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1.发明授权Water-soluble film having blend of PVOH polymers, and packets made therefrom 有权具有PVOH聚合物共混物的水溶性薄膜和由其制成的包装公开(公告)号：US09133329B2
公开(公告)日：2015-09-15
申请号：US13016612
申请日：2011-01-28
申请人： Frank W. Denome , Steven G. Friedrich , Regine Labeque , David M. Lee , Roxane Rosmaninho , Jichun Shi , Andrew P. Verrall
发明人： Frank W. Denome , Steven G. Friedrich , Regine Labeque , David M. Lee , Roxane Rosmaninho , Jichun Shi , Andrew P. Verrall
CPC分类号： C08L29/04 , B65D65/46 , C08J5/18 , C08J2329/04 , C08L2203/16 , C08L2205/025 , C11D17/042 , C11D17/045 , Y10T428/1334 , Y10T428/1341 , Y10T428/1345
摘要： Disclosed are plasticized, water-soluble films having favorable cold-water solubility, wet handling, and thermoforming characteristics, and which can include a PVOH resin made up of blend of two or more PVOH polymers each having a monomodal molecular weight distribution, and the PVOH resin characterized by a viscosity in a range of about 13.5 cP to about 20 cP (or a corresponding weight average molecular weight), a degree of hydrolysis of about 84% to about 92%, a polydispersity index value in a range of about 1 to about 5, a residual water content of about 4 wt. % to about 10 wt. %, and a Resin Selection Index value in a range of 0.255 to 0.315; methods of making the films; compositions including PVOH resins for making the films; and pouch and packet articles made from the films.
摘要翻译： 公开了具有良好的冷水溶解性，湿处理性和热成型特性的增塑的水溶性膜，其可以包括由两种或多种各自具有单峰分子量分布的PVOH聚合物和PVOH的共混物组成的PVOH树脂 树脂，其特征在于粘度在约13.5cP至约20cP（或相应的重均分子量）的范围内，水解度为约84％至约92％，多分散指数值在约1至 约5，残留水含量约4wt。 ％至约10wt。 ％，树脂选择指数值在0.255〜0.315的范围内; 制作薄膜的方法; 包括用于制造膜的PVOH树脂的组合物; 以及由电影制成的袋和包装物品。
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公开(公告)号：US09624457B2
公开(公告)日：2017-04-18
申请号：US13325656
申请日：2011-12-14
CPC分类号： C11D17/043 , C11D1/02 , C11D3/2044 , C11D3/2065 , C11D3/2068 , C11D3/43 , C11D17/042
摘要： The present invention relates to a method for controlling the plasticization of a water soluble film comprising preparing a detergent composition comprising anionic surfactant and solvent system comprising at least one primary solvent having Hansen solubility (δ) of less than 30 and encapsulating said composition in a water soluble film to form a pouch unitized dose product.
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3.发明申请WATER-SOLUBLE FILM HAVING BLEND OF PVOH POLYMERS, AND PACKETS MADE THEREFROM 有权具有PVOH聚合物混合物的水溶性薄膜及其制备的包装公开(公告)号：US20110189413A1
公开(公告)日：2011-08-04
申请号：US13016612
申请日：2011-01-28
申请人： Frank W. Denome , Steven G. Friedrich , Regine Labeque , David M. Lee , Roxane Rosmaninho , Jichun Shi , Andrew P. Verrall
发明人： Frank W. Denome , Steven G. Friedrich , Regine Labeque , David M. Lee , Roxane Rosmaninho , Jichun Shi , Andrew P. Verrall
CPC分类号： C08L29/04 , B65D65/46 , C08J5/18 , C08J2329/04 , C08L2203/16 , C08L2205/025 , C11D17/042 , C11D17/045 , Y10T428/1334 , Y10T428/1341 , Y10T428/1345
摘要： Disclosed are plasticized, water-soluble films having favorable cold-water solubility, wet handling, and thermoforming characteristics, and which can include a PVOH resin made up of blend of two or more PVOH polymers each having a monomodal molecular weight distribution, and the PVOH resin characterized by a viscosity in a range of about 13.5 cP to about 20 cP (or a corresponding weight average molecular weight), a degree of hydrolysis of about 84% to about 92%, a polydispersity index value in a range of about 1 to about 5, a residual water content of about 4 wt. % to about 10 wt. %, and a Resin Selection Index value in a range of 0.255 to 0.315; methods of making the films; compositions including PVOH resins for making the films; and pouch and packet articles made from the films.
摘要翻译： 公开了具有良好的冷水溶解性，湿处理性和热成型特性的增塑的水溶性膜，其可以包括由两种或多种各自具有单峰分子量分布的PVOH聚合物和PVOH的共混物组成的PVOH树脂 树脂，其特征在于粘度在约13.5cP至约20cP（或相应的重均分子量）的范围内，水解度为约84％至约92％，多分散指数值在约1至 约5，残留水含量约4wt。 ％至约10wt。 ％，树脂选择指数值在0.255〜0.315的范围内; 制作薄膜的方法; 包括用于制造膜的PVOH树脂的组合物; 以及由电影制成的袋和包装物品。
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公开(公告)号：US20120175797A1
公开(公告)日：2012-07-12
申请号：US13325656
申请日：2011-12-14
IPC分类号： A61J3/07
CPC分类号： C11D17/043 , C11D1/02 , C11D3/2044 , C11D3/2065 , C11D3/2068 , C11D3/43 , C11D17/042
摘要： The present invention relates to a method for controlling the plasticization of a water soluble film comprising preparing a detergent composition comprising anionic surfactant and solvent system comprising at least one primary solvent having Hansen solubility (δ) of less than 30 and encapsulating said composition in a water soluble film to form a pouch unitized dose product.
摘要翻译： 本发明涉及一种用于控制水溶性薄膜增塑的方法，包括制备包含阴离子表面活性剂和溶剂体系的洗涤剂组合物，所述溶剂体系包含至少一种Hansen溶解度（δ）小于30的一级溶剂，并将所述组合物包封在水中 可溶性膜以形成袋状单位剂量产品。
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5.发明授权Water-soluble film having blend of PVOH polymers, and packets made therefrom 有权具有PVOH聚合物共混物的水溶性薄膜和由其制成的包装公开(公告)号：US08697624B2
公开(公告)日：2014-04-15
申请号：US13017437
申请日：2011-01-31
申请人： Frank William Denome , Steven G. Friedrich , Regine Labeque , David M Lee , Jichun Shi , Andrew P. Verrall , Roxane Rosmaninho
发明人： Frank William Denome , Steven G. Friedrich , Regine Labeque , David M Lee , Jichun Shi , Andrew P. Verrall , Roxane Rosmaninho
CPC分类号： C08L29/04 , B65D65/46 , C08J5/18 , C08J2329/04 , C08L2203/16 , C08L2205/025 , C11D17/042 , C11D17/045 , Y10T428/1334 , Y10T428/1341 , Y10T428/1345
摘要： Disclosed are plasticized, water-soluble films having favorable cold-water solubility, wet handling, and thermoforming characteristics, and which can include a PVOH resin made up of blend of two or more PVOH polymers each having a monomodal molecular weight distribution, and the PVOH resin characterized by a viscosity in a range of about 13.5 cP to about 20 cP (or a corresponding weight average molecular weight), a degree of hydrolysis of about 84% to about 92%, a polydispersity index value in a range of about 1 to about 5, a residual water content of about 4 wt. % to about 10 wt. %, and a Resin Selection Index value in a range of 0.255 to 0.315; methods of making the films; compositions including PVOH resins for making the films; and pouch and packet articles made from the films.
摘要翻译： 公开了具有良好的冷水溶解性，湿处理性和热成型特性的增塑的水溶性膜，其可以包括由两种或多种各自具有单峰分子量分布的PVOH聚合物和PVOH的共混物组成的PVOH树脂 树脂，其特征在于粘度在约13.5cP至约20cP（或相应的重均分子量）的范围内，水解度为约84％至约92％，多分散指数值在约1至 约5，残留水含量约4wt。 ％至约10wt。 ％，树脂选择指数值在0.255〜0.315的范围内; 制作薄膜的方法; 包括用于制造膜的PVOH树脂的组合物; 以及由电影制成的袋和包装物品。
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公开(公告)号：US20130029895A1
公开(公告)日：2013-01-31
申请号：US13548306
申请日：2012-07-13
申请人： Jean-Luc Phillippe Bettiol , Katrien Decraene , Marc Francois Theophile Evers , Karl Ghislain Braeckman , Bjorn Van Overstraete , Robby Renilde Francoise Keuleers , Joanna Margaret Clarke , Roxane Rosmaninho , Raffaele Pinna , Christopher Stephen Jones
发明人： Jean-Luc Phillippe Bettiol , Katrien Decraene , Marc Francois Theophile Evers , Karl Ghislain Braeckman , Bjorn Van Overstraete , Robby Renilde Francoise Keuleers , Joanna Margaret Clarke , Roxane Rosmaninho , Raffaele Pinna , Christopher Stephen Jones
IPC分类号： C11D17/00
CPC分类号： C11D11/0023 , C11D3/1253 , C11D3/1266 , C11D3/2086 , C11D3/2093 , C11D3/222 , C11D3/37 , C11D17/0017
摘要： The invention relates to a multiphase liquid detergent composition comprising at least one cleaning phase and at least one benefit phase, a surfactant, and a crystalline structurant. The crystalline structurant being substantially present in a non-lamellar phase. The invention also relates to a multiphase liquid detergent composition comprising at least two visually distinct liquid phases, a surfactant, and at least two incompatible or reactive materials. The first incompatible or reactive material is distributed in a first visually distinct phase and a second incompatible or reactive material is distributed in a second visually distinct phase. The present invention further relates to methods of cleaning dishware using such multiphase liquid detergent compositions.
摘要翻译： 本发明涉及包含至少一个清洗相和至少一个有益相，表面活性剂和结晶结构剂的多相液体洗涤剂组合物。 晶体结构剂基本上存在于非层状相中。 本发明还涉及一种多相液体洗涤剂组合物，其包含至少两个视觉上不同的液相，表面活性剂和至少两种不相容或反应性材料。 第一不相容或反应性材料分布在第一视觉上不同的相中，并且第二不相容或反应性材料分布在第二视觉上不同的相中。 本发明还涉及使用这种多相液体洗涤剂组合物清洁餐具的方法。
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7.发明授权Water-soluble film having improved dissolution and stress properties, and packets made therefrom 有权具有改善的溶解和应力性质的水溶性薄膜和由其制成的包装公开(公告)号：US08905236B2
公开(公告)日：2014-12-09
申请号：US13016621
申请日：2011-01-28
申请人： Frank W. Denome , Steven G. Friedrich , Regine Labeque , David M. Lee , Roxane Rosmaninho , Jichun Shi , Andrew P. Verrall
发明人： Frank W. Denome , Steven G. Friedrich , Regine Labeque , David M. Lee , Roxane Rosmaninho , Jichun Shi , Andrew P. Verrall
CPC分类号： C08L29/04 , B65D65/46 , C08J5/18 , C08J2329/04 , C08L2203/16 , C08L2205/025 , C11D17/042 , C11D17/045 , Y10T428/1334 , Y10T428/1341 , Y10T428/1345
摘要： Disclosed is a pouch having at least one sealed compartment containing a first composition. At least one wall of the at least one sealed compartment is made from a water-soluble film having any suitable thickness. The water-soluble film comprises PVOH polymer such that when the film has a thickness of about 76 microns the film is characterized by a Dissolution Index of about 620 to about 920, or of about 665 to about 920, or about 710 to about 920; and a Stress Index of about 145 to about 626, or about 155 to about 480, or about 165 to about 325.
摘要翻译： 公开了一种具有至少一个包含第一组合物的密封隔室的袋。 至少一个密封隔室的至少一个壁由具有任何合适厚度的水溶性薄膜制成。 该水溶性膜包含PVOH聚合物，使得当该膜的厚度为约76微米时，该膜的特征在于溶解指数为约620至约920，或约665至约920，或约710至约920; 和约145至约626，或约155至约480，或约165至约325的应力指数。
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公开(公告)号：US20130029894A1
公开(公告)日：2013-01-31
申请号：US13548300
申请日：2012-07-13
申请人： Jean-Luc Philippe Bettiol , Katrien Decraene , Marc Francois Theophile Evers , Karl Ghislain Braeckman , Bjorn Van Overstraete , Robby Renilde Francoise Keuleers , Joanna Margaret Clarke , Roxane Rosmaninho , Raffaele Pinna , Christopher Stephen Jones
发明人： Jean-Luc Philippe Bettiol , Katrien Decraene , Marc Francois Theophile Evers , Karl Ghislain Braeckman , Bjorn Van Overstraete , Robby Renilde Francoise Keuleers , Joanna Margaret Clarke , Roxane Rosmaninho , Raffaele Pinna , Christopher Stephen Jones
IPC分类号： C11D17/00
CPC分类号： C11D11/0023 , C11D3/1253 , C11D3/1266 , C11D3/2086 , C11D3/2093 , C11D3/222 , C11D3/37 , C11D17/0017
摘要： The invention relates to a multiphase liquid detergent composition comprising at least two visually distinct liquid phases and a surfactant. At least one of the visually distinct phases has a high shear viscosity between about 100 cps and 15,000 cps at 20° C., a medium shear viscosity between about 5,000 cps and about 60,000 at 20° C., and a low shear viscosity between about 10,000 cps and 500,000 cps at 20° C. The present invention further relates to methods of cleaning dishware using such multiphase liquid detergent compositions.
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9.发明授权Water-soluble film having improved dissolution and stress properties, and packets made therefrom 有权具有改善的溶解和应力性质的水溶性薄膜和由其制成的包装公开(公告)号：US08276756B2
公开(公告)日：2012-10-02
申请号：US13017382
申请日：2011-01-31
申请人： Frank William Denome , Steven G. Friedrich , Regine Labeque , David M Lee , Jichun Shi , Andrew P. Verrall , Roxane Rosmaninho
发明人： Frank William Denome , Steven G. Friedrich , Regine Labeque , David M Lee , Jichun Shi , Andrew P. Verrall , Roxane Rosmaninho
IPC分类号： B65D85/84
CPC分类号： C08L29/04 , B65D65/46 , C08J5/18 , C08J2329/04 , C08L2203/16 , C08L2205/025 , C11D17/042 , C11D17/045 , Y10T428/1334 , Y10T428/1341 , Y10T428/1345
摘要： Disclosed is a pouch having at least one sealed compartment containing a first composition. At least one wall of the at least one sealed compartment is made from a water-soluble film having any suitable thickness. The water-soluble film comprises PVOH polymer such that when the film has a thickness of about 76 microns the film is characterized by a Dissolution Index of about 620 to about 920, or of about 665 to about 920, or about 710 to about 920; and a Stress Index of about 145 to about 626, or about 155 to about 480, or about 165 to about 325.
摘要翻译： 公开了一种具有至少一个包含第一组合物的密封隔室的袋。 至少一个密封隔室的至少一个壁由具有任何合适厚度的水溶性薄膜制成。 该水溶性膜包含PVOH聚合物，使得当该膜的厚度为约76微米时，该膜的特征在于溶解指数为约620至约920，或约665至约920，或约710至约920; 和约145至约626，或约155至约480，或约165至约325的应力指数。
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公开(公告)号：US20110188784A1
公开(公告)日：2011-08-04
申请号：US13017437
申请日：2011-01-31
申请人： Frank William DENOME , Steven G. Friedrich , Regine Labeque , David M. Lee , Jichun Shi , Andrew P. Verrall , Roxane Rosmaninho
发明人： Frank William DENOME , Steven G. Friedrich , Regine Labeque , David M. Lee , Jichun Shi , Andrew P. Verrall , Roxane Rosmaninho
CPC分类号： C08L29/04 , B65D65/46 , C08J5/18 , C08J2329/04 , C08L2203/16 , C08L2205/025 , C11D17/042 , C11D17/045 , Y10T428/1334 , Y10T428/1341 , Y10T428/1345
摘要： Disclosed are plasticized, water-soluble films having favorable cold-water solubility, wet handling, and thermoforming characteristics, and which can include a PVOH resin made up of blend of two or more PVOH polymers each having a monomodal molecular weight distribution, and the PVOH resin characterized by a viscosity in a range of about 13.5 cP to about 20 cP (or a corresponding weight average molecular weight), a degree of hydrolysis of about 84% to about 92%, a polydispersity index value in a range of about 1 to about 5, a residual water content of about 4 wt. % to about 10 wt. %, and a Resin Selection Index value in a range of 0.255 to 0.315; methods of making the films; compositions including PVOH resins for making the films; and pouch and packet articles made from the films.
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