摘要:
A thermoplastic elastomer composition for use in automotive interiors, wallcoverings, upholstery, advertising banners and films and tenting which comprises a major amount of a thermoplastic elastomer or elastomers having a weight average melt index of less than 6, a minor amount of polyolefin, a minor amount of a polymeric elastomer and a filler material.
摘要:
Sodium (S)-2-(6-methoxy-2-naphthyl)propionate of at least 99% chiral purity is formed from (S)-2-(6-methoxy-2-naphthyl)propionic acid having a chiral purity of at least about 82%, but below 99%. This is done by distilling a two-phase mixture formed from (i) the (S)-2-(6-methoxy-2-naphthyl)propionic acid, (ii) water, (iii) sodium hydroxide, sodium oxide and/or at least one basic inorganic sodium salt in an amount proportioned to neutralize from about 50 to about 99% of said acid, and optionally but preferably, (iv) an inert organic solvent that has a boiling point of at least 95.degree. C. at 760 mm Hg such that water is removed from said mixture, and a pot residue containing sodium (S)-2-(6-methoxy-2-naphthyl)propionate of at least 99% chiral purity is formed.
摘要翻译:具有至少99%手性纯度的(S)-2-(6-甲氧基-2-萘基)丙酸钠由手性纯度为(S)-2-(6-甲氧基-2-萘基)丙酸形成 至少约82%,但低于99%。 这是通过蒸馏由(i)(S)-2-(6-甲氧基-2-萘基)丙酸形成的两相混合物,(ii)水,(iii)氢氧化钠,氧化钠和/或 至少一种碱性无机钠盐,其成分为中和所述酸的约50至约99%,并且任选但优选(iv)在760℃下具有至少95℃的沸点的惰性有机溶剂 mm Hg,使得从所述混合物中除去水,并形成含有至少99%手性纯度的(S)-2-(6-甲氧基-2-萘基)丙酸钠的罐残渣。
摘要:
Optically active carboxylic acids, salts or esters, such as the profen-type compounds, are racemized in the presence by nitrogenous bases such as methylbenzylamine by heating an aqueous solution of such optically active compounds in the presence of a suitable excess of an alkali metal hydroxide relative to the amount optically active carboxylic compound present in the solution. The process not only enables conversion of inactive or undesirable enantiomers of compounds such as naproxen or ibuprofen into a usable, desirable enantiomers in an efficient and economical manner, but avoids conversion of the nitrogenous base into amide. Thus the deleterious consequences of amide formation are avoided.
摘要:
The yield of acetyl chloride from the reaction between acetic anhydride and hydrogen chloride is increased by withdrawing acetyl chloride, optionally together with at least some of the acetic acid by-product, from the reaction mixture as the reaction proceeds and recycling the remainder of the reaction mixture to the reactor for reaction with additional hydrogen chloride.
摘要:
A thermoplastic elastomer composition for use in automotive interiors, wallcoverings, upholstery, advertising banners and films and tenting which comprises a major amount of a thermoplastic elastomer or elastomers having a weight average melt index of less than 6, a minor amount of a polymeric elastomer, a flame retardant, a maleated polypropylene, and a filler material.
摘要:
A process for obtaining a substantially pure enantiomer of an aryl-substituted aliphatic carboxylic acid is described. In this process, the aryl-substituted aliphatic carboxylic acid is reacted with an inorganic base in the presence of an organic base to substantially enrich the precipitate in one of the enantiomers and an improved yield. Substantially pure, enantiomeric salt is separated, leaving a mother liquor comprising the solvent and aryl-substituted aliphatic carboxylic acid enriched in the other enantiomer.
摘要:
Apparatus is provided for eliminating manual completion of tickets by operators at operator positions, one or more of which are operator cordboard positions, of a telephone exchange. The apparatus comprises a keyboard and display unit and an independently operable processing and storage unit provided individually for each operator position, the operator position and keyboard and display unit being connected to the processing and storage unit. Each operator position functions with its associated units independently of the other operator positions and any central processing unit. All of the processing and storage units are coupled via a concentrator to automatic message accounting equipment for forwarding call records thereto for billing. The concentrator is connected to teletypewriters and also to a storage unit for storage of call records in the event of failure of the automatic message accounting equipment.
摘要:
An infantry training simulation system comprising at least one firing lane, with at least one display arranged substantially near the end of the firing lane. A trainee experiencing the simulation can carry at least one physical or virtual weapon, which is typically similar to a traditional infantry weapon. To facilitate navigation and other interaction with the simulation, the weapon is preferably outfitted with at least one controller. At least one computer is communicatively coupled to the display and the weapon. The computer can monitor input from the at least one controller, and modifies the training simulation displayed on the display based on the input.
摘要:
A plastic ignition high voltage switch housing comprising two separately molded components formed of a high temperature, high strength insulating thermoplastic material, each component containing one bushing. The two components are spun welded together while maintaining axial alignment of the bushings. The two components can be designed to permit the placement of a gasket between them prior to spin welding, thereby capturing the gasket within the housing.
摘要:
A coupling for connecting the end of the camshaft of an internal combustion engine to the drive shaft of an ignition distributor. The coupling comprises a drive coupling member that is fixed to the drive shaft of the ignition distributor. The coupling member has a pair of axially extending lugs that have surfaces that engage surfaces formed on a pair of lugs that extend axially from the end of the camshaft. A spring member is fixed to the coupling member which has a pair of curved spring portions that engage other surfaces on the camshaft lugs and which serve to prevent backlash between the shafts.