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公开(公告)号：US10739269B2
公开(公告)日：2020-08-11
申请号：US16164011
申请日：2018-10-18
申请人： Sankaran Murugesan , Radhika Suresh , Valery N. Khabashesku , Qusai Darugar , Stephen Mark Heath
发明人： Sankaran Murugesan , Radhika Suresh , Valery N. Khabashesku , Qusai Darugar , Stephen Mark Heath
摘要： A method of analyzing a well sample for a well treatment additive includes contacting the sample with functionalized metallic nanoparticles that contain metallic nanoparticles functionalized with a functional group including a cyano group, a thiol group, a carboxyl group, an amino group, a boronic acid group, an aza group, an ether group, a hydroxyl group, or a combination including at least one of the foregoing; irradiating the sample contacted with the functionalized metallic nanoparticles with electromagnetic radiation at a selected energy level; measuring a Raman spectrum emitted from the sample; and determining presence, type or concentration of the well treatment additive in the sample from the Raman spectrum.
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2.发明授权公开(公告)号：US10209193B2
公开(公告)日：2019-02-19
申请号：US15143886
申请日：2016-05-02
IPC分类号： G01N21/65
摘要： A method and apparatus for estimating a concentration of chemicals in a fluid flowing in a fluid passage is disclosed. A sample of the fluid is placed on a substrate comprising a first layer of carbon nanotubes and a second layer of metal nanowires. An energy source radiates the fluid sample with electromagnetic radiation at a selected energy level, and a detector measures an energy level of radiation emitted from the fluid sample in response to the electromagnetic radiation. A processor determines a Raman spectrum of the fluid sample from the energy level of the emitted radiation and estimates the concentration of a selected chemical in the fluid sample based on the Raman spectrum.
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公开(公告)号：US09958394B2
公开(公告)日：2018-05-01
申请号：US15677813
申请日：2017-08-15
申请人： Sankaran Murugesan , Radhika Suresh , Darryl N. Ventura , Bradley G. Harrell , Valery N. Khabashesku , Qusai A. Darugar
发明人： Sankaran Murugesan , Radhika Suresh , Darryl N. Ventura , Bradley G. Harrell , Valery N. Khabashesku , Qusai A. Darugar
CPC分类号： G01N21/65 , C10G29/00 , C10G2300/202 , C10G2300/4075 , G01J3/02 , G01N21/658 , G01N33/2835
摘要： A system and method for estimating a concentration of monoethanolamine (MEA) in a fluid. A substrate for supporting a sample of the fluid during testing includes a carbon nanotube mat layer, a silver nanowire layer disposed on the carbon nanotube mat layer, and a chemical enhancer layer disposed on the silver nanowire layer. A sample of the fluid is placed on the substrate, and the fluid sample is radiated with electromagnetic radiation at a selected energy level. A detector measures a Raman spectrum emitted from the sample in response to the electromagnetic radiation. A processor estimates the concentration of MEA in the sample from the Raman spectrum and adds a corrosion inhibitor to the fluid in an amount based on the estimated concentration of MEA to reduce the concentration of MEA in the fluid.
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4.发明申请公开(公告)号：US20180067054A1
公开(公告)日：2018-03-08
申请号：US15698007
申请日：2017-09-07
IPC分类号： G01N21/65
CPC分类号： G01N21/658 , G01N2201/127 , G01N2201/12746
摘要： A method of analyzing a selected refinery chemical at a low concentration comprises contacting a sample with functionalized metallic nanoparticles that contain metallic nanoparticles functionalized with a functional group comprising a cyano group, a thiol group, a carboxyl group, an amino group, a boronic acid group, an aza group, an ether group, a hydroxyl group, or a combination comprising at least one of the foregoing; radiating the sample contacted with the functionalized metallic nanoparticles with electromagnetic radiation at a selected energy level; measuring a Raman spectrum emitted from the sample; and determining the presence or a concentration of a selected refinery chemical in the sample from the Raman spectrum.
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公开(公告)号：US20200124534A1
公开(公告)日：2020-04-23
申请号：US16164011
申请日：2018-10-18
申请人： Sankaran Murugesan , Radhika Suresh , Valery N. Khabashesku , Qusai Darugar , Stephen Mark Heath
发明人： Sankaran Murugesan , Radhika Suresh , Valery N. Khabashesku , Qusai Darugar , Stephen Mark Heath
摘要： A method of analyzing a well sample for a well treatment additive includes contacting the sample with functionalized metallic nanoparticles that contain metallic nanoparticles functionalized with a functional group including a cyano group, a thiol group, a carboxyl group, an amino group, a boronic acid group, an aza group, an ether group, a hydroxyl group, or a combination including at least one of the foregoing; irradiating the sample contacted with the functionalized metallic nanoparticles with electromagnetic radiation at a selected energy level; measuring a Raman spectrum emitted from the sample; and determining presence, type or concentration of the well treatment additive in the sample from the Raman spectrum.
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6.发明申请公开(公告)号：US20170315061A1
公开(公告)日：2017-11-02
申请号：US15143886
申请日：2016-05-02
IPC分类号： G01N21/65
CPC分类号： G01N21/658
摘要： A method and apparatus for estimating a concentration of chemicals in a fluid flowing in a fluid passage is disclosed. A sample of the fluid is placed on a substrate comprising a first layer of carbon nanotubes and a second layer of metal nanowires. An energy source radiates the fluid sample with electromagnetic radiation at a selected energy level, and a detector measures an energy level of radiation emitted from the fluid sample in response to the electromagnetic radiation. A processor determines a Raman spectrum of the fluid sample from the energy level of the emitted radiation and estimates the concentration of a selected chemical in the fluid sample based on the Raman spectrum.
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公开(公告)号：US10908092B2
公开(公告)日：2021-02-02
申请号：US16157574
申请日：2018-10-11
摘要： A cyanide-functionalized gold nanoparticle. A method of making cyanide-functionalized gold nanoparticles includes forming an aqueous reaction mixture comprising a gold precursor and glycine, keeping the reaction mixture at about 18° C. to about 50° C. for at least 6 days to provide formation of the cyanide-functionalized gold nanoparticles, and isolating the cyanide-functionalized gold nanoparticles from the reaction mixture. A method of analyzing a sample, comprising contacting cyanide-functionalized gold nanoparticles with the sample and performing an analytical method on the sample. A sensor comprises cyanide-functionalized gold nanoparticles.
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8.发明申请公开(公告)号：US20180363452A1
公开(公告)日：2018-12-20
申请号：US15626389
申请日：2017-06-19
CPC分类号： E21B47/1015 , B82Y15/00 , C09K8/032 , C09K8/035 , C09K8/56 , C09K8/58 , C09K8/665 , C09K8/72 , C09K8/805 , C09K2208/10 , G01N33/241
摘要： A method of determining a property within a subterranean formation comprises introducing silica nanoparticles into a well; obtaining a sample of a fluid produced from the well; and analyzing the sample for presence of the silica nanoparticles, wherein the silica nanoparticles comprise a core, a donor chromophore, an acceptor chromophore, and an outer silica shell; the donor chromophore and the acceptor chromophore being selected such that an emission spectrum of the donor chromophore overlaps with an absorption spectrum of the acceptor chromophore.
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9.发明申请公开(公告)号：US20180246039A1
公开(公告)日：2018-08-30
申请号：US15968506
申请日：2018-05-01
申请人： Sankaran Murugesan , Radhika Suresh , Darryl N. Ventura , Bradley G. Harrell , Valery N. Khabashesku , Qusai A. Darugar
发明人： Sankaran Murugesan , Radhika Suresh , Darryl N. Ventura , Bradley G. Harrell , Valery N. Khabashesku , Qusai A. Darugar
CPC分类号： G01N21/65 , C10G29/00 , C10G2300/202 , C10G2300/4075 , G01J3/02 , G01N21/658 , G01N33/2835
摘要： A system and method for estimating a concentration of monoethanolamine (MEA) in a fluid. A substrate for supporting a sample of the fluid during testing includes a carbon nanotube mat layer, a silver nanowire layer disposed on the carbon nanotube mat layer, and a chemical enhancer layer disposed on the silver nanowire layer. A sample of the fluid is placed on the substrate, and the fluid sample is radiated with electromagnetic radiation at a selected energy level. A detector measures a Raman spectrum emitted from the sample in response to the electromagnetic radiation. A processor estimates the concentration of MEA in the sample from the Raman spectrum and adds a corrosion inhibitor to the fluid in an amount based on the estimated concentration of MEA to reduce the concentration of MEA in the fluid.
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公开(公告)号：US20140027116A1
公开(公告)日：2014-01-30
申请号：US13561314
申请日：2012-07-30
CPC分类号： C09K8/56 , C09K2208/10 , E21B33/13
摘要： A process for stabilizing particles includes disposing reactive nanoparticles in a borehole; contacting the reactive nanoparticles with a resin; introducing a curing agent; and curing the resin and reactive nanoparticles with the curing agent to form a nanocomposite, wherein, during curing, the nanocomposite is bonded to the particles to stabilize the particles. A process for consolidating particles includes coating the particles with a resin; introducing reactive nanoparticles; curing the resin and reactive nanoparticles with a curing agent to form a nanocomposite which is bonded to the particles; and controlling a rate of the curing by an amount of the curing agent which is present with the resin, wherein the nanocomposite bonded to the particles is thermally stable up to at least 600° F. (315° C.). A system comprises a resin; reactive nanoparticles; a curing agent to form a nanocomposite; and particles disposed in a downhole location to which the nanocomposite binds.
摘要翻译： 用于稳定颗粒的方法包括将反应性纳米颗粒设置在钻孔中; 使反应性纳米粒子与树脂接触; 引入固化剂; 并用固化剂固化树脂和活性纳米颗粒以形成纳米复合材料，其中在固化过程中，将纳米复合材料结合到颗粒上以稳定颗粒。 固结颗粒的方法包括用树脂涂覆颗粒; 引入反应性纳米粒子; 用固化剂固化树脂和反应性纳米颗粒以形成结合到颗粒的纳米复合材料; 并且通过树脂存在的固化剂的量控制固化速率，其中结合到颗粒的纳米复合材料在至少600°F（315℃）下是热稳定的。 系统包括树脂; 反应性纳米粒子; 形成纳米复合材料的固化剂; 以及设置在纳米复合物结合到的井下位置的颗粒。
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