嘴的喷雾装置喷涂熔融的氰尿酰氯。 通过将过热蒸汽通过喷雾装置的与喷雾过程之前和之后的氰尿酰氯熔体接触的那些部分来避免临界起始和停止阶段的喷嘴堵塞。 通过喷洒氰尿酰氯熔体和过热蒸汽的混合物获得特别反应的氰尿酰氯悬浮液。

公开(公告)号：US4351644A

公开(公告)日：1982-09-28

申请号：US248442

申请日：1981-03-27

申请人： Norbert Kriebitzsch ,  Kurt Puschner ,  Klaus Hentschel

发明人： Norbert Kriebitzsch ,  Kurt Puschner ,  Klaus Hentschel

IPC分类号： B01J8/00 ,  B01J19/00 ,  C07D251/28 ,  B01J8/08

CPC分类号： C07D251/28 ,  B01J8/002

摘要： Solid cyanuric chloride is supplied to the gas space of a cyanuric chloride melt with the help of a gas tight product stopper. Preferably there is used for this a screw conveyor in which the gas tight stopper is formed at the end of the screw conveyor; it is most favorable if the helix ends before the last section of the tube of the screw conveyor.

摘要翻译： 借助于气密产品塞，将固体氰尿酰氯供应到氰尿酰氯熔体的气体空间。 优选地，使用螺旋输送机，其中气密塞在螺旋输送机的端部形成; 如果螺旋输送机的管的最后部分之前螺旋结束，则是最有利的。

公开(公告)号：US4328010A

公开(公告)日：1982-05-04

申请号：US174180

申请日：1980-07-31

申请人： Friedrich Bittner ,  Werner Heimberger ,  Kurt Henkel ,  Norbert Kriebitzsch ,  Martin Petzold ,  Kurt Puschner

发明人： Friedrich Bittner ,  Werner Heimberger ,  Kurt Henkel ,  Norbert Kriebitzsch ,  Martin Petzold ,  Kurt Puschner

IPC分类号： B01D3/00 ,  B01D3/14 ,  B01D3/32 ,  B01D3/34 ,  C01C3/00 ,  B01D53/14

CPC分类号： C01C3/004 ,  B01D3/148 ,  B01D3/322 ,  B01D3/343

摘要： To obtain a cyanogen chloride which is practically free from water and preferably also free from hydrogen cyanide, hydrogen chloride and organic compounds, the crude cyanogen chloride is fractionally distilled. The return is led in countercurrent flow to the crude gas, thereby takes up the impurities and is further evaporated in the lower portion of the column, respectively in a special apparatus, by a liquid whose temperature is higher than the boiling temperature of cyanogen chloride. Thereby this liquid also takes up the impurities. The purification action is aided by a wash for the crude cyanogen chloride connected in series before it enters the fractionating column. It is very advantageous to combine the process with a plant for the production of cyanogen chloride.

摘要翻译： 为了获得实际上不含水的氰氯化物，优选也不含氰化氢，氯化氢和有机化合物，分馏了粗氯化氰。 回流以逆流流向粗气体，从而占据杂质，并在专用设备中通过温度高于氯化氰沸点的液体分别在塔的下部蒸发。 因此，这种液体也会占据杂质。 纯化作用通过在进入分馏塔之前串联连接的氯化氰原料的洗涤来辅助。 将该方法与用于生产氯化氰的设备相结合是非常有利的。