High-grade ethanol production system

    公开(公告)号:US12122738B2

    公开(公告)日:2024-10-22

    申请号:US18219470

    申请日:2023-07-07

    Abstract: The present disclosure provides high-grade ethanol production systems and methods that increase energy efficiency as compared to typical systems and methods by minimizing undesired acetal formation. The provided ethanol production method may include a low boilers removal distillation column and/or a stripper column constructed to simultaneously remove at least a portion of the acetaldehyde and at least a portion of the acetal from a feed stream in the presence of water. In some aspects, a low boilers removal process may be followed by a water removal process, which may be followed by a high boilers removal process. Acidity (e.g., carbon dioxide) may also be removed from a feed stream prior to or during the low boilers removal process. By minimizing acetal production, the provided method minimizes the amount of energy that is required to remove acetal when producing high-grade ethanol.

    METHOD AND DEVICE FOR THE PRODUCTION OF LACTIDE

    公开(公告)号:US20240140928A1

    公开(公告)日:2024-05-02

    申请号:US18547433

    申请日:2021-02-22

    Inventor: Jianjun SUI

    CPC classification number: C07D319/12 B01D3/009 B01D3/148 B01D5/006

    Abstract: This invention relates to a method for the continuous production of optically pure lactide comprising a first reactive distillation system, a second reactive distillation system, a main distillation system and the side-draw refluxer. For each of the four systems a novel horizontally top-mounted condenser is used in order to decrease its total pressure drop and thus reduce side-reactions associated with high bottom temperature. In addition, a wiped film evaporator, a short path evaporator or a combination thereof is utilized for the concentration of the purge stream from the second reactive distillation, in a purpose of removing the metal contaminants contained in the purge stream and depolymerizing the contained unconverted lactic acid oligomers to crude lactide, all of which give additional advantages for the lactide production.

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