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公开(公告)号：US08104309B2
公开(公告)日：2012-01-31
申请号：US11961515
申请日：2007-12-20
申请人： Manfred Borens , Franz-Peter Eckes , Janus Zborowski , Karsten V. Westernhagen , Stefano Merolla , Joerg Witte , Joachim Kuester , Marcus Holla
发明人： Manfred Borens , Franz-Peter Eckes , Janus Zborowski , Karsten V. Westernhagen , Stefano Merolla , Joerg Witte , Joachim Kuester , Marcus Holla
CPC分类号： C03C3/06 , B28B1/16 , B28B1/265 , B28B23/0006 , C03B19/06 , C03B19/066 , C03B20/00 , C30B11/002 , C30B35/002 , H01L31/1804 , Y02P70/521
摘要： The method provides an improved quartz glass body, especially an improved quartz glass crucible for melting non-metals, non-ferrous metals, or silicon. The quartz glass body is made by a method in which a quartz glass-water mixture is supplied to a gypsum casting mold comprising an outer part and an inner part, dried in the gypsum mold, and put under an overpressure via a system of ducts in the form of textile tubes embedded in the mold during the drying. Later a resulting green glass body is removed from the mold. At least a portion of the shaping surfaces of the inner part of the gypsum mold are surfaces of a water-impermeable substance. The method provides a cast body with a reduced tendency to crack and with a smaller open porosity.
摘要翻译： 该方法提供了改进的石英玻璃体，特别是用于熔化非金属，有色金属或硅的改进的石英玻璃坩埚。 石英玻璃体通过将石英玻璃 - 水混合物供给到包括外部部分和内部的石膏铸造模具的方法制成，在石膏模具中干燥，并通过管道系统在超压下 在干燥期间嵌入模具中的纺织管的形式。 然后将得到的绿色玻璃体从模具中取出。 石膏模具的内部的至少一部分成形表面是不透水物质的表面。 该方法提供具有降低的裂纹倾向和较小开孔度的铸体。
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公开(公告)号：US20080176054A1
公开(公告)日：2008-07-24
申请号：US12018146
申请日：2008-01-22
CPC分类号： C03C3/06 , B32B18/00 , B32B37/06 , C03C4/20 , C03C17/02 , C03C27/06 , C04B14/06 , C04B14/22 , C04B35/14 , C04B35/64 , C04B37/005 , C04B2111/0025 , C04B2235/6027 , C04B2235/76 , C04B2235/77 , C04B2235/783 , C04B2235/95 , C04B2237/062 , C04B2237/341 , Y10T156/10 , Y10T428/249921 , Y10T428/249953 , Y10T428/249981 , Y10T428/26 , Y10T428/31504
摘要： To provide a material for use at high temperatures of several 100° C. which is simple and quick to produce, the invention provides a composite having a layer structure and a process for producing it, which comprises the following steps: a) provision of at least two plates which each have at least one main area of extension, b) stacking of the plates in such a way that a main area of extension of one plate is essentially opposite a main area of extension of the subsequent plate in the stack, c) joining of the stacked plates to form a block using a sinterable composition, d) carrying out a heat treatment on the block so that at least sintering of the sinterable composition occurs and a strong composite body is formed from the block.
摘要翻译： 为了提供在几个100℃的高温下使用的材料，其简单且快速地生产，本发明提供了具有层结构和其制备方法的复合材料，其包括以下步骤：a） 至少两个板，它们各自具有至少一个主要的延伸区域，b）板的堆叠，使得一个板的主要延伸区域基本上与堆叠中随后的板的延伸的主要区域相对，c ）接合堆叠板以形成使用可烧结组合物的块，d）对块进行热处理，使得至少烧结可烧结组合物，并从块形成强复合体。
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3.发明授权Sintering of fused silica to produce shaped bodies comprising crystalline SiO2 有权熔融二氧化硅的烧结以产生包含结晶SiO 2的成形体公开(公告)号：US08863552B2
公开(公告)日：2014-10-21
申请号：US12014618
申请日：2008-01-15
IPC分类号： C03B19/01 , C03B19/02 , C03B19/06 , C04B35/14 , C04B35/626 , C03B20/00 , C03C3/06 , B82Y5/00 , C03B5/43
CPC分类号： C03C3/06 , B82Y5/00 , C03B5/43 , C03B19/06 , C03B19/066 , C03B20/00 , C04B35/14 , C04B35/62665 , C04B2235/5427 , C04B2235/5472 , C04B2235/6027 , C04B2235/6028 , C04B2235/656 , C04B2235/6562 , C04B2235/6565 , C04B2235/72 , C04B2235/77 , C04B2235/95 , C04B2235/96 , C04B2235/9607 , Y10T428/131 , Y10T428/1317
摘要： A process is disclosed for simple and rapid production of a shaped body comprising fused silica and a shaped body which leads to virtually no contamination of a melt in contact with the shaped body even at high temperatures. The disclosed process comprises the steps of: a) provision of fused silica in the form of essentially amorphous SiO2 grains of which not more than 5% have a diameter greater than 15 mm, b) addition of water to the fused silica grains to produce a slip, c) casting of the slip into a mold which comprises a hollow body having the inverse shape of the shaped body to be produced, and d) drying of the slip to give an intermediate body, which is then sintered and cooled. A shaped body producible in accordance with the aforementioned process is also disclosed, which comprises at least 99.0 mol % of SiO2.
摘要翻译： 公开了一种简单快速地生产包括熔融二氧化硅和成型体的成形体的方法，即使在高温下也能使与熔体接触的熔体几乎没有污染。 所公开的方法包括以下步骤：a）提供基本无定形SiO 2颗粒形式的熔融二氧化硅，其中不超过5％的直径大于15mm，b）向熔融二氧化硅颗粒中加入水以产生 滑动，c）将滑动件浇铸到模具中，该模具包括具有待制造的成形体的相反形状的中空体，以及d）干燥滑动件，得到中间体，然后烧结并冷却。 还公开了根据上述方法可生产的成形体，其包含至少99.0mol％的SiO 2。
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公开(公告)号：US08999091B2
公开(公告)日：2015-04-07
申请号：US12018146
申请日：2008-01-22
IPC分类号： C03C3/06 , C03C4/20 , C03C17/02 , C03C27/06 , C04B37/00 , C04B111/00 , C04B14/06 , C04B14/22 , C04B35/14 , C04B35/64 , B32B18/00 , B32B37/06
CPC分类号： C03C3/06 , B32B18/00 , B32B37/06 , C03C4/20 , C03C17/02 , C03C27/06 , C04B14/06 , C04B14/22 , C04B35/14 , C04B35/64 , C04B37/005 , C04B2111/0025 , C04B2235/6027 , C04B2235/76 , C04B2235/77 , C04B2235/783 , C04B2235/95 , C04B2237/062 , C04B2237/341 , Y10T156/10 , Y10T428/249921 , Y10T428/249953 , Y10T428/249981 , Y10T428/26 , Y10T428/31504
摘要： To provide a material for use at high temperatures of several 100° C. which is simple and quick to produce, the invention provides a composite having a layer structure and a process for producing it, which comprises the following steps: a) provision of at least two plates which each have at least one main area of extension, b) stacking of the plates in such a way that a main area of extension of one plate is essentially opposite a main area of extension of the subsequent plate in the stack, c) joining of the stacked plates to form a block using a sinterable composition, d) carrying out a heat treatment on the block so that at least sintering of the sinterable composition occurs and a strong composite body is formed from the block.
摘要翻译： 为了提供在几个100℃的高温下使用的材料，其简单且快速地生产，本发明提供了具有层结构和其制备方法的复合材料，其包括以下步骤：a） 至少两个板，它们各自具有至少一个主要的延伸区域，b）板的堆叠，使得一个板的主要延伸区域基本上与堆叠中随后的板的延伸的主要区域相对，c ）接合堆叠板以形成使用可烧结组合物的块，d）对块进行热处理，使得至少烧结可烧结组合物，并从块形成强复合体。
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5.发明申请Sintering of fused silica to produce shaped bodies comprising crystalline SiO2 有权熔融二氧化硅的烧结以产生包含结晶SiO 2的成形体公开(公告)号：US20080196448A1
公开(公告)日：2008-08-21
申请号：US12014618
申请日：2008-01-15
CPC分类号： C03C3/06 , B82Y5/00 , C03B5/43 , C03B19/06 , C03B19/066 , C03B20/00 , C04B35/14 , C04B35/62665 , C04B2235/5427 , C04B2235/5472 , C04B2235/6027 , C04B2235/6028 , C04B2235/656 , C04B2235/6562 , C04B2235/6565 , C04B2235/72 , C04B2235/77 , C04B2235/95 , C04B2235/96 , C04B2235/9607 , Y10T428/131 , Y10T428/1317
摘要： For simple and rapid production of a shaped body comprising fused silica and a shaped body which leads to virtually no contamination of a melt in contact with the shaped body even at high temperatures, the invention provides a process comprising the steps: a) provision of fused silica in the form of essentially amorphous SiO2 grains of which not more than 5% have a diameter greater than 15 mm, b) addition of water to the fused silica grains to produce a slip, c) casting of the slip into a mould which comprises a hollow body having the inverse shape of the shaped body to be produced, d) drying of the slip to give an intermediate body, e) sintering of the intermediate body at a sintering temperature at which at least part of the fused silica is transformed from the amorphous modification into a crystalline modification, f) cooling of the sintered shaped body to a temperature below 300° C., so that a microstructure containing crystalline SiO2 is formed, and also a shaped body which comprises at least 99.0 mol % of SiO2.
摘要翻译： 为了简单且快速地生产包括熔融二氧化硅和成形体的成形体，即使在高温下也几乎不导致与成形体接触的熔体的污染，本发明提供了一种方法，包括以下步骤：a） 基本上无定形的SiO 2颗粒形式的二氧化硅，其中不超过5％的直径大于15mm，b）向熔融二氧化硅颗粒中加入水以产生滑动，c）铸造 滑入模具中，其包括具有待制造的成形体的相反形状的中空体，d）干燥滑移以产生中间体，e）在至少在烧结温度下烧结中间体 熔融二氧化硅的一部分从无定形改性物转化为结晶改性，f）将烧结成形体冷却至低于300℃的温度，从而形成含有结晶SiO 2的微结构 ，还有 包含至少99.0mol％的SiO 2的成形体。
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公开(公告)号：US20080153688A1
公开(公告)日：2008-06-26
申请号：US11961515
申请日：2007-12-20
申请人： Manfred Borens , Franz-Peter Eckes , Janus Zborowski , Karsten V. Westernhagen , Stefano Merolla , Joerg Witte , Joachim Kuester , Marcus Holla
发明人： Manfred Borens , Franz-Peter Eckes , Janus Zborowski , Karsten V. Westernhagen , Stefano Merolla , Joerg Witte , Joachim Kuester , Marcus Holla
IPC分类号： C03C3/06
CPC分类号： C03C3/06 , B28B1/16 , B28B1/265 , B28B23/0006 , C03B19/06 , C03B19/066 , C03B20/00 , C30B11/002 , C30B35/002 , H01L31/1804 , Y02P70/521
摘要： The invention includes an improved quartz glass body, especially an improved quartz glass crucible for melting non-metals, non-ferrous metals, or silicon, and a method and casting mold for making it The quartz glass body is made by a method in which a quartz glass-water mixture is supplied to a casting mold comprising an outer part and an inner part, dried in the mold, and put under an overpressure during the drying. Later a resulting green glass body is removed from the mold. At least a portion of the shaping surfaces of the inner part of the mold are surfaces of a water-impermeable substance. The method provides a cast body with a reduced tendency to crack and with a smaller open porosity.
摘要翻译： 本发明包括改进的石英玻璃体，特别是用于熔化非金属，有色金属或硅的改进的石英玻璃坩埚，以及用于制造石英玻璃体的方法和铸模。石英玻璃体通过以下方法制成： 将石英玻璃 - 水混合物供给到包括外部部分和内部的铸模，在模具中干燥，并在干燥期间处于过压状态。 然后将得到的绿色玻璃体从模具中取出。 模具内部的至少一部分成形表面是不透水物质的表面。 该方法提供具有降低的裂纹倾向和较小开孔度的铸体。
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