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1.发明申请PROCESS FOR PRODUCING PENTAERYTHRITOL MERCAPTOCARBOXYLIC ACID ESTER, PENTAERYTHRITOL MERCAPTOCARBOXYLIC ACID ESTER OBTAINED BY THE SAME, AND USE THEREOF 审中-公开生产戊二酸三辛酯酸酯的方法，由其获得的戊二酸甘油酸酯酯及其用途公开(公告)号：US20110245531A1
公开(公告)日：2011-10-06
申请号：US13160988
申请日：2011-06-15
IPC分类号： C07C323/52
CPC分类号： C07C319/12 , C08G18/3876 , C08G18/7642 , G02B1/04 , C08L75/04 , C07C323/52
摘要： Pentaerythritol which contains none of the alkali metals and the alkaline earth metals or which contains at least one of these in a total amount of 1.0 weight % or smaller is reacted with a mercaptocarboxylic acid to produce a pentaerythritol mercaptocarboxylic acid ester.
摘要翻译： 不含有碱金属和碱土金属或其中至少一种的总量为1.0重量％以下的季戊四醇与巯基羧酸反应，生成季戊四醇巯基羧酸酯。
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2.发明申请PROCESS FOR PRODUCING PENTAERYTHRITOL MERCAPTOCARBOXYLIC ACID ESTER, PENTAERYTHRITOL MERCAPTOCARBOXYLIC ACID ESTER OBTAINED BY THE SAME, AND USE THEREOF 审中-公开生产戊二酸三辛酯酸酯的方法，由其获得的戊二酸甘油酯酸酯及其用途公开(公告)号：US20110065887A1
公开(公告)日：2011-03-17
申请号：US12845128
申请日：2010-07-28
CPC分类号： C07C319/12 , C08G18/3876 , C08G18/7642 , G02B1/04 , C08L75/04 , C07C323/52
摘要： A process for producing pentaerythritol mercaptocarboxylic ester by reacting pentaerythritol with a mercaptocarboxylic acid having a content of thioester formed by condensation of two molecules of the acid of 5% or below (in terms of area percentage) as determined by the high-performance liquid chromatography in the case of the total area of the mercaptocarboxylic acid and thioester formed by intermolecular condensation of the acid is taken as 100%.
摘要翻译： 通过使季戊四醇与巯基羧酸反应来制备季戊四醇巯基羧酸酯的方法，该季戊四醇与巯基羧酸反应，所述巯基羧酸通过两分子酸浓度为5％以下（以面积百分比计）缩合而形成，通过高效液相色谱法测定 通过酸的分子间缩合形成的巯基羧酸和硫酯的总面积的情况为100％。
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公开(公告)号：US5393400A
公开(公告)日：1995-02-28
申请号：US789489
申请日：1991-11-08
申请人： Shu Yamaguchi , Norihiko Fukatsu , Hideo Kimura
发明人： Shu Yamaguchi , Norihiko Fukatsu , Hideo Kimura
IPC分类号： G01N27/30 , G01N27/406 , G01N27/411 , G01N33/20
CPC分类号： G01N33/206
摘要： A metal melt is used as a measuring electrode while a pure form of a particular metal component to be measured or an alloy containing it is used as a standard electrode. The active substance to come in contact with the standard electrode includes at least one halide of an alkali halide and an alkaline earth halide, both having ion conductivity, and a halide of the particular metal component, any one of such halides consisting of a solid phase and a liquid phase. This active substance is provided such that it can come into contact with the metal melt and is used as an electrolyte as well. It is thus possible to provide a continuous detection of the concentration of the particular component in the molten metal to be measured.
摘要翻译： 将金属熔体用作测量电极，同时将待测量的特定金属组分的纯形式或含有它的合金用作标准电极。 与标准电极接触的活性物质包括至少一种具有离子传导性的碱金属卤化物和碱土金属卤化物的卤化物，以及特定金属组分的卤化物，任何一种由固相组成的卤化物 和液相。 该活性物质被设置为使其能够与金属熔体接触并且也用作电解质。 因此，可以提供对待测量的熔融金属中特定组分的浓度的连续检测。
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4.发明申请PROCESS FOR PRODUCING DICYANONORBORNANE AND ZEROVALENT NICKEL COMPLEX CATALYST 有权生产二氰基硼烷和零镍镍复合催化剂的方法公开(公告)号：US20090198082A1
公开(公告)日：2009-08-06
申请号：US12306889
申请日：2007-06-22
申请人： Norihiko Fukatsu , Hiroyuki Morijiri , Chitoshi Shimakawa , Koichi Tokunaga , Seiichi Kobayashi
发明人： Norihiko Fukatsu , Hiroyuki Morijiri , Chitoshi Shimakawa , Koichi Tokunaga , Seiichi Kobayashi
IPC分类号： C07C255/47 , C07C253/10 , B01J31/22 , C07C209/48
CPC分类号： B01J31/185 , B01J2231/32 , B01J2531/847 , C07C209/48 , C07C253/10 , C07C2602/42 , C07C211/19 , C07C255/47
摘要： The present invention is to provide a process for producing dicyanonorbornane characterized by causing hydrogen cyanide to undergo addition reaction with cyanonorbornene (bicyclo[2.2.1]-5-heptene-2-carbonitrile) in the presence of a zerovalent nickel complex catalyst which is produced by using a phosphite represented by P(x)(y)(z) (wherein P is a phosphorus atom, and x, y and z are each OR, where R represents an aryl group having not more than 18 carbon atoms) as a ligand to reduce a nickel halide with at least one metal selected among zinc, cadmium, beryllium, aluminum, iron and cobalt, wherein the phosphite is one which has a phosphate content of 1.0 weight % or lower based on the whole phosphite.
摘要翻译： 本发明提供一种制备二氰基降冰片烷的方法，其特征在于在生成的零价镍络合物催化剂存在下使氰化氢与氰基降冰片烯（双环[2.2.1] -5-庚烯-2-腈）进行加成反应 通过使用由P（x）（y）（z）表示的亚磷酸酯（其中P为磷原子，x，y和z各自为OR，其中R为不大于18个碳原子的芳基）为 配体，用锌，镉，铍，铝，铁和钴中的至少一种金属还原卤化镍，其中亚磷酸盐是基于全部亚磷酸盐的磷酸盐含量为1.0重量％以下的亚磷酸盐。
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5.发明申请Process for production of isocyanate, isocyanate produced by the process, and use of the isocyanate 有权通过该方法生产异氰酸酯，异氰酸酯和使用异氰酸酯的方法公开(公告)号：US20090124785A1
公开(公告)日：2009-05-14
申请号：US11988490
申请日：2006-07-20
申请人： Chitoshi Shimakawa , Hiroyuki Morijiri , Hidetoshi Hayashi , Norihiko Fukatsu , Seiichi Kobayashi , Homare Yumoto , Junichi Ishiyama , Shinya Tsuchiyama
发明人： Chitoshi Shimakawa , Hiroyuki Morijiri , Hidetoshi Hayashi , Norihiko Fukatsu , Seiichi Kobayashi , Homare Yumoto , Junichi Ishiyama , Shinya Tsuchiyama
IPC分类号： C08G18/32 , C07C263/00 , C07C209/74
CPC分类号： C08G18/72 , C07C263/10 , C08G18/757 , C08G18/7642 , C07C265/14
摘要： An isocyanate has been widely used as a starting material for the production of a polyurethane material, a polyisocyanurate material or the like which is suitably applicable to the field of optical materials. Disclosed is a process for producing an isocyanate which includes a step for producing the isocyanate in the form of a hydrochloride with improved productivity. A process for producing a linear or cyclic aliphatic isocyanate comprising the step of reacting a linear or cyclic aliphatic amine with hydrogen chloride to yield a hydrochloride of the linear or cyclic aliphatic amine, the step being performed under a pressure higher by 0.01 MPa or more than the atmospheric pressure.
摘要翻译： 异氰酸酯已经广泛用作生产适用于光学材料领域的聚氨酯材料，聚异氰脲酸酯材料等的起始材料。 公开了一种异氰酸酯的制造方法，其包括以生产率提高的盐酸盐形式的异氰酸酯的制造工序。 一种直链或环状脂肪族异氰酸酯的制造方法，其特征在于，使直链状或环状的脂肪族胺与氯化氢反应，生成线性或环状脂族胺的盐酸盐，该步骤是在高于0.01MPa以上的压力下进行的 大气压力。
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6.发明授权Process for production of isocyanate, isocyanate produced by the process, and use of the isocyanate 有权通过该方法生产异氰酸酯，异氰酸酯和使用异氰酸酯的方法公开(公告)号：US08183407B2
公开(公告)日：2012-05-22
申请号：US11988490
申请日：2006-07-20
申请人： Chitoshi Shimakawa , Hiroyuki Morijiri , Hidetoshi Hayashi , Norihiko Fukatsu , Seiichi Kobayashi , Homare Yumoto , Junichi Ishiyama , Shinya Tsuchiyama
发明人： Chitoshi Shimakawa , Hiroyuki Morijiri , Hidetoshi Hayashi , Norihiko Fukatsu , Seiichi Kobayashi , Homare Yumoto , Junichi Ishiyama , Shinya Tsuchiyama
IPC分类号： C07C291/00
CPC分类号： C08G18/72 , C07C263/10 , C08G18/757 , C08G18/7642 , C07C265/14
摘要： An isocyanate has been widely used as a starting material for the production of a polyurethane material, a polyisocyanurate material or the like which is suitably applicable to the field of optical materials. Disclosed is a process for producing an isocyanate which includes a step for producing the isocyanate in the form of a hydrochloride with improved productivity. A process for producing a linear or cyclic aliphatic isocyanate comprising the step of reacting a linear or cyclic aliphatic amine with hydrogen chloride to yield a hydrochloride of the linear or cyclic aliphatic amine, the step being performed under a pressure higher by 0.01 MPa or more than the atmospheric pressure.
摘要翻译： 异氰酸酯已经广泛用作生产适用于光学材料领域的聚氨酯材料，聚异氰脲酸酯材料等的起始材料。 公开了一种异氰酸酯的制造方法，其包括以生产率提高的盐酸盐形式的异氰酸酯的制造工序。 一种直链或环状脂肪族异氰酸酯的制造方法，其特征在于，使直链状或环状的脂肪族胺与氯化氢反应，生成线性或环状脂族胺的盐酸盐，该步骤是在高于0.01MPa以上的压力下进行的 大气压力。
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7.发明申请Process for Producing Pentaerythritol Mercaptocarboxylic Acid Ester, Pentaerythritol Mercaptocarboxylic Acid Ester Obtained by the Same, and Use Thereof 审中-公开制备季戊四醇巯基羧酸酯的方法，由其获得的季戊四醇巯基羧酸酯及其用途公开(公告)号：US20090270583A1
公开(公告)日：2009-10-29
申请号：US12084257
申请日：2005-10-31
CPC分类号： C07C319/12 , C08G18/3876 , C08G18/7642 , G02B1/04 , C08L75/04 , C07C323/52
摘要： Pentaerythritol which contains none of the alkali metals and the alkaline earth metals or which contains at least one of these in a total amount of 1.0 weight % or smaller is reacted with a mercaptocarboxylic acid to produce a pentaerythritol mercaptocarboxylic acid ester.
摘要翻译： 不含碱金属和碱土金属或其中至少一种的总量为1.0重量％以下的季戊四醇与巯基羧酸反应，生成季戊四醇巯基羧酸酯。
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8.发明授权Process for producing dicyanonorbornane and zerovalent nickel complex catalyst 有权生产二氰基降冰片烷和零价镍络合物催化剂的方法公开(公告)号：US08183404B2
公开(公告)日：2012-05-22
申请号：US12306889
申请日：2007-06-22
申请人： Norihiko Fukatsu , Hiroyuki Morijiri , Chitoshi Shimakawa , Koichi Tokunaga , Seiichi Kobayashi
发明人： Norihiko Fukatsu , Hiroyuki Morijiri , Chitoshi Shimakawa , Koichi Tokunaga , Seiichi Kobayashi
IPC分类号： C07C253/10
CPC分类号： B01J31/185 , B01J2231/32 , B01J2531/847 , C07C209/48 , C07C253/10 , C07C2602/42 , C07C211/19 , C07C255/47
摘要： The present invention is to provide a process for producing dicyanonorbornane characterized by causing hydrogen cyanide to undergo addition reaction with cyanonorbornene (bicyclo[2.2.1]-5-heptene-2-carbonitrile) in the presence of a zerovalent nickel complex catalyst which is produced by using a phosphite represented by P(x)(y)(z) (wherein P is a phosphorus atom, and x, y and z are each OR, where R represents an aryl group having not more than 18 carbon atoms) as a ligand to reduce a nickel halide with at least one metal selected among zinc, cadmium, beryllium, aluminum, iron and cobalt, wherein the phosphite is one which has a phosphate content of 1.0 weight % or lower based on the whole phosphite.
摘要翻译： 本发明提供一种制备二氰基降冰片烷的方法，其特征在于在生成的零价镍络合物催化剂存在下使氰化氢与氰基降冰片烯（双环[2.2.1] -5-庚烯-2-腈）进行加成反应 通过使用由P（x）（y）（z）表示的亚磷酸酯（其中P是磷原子，x，y和z各自为OR，其中R表示不超过18个碳原子的芳基）作为 配体，用锌，镉，铍，铝，铁和钴中的至少一种金属还原卤化镍，其中亚磷酸盐是基于全部亚磷酸盐的磷酸盐含量为1.0重量％以下的亚磷酸盐。
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