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    Process for producing dicyanonorbornane and zerovalent nickel complex catalyst
    4.
    发明授权
    Process for producing dicyanonorbornane and zerovalent nickel complex catalyst 有权
    生产二氰基降冰片烷和零价镍络合物催化剂的方法

    公开(公告)号：US08183404B2

    公开(公告)日：2012-05-22

    申请号：US12306889

    申请日：2007-06-22

    申请人： Norihiko Fukatsu ,  Hiroyuki Morijiri ,  Chitoshi Shimakawa ,  Koichi Tokunaga ,  Seiichi Kobayashi

    发明人： Norihiko Fukatsu ,  Hiroyuki Morijiri ,  Chitoshi Shimakawa ,  Koichi Tokunaga ,  Seiichi Kobayashi

    IPC分类号： C07C253/10

    CPC分类号： B01J31/185 ,  B01J2231/32 ,  B01J2531/847 ,  C07C209/48 ,  C07C253/10 ,  C07C2602/42 ,  C07C211/19 ,  C07C255/47

    摘要： The present invention is to provide a process for producing dicyanonorbornane characterized by causing hydrogen cyanide to undergo addition reaction with cyanonorbornene (bicyclo[2.2.1]-5-heptene-2-carbonitrile) in the presence of a zerovalent nickel complex catalyst which is produced by using a phosphite represented by P(x)(y)(z) (wherein P is a phosphorus atom, and x, y and z are each OR, where R represents an aryl group having not more than 18 carbon atoms) as a ligand to reduce a nickel halide with at least one metal selected among zinc, cadmium, beryllium, aluminum, iron and cobalt, wherein the phosphite is one which has a phosphate content of 1.0 weight % or lower based on the whole phosphite.

    摘要翻译： 本发明提供一种制备二氰基降冰片烷的方法，其特征在于在生成的零价镍络合物催化剂存在下使氰化氢与氰基降冰片烯（双环[2.2.1] -5-庚烯-2-腈）进行加成反应 通过使用由P（x）（y）（z）表示的亚磷酸酯（其中P是磷原子，x，y和z各自为OR，其中R表示不超过18个碳原子的芳基）作为 配体，用锌，镉，铍，铝，铁和钴中的至少一种金属还原卤化镍，其中亚磷酸盐是基于全部亚磷酸盐的磷酸盐含量为1.0重量％以下的亚磷酸盐。

    Polycyclic polyamines
    6.
    发明授权
    Polycyclic polyamines 失效
    多环多胺

    公开(公告)号：US4296004A

    公开(公告)日：1981-10-20

    申请号：US152905

    申请日：1980-05-23

    申请人： Edgar R. Rogier

    发明人： Edgar R. Rogier

    IPC分类号： C07C211/19 ,  C08G59/50

    CPC分类号： C08G59/5026 ,  C07C211/19 ,  C07C2103/68 ,  C07C2103/91

    摘要： Disclosed herein are tricyclic and pentacyclic polyamines having a secondary or tertiary amine group on an amine functional substituent and at least one primary amine group on each of two amine functional substituents in the molecule. These compounds function excellently as non-visibly carbonating epoxy curing agents and in addition unlike most other amines exhibit a mild amine odor.

    摘要翻译： 本文公开了在胺官能取代基上具有仲胺或叔胺基团的三环和五环多胺，以及分子中两个胺官能取代基中的每一个上的至少一个伯胺基团。 这些化合物作为非显着的碳酸化环氧固化剂具有优异的功能，此外与大多数其他胺不同，胺显示温和的胺气味。

    PREPARATION METHOD OF ALDEHYDE COMPOUND
    10.
    发明申请
    PREPARATION METHOD OF ALDEHYDE COMPOUND 有权
    醛类化合物的制备方法

    公开(公告)号：US20150299109A1

    公开(公告)日：2015-10-22

    申请号：US14440992

    申请日：2013-11-08

    申请人： MITSUI CHEMICALS, INC.

    发明人： Koichi Tokunaga ,  Naoyuki Kakinuma ,  Shigetoshi Kuma

    IPC分类号： C07C255/47 ,  C07C211/38

    CPC分类号： C07C255/47 ,  B01J31/24 ,  C07C211/19 ,  C07C211/38 ,  C07C265/14 ,  C07C2602/40 ,  C07C2602/42

    摘要： A preparation method of an aldehyde compound of the present invention includes a step of reacting a compound represented by the following general formula (a1) with hydrogen and carbon monoxide in the presence of a metal compound including 0.01 ppmmol to 10 ppmmol of a metal belonging to Groups 8 to 10 with respect to 1 mole of the compound and a phosphorus compound, and in the step, the amount of acrylonitrile included in the compound represented by the general formula (a1) is equal to or less than 200-fold by mole with respect to 1 mole of the metal belonging to Groups 8 to 10.

    摘要翻译： 本发明的醛化合物的制备方法包括以下通式（a1）表示的化合物与氢和一氧化碳在金属化合物的存在下反应的步骤，所述金属化合物包括0.01ppmmol至10ppmmol的属于 组8〜10相对于1摩尔化合物和磷化合物，在该步骤中，通式（a1）表示的化合物中所含的丙烯腈的量等于或小于200倍摩尔，与 相对于1摩尔属于第8至10族的金属。