公开(公告)号：US20050136350A1

公开(公告)日：2005-06-23

申请号：US10744791

申请日：2003-12-23

申请人： Vincenzo Marcello ,  David Kurceba ,  Nancy Hunt ,  Cheih-Min Cheng ,  Tie Ng

发明人： Vincenzo Marcello ,  David Kurceba ,  Nancy Hunt ,  Cheih-Min Cheng ,  Tie Ng

IPC分类号： B01F3/12 ,  G03G9/00 ,  G03G9/08 ,  G03G9/087

CPC分类号： G03G9/0804

摘要： Disclosed is an oil-less toner composition exhibiting good low temperature release and stripping in fixing, enhanced surface gloss of fixed image, and/or OHP transparency. By controlling one or more properties, such as the relative thermal energy input during the EA aggregation/coalescence process, using a wax having a certain dispersion size (D50), molecular weight and/or melting temperature, the toner particle produced thereby can achieve optimal surface wax protrusion with a surface wax content of about 12 to about 25 weight percent. This is based on the total amount of wax in the toner, as determined by x-ray photoelectron spectroscopy (XPS). The contamination of wax on developing rolls, photoreceptor and carriers, which lowers the reliability of the developer, is suppressed with the present exemplary embodiment.

摘要翻译： 公开了一种无油调色剂组合物，其在定影中表现出良好的低温释放和剥离，增强固定图像的表面光泽度和/或OHP透明度。 通过控制一个或多个性能，例如在EA聚集/聚结过程期间的相对热能输入，使用具有一定分散体尺寸（D50），分子量和/或熔融温度的蜡，由此产生的调色剂颗粒可以达到最佳 表面蜡突起具有约12至约25重量％的表面蜡含量。 这是基于通过x射线光电子能谱（XPS）测定的调色剂中蜡的总量。 在本示例性实施例中，抑制了显影辊，感光体和载体上的蜡污染，这降低了显影剂的可靠性。

公开(公告)号：US20060194134A1

公开(公告)日：2006-08-31

申请号：US11396817

申请日：2006-04-03

申请人： Vincenzo Marcello ,  David Kurceba ,  Nancy Hunt ,  Cheih-Min Cheng ,  Tie Ng

发明人： Vincenzo Marcello ,  David Kurceba ,  Nancy Hunt ,  Cheih-Min Cheng ,  Tie Ng

IPC分类号： G03G9/08

CPC分类号： G03G9/0804

摘要： Disclosed is an oil-less toner composition exhibiting good low temperature release and stripping in fixing, enhanced surface gloss of fixed image, and/or OHP transparency. By controlling one or more properties, such as the relative thermal energy input during the EA aggregation/coalescence process, using a wax having a certain dispersion size (D50), molecular weight and/or melting temperature, the toner particle produced thereby can achieve optimal surface wax protrusion with a surface wax content of about 12 to about 25 weight percent. This is based on the total amount of wax in the toner, as determined by x-ray photoelectron spectroscopy (XPS). The contamination of wax on developing rolls, photoreceptor and carriers, which lowers the reliability of the developer, is suppressed with the present exemplary embodiment.

摘要翻译： 公开了一种无油调色剂组合物，其在定影中表现出良好的低温释放和剥离，增强固定图像的表面光泽度和/或OHP透明度。 通过控制一个或多个性能，例如在EA聚集/聚结过程期间的相对热能输入，使用具有一定分散体尺寸（D50），分子量和/或熔融温度的蜡，由此产生的调色剂颗粒可以达到最佳 表面蜡突起具有约12至约25重量％的表面蜡含量。 这是基于通过x射线光电子能谱（XPS）测定的调色剂中蜡的总量。 在本示例性实施例中，抑制了显影辊，感光体和载体上的蜡污染，这降低了显影剂的可靠性。

公开(公告)号：US20050136351A1

公开(公告)日：2005-06-23

申请号：US10743096

申请日：2003-12-23

申请人： Judith Vandewinckel ,  Vincenzo Marcello ,  Grazyna Kmiecik-Lawrynowicz ,  Tie Ng ,  Chieh-Min Cheng

发明人： Judith Vandewinckel ,  Vincenzo Marcello ,  Grazyna Kmiecik-Lawrynowicz ,  Tie Ng ,  Chieh-Min Cheng

IPC分类号： G03G9/08 ,  G03G9/087 ,  G03G9/09 ,  G03G9/097

CPC分类号： G03G9/08708 ,  G03G9/0806 ,  G03G9/0819 ,  G03G9/0827 ,  G03G9/08711 ,  G03G9/08782 ,  G03G9/09708

摘要： A toner of the invention includes toner particles comprising a styrene acrylate binder and at least one colorant, and wherein the toner particles, in the absence of external additives, have a mean circularity of from about 0.94 to about 0.98 and a particle size distribution with a lower number ratio geometric standard deviation (GSD) of approximately 1.28 to approximately 1.31 and an upper volume GSD of approximately 1.24 to approximately 1.27. Also included is a set of toners for forming a color image, comprising a cyan toner, a magenta toner, a yellow toner and a black toner, wherein each of the cyan toner, the magenta toner, the yellow toner and the black toner, wherein each of about 70 to about 95% by weight, dry basis, of a styrene acrylate binder, about 5 to about 15% by weight, dry basis, of a wax dispersion, and at least one colorant.

摘要翻译： 本发明的调色剂包括包含苯乙烯丙烯酸酯粘合剂和至少一种着色剂的调色剂颗粒，并且其中调色剂颗粒在没有外部添加剂的情况下具有约0.94至约0.98的平均圆形度，并且具有 约1.28至约1.31的较低数值比几何标准偏差（GSD）和约1.24至约1.27的上部体积GSD。 还包括用于形成彩色图像的一组调色剂，包括青色调色剂，品红色调色剂，黄色调色剂和黑色调色剂，其中每个青色调色剂，品红色调色剂，黄色调色剂和黑色调色剂，其中 约70至约95重量％，基于干燥的苯乙烯丙烯酸酯粘合剂，约5至约15重量％，干基，蜡分散体和至少一种着色剂。

公开(公告)号：US20080107988A1

公开(公告)日：2008-05-08

申请号：US11937244

申请日：2007-11-08

申请人： Judith VANDEWINCKEL ,  Vincenzo MARCELLO ,  Grazyna KMIECIK-LAWRYNOWICZ ,  Tie NG ,  Chieh-Min CHENG

发明人： Judith VANDEWINCKEL ,  Vincenzo MARCELLO ,  Grazyna KMIECIK-LAWRYNOWICZ ,  Tie NG ,  Chieh-Min CHENG

IPC分类号： G03G9/087

CPC分类号： G03G9/08795 ,  G03G9/0806 ,  G03G9/0819 ,  G03G9/0821 ,  G03G9/08708 ,  G03G9/08711 ,  G03G9/08793 ,  G03G9/08797 ,  G03G9/09708 ,  G03G9/09791

摘要： A toner including toner particles of a styrene acrylate binder and at least one colorant, wherein the styrene acrylate binder has a weight average molecular weight of about 20 to about 30 kpse and a molecular peak of about 23 to about 28 kpse, the toner particles have a weight average molecular weight of about 28 to about 130 kpse, a number average molecular weight of about 9 to about 13.4 and a MWD of about 2.2 to about 10, and the toner particles have a cohesion of about 55 to about 98% at a mean circularity of about 0.94 to about 0.98. Also included is a set of toners for forming a color image, comprising a cyan toner, a magenta toner, a yellow toner and a black toner, wherein each of they cyan toner, the magenta toner, the yellow toner and the black toner have toner particles of about 70 to about 95% by weight, solids basis, of a styrene acrylate binder, about 5 to about 15% by weight, solids basis, of a wax dispersion, and at least one colorant.

摘要翻译： 一种调色剂，包括苯乙烯丙烯酸酯粘合剂和至少一种着色剂的调色剂颗粒，其中苯乙烯丙烯酸酯粘合剂的重均分子量为约20至约30kpse，分子峰为约23至约28kpse，调色剂颗粒具有 约28至约130kpse的重均分子量，约9至约13.4的数均分子量和约2.2至约10的MWD，并且调色剂颗粒的粘度为约55至约98％ 平均圆形度为约0.94至约0.98。 还包括用于形成彩色图像的一组调色剂，包括青色调色剂，品红色调色剂，黄色调色剂和黑色调色剂，其中它们中的青色调色剂，品红色调色剂，黄色调色剂和黑色调色剂均具有调色剂 约70至约95重量％，基于固体的苯乙烯丙烯酸酯粘合剂，约5至约15重量％的基于固体的蜡分散体和至少一种着色剂的颗粒。

公开(公告)号：US07217484B2

公开(公告)日：2007-05-15

申请号：US11396817

申请日：2006-04-03

申请人： Vincenzo Marcello ,  David Kurceba ,  Nancy Hunt ,  Cheih-Min Cheng ,  Tie Hwee Ng

发明人： Vincenzo Marcello ,  David Kurceba ,  Nancy Hunt ,  Cheih-Min Cheng ,  Tie Hwee Ng

IPC分类号： G03G9/08

CPC分类号： G03G9/0804

摘要： Disclosed is an oil-less toner composition exhibiting good low temperature release and stripping in fixing, enhanced surface gloss of fixed image, and/or OHP transparency. By controlling one or more properties, such as the relative thermal energy input during the EA aggregation/coalescence process, using a wax having a certain dispersion size (D50), molecular weight and/or melting temperature, the toner particle produced thereby can achieve optimal surface wax protrusion with a surface wax content of about 12 to about 25 weight percent. This is based on the total amount of wax in the toner, as determined by x-ray photoelectron spectroscopy (XPS). The contamination of wax on developing rolls, photoreceptor and carriers, which lowers the reliability of the developer, is suppressed with the present exemplary embodiment.

摘要翻译： 公开了一种无油调色剂组合物，其在定影中表现出良好的低温释放和剥离，增强固定图像的表面光泽度和/或OHP透明度。 通过控制一个或多个性能，例如在EA聚集/聚结过程期间的相对热能输入，使用具有一定分散体尺寸（D50），分子量和/或熔融温度的蜡，由此产生的调色剂颗粒可以达到最佳 表面蜡突起具有约12至约25重量％的表面蜡含量。 这是基于通过x射线光电子能谱（XPS）测定的调色剂中蜡的总量。 在本示例性实施例中，抑制了显影辊，感光体和载体上的蜡污染，这降低了显影剂的可靠性。

公开(公告)号：US07052818B2

公开(公告)日：2006-05-30

申请号：US10744791

申请日：2003-12-23

申请人： Vincenzo Marcello ,  David Kurceba ,  Nancy Hunt ,  Cheih-Min Cheng ,  Tie Hwee Ng

发明人： Vincenzo Marcello ,  David Kurceba ,  Nancy Hunt ,  Cheih-Min Cheng ,  Tie Hwee Ng

IPC分类号： G03G9/00 ,  B01F3/12

CPC分类号： G03G9/0804

摘要： Disclosed is an oil-less toner composition exhibiting good low temperature release and stripping in fixing, enhanced surface gloss of fixed image, and/or OHP transparency. By controlling one or more properties, such as the relative thermal energy input during the EA aggregation/coalescence process, using a wax having a certain dispersion size (D50), molecular weight and/or melting temperature, the toner particle produced thereby can achieve optimal surface wax protrusion with a surface wax content of about 12 to about 25 weight percent. This is based on the total amount of wax in the toner, as determined by x-ray photoelectron spectroscopy (XPS). The contamination of wax on developing rolls, photoreceptor and carriers, which lowers the reliability of the developer, is suppressed with the present exemplary embodiment.

公开(公告)号：US20070020553A1

公开(公告)日：2007-01-25

申请号：US11187030

申请日：2005-07-22

申请人： Vincenzo Marcello ,  Steven Malachowski ,  Tie Ng ,  Chieh-Min Cheng

发明人： Vincenzo Marcello ,  Steven Malachowski ,  Tie Ng ,  Chieh-Min Cheng

IPC分类号： G03G9/08

CPC分类号： C08F6/18 ,  C08F6/22 ,  G03G9/0804 ,  G03G9/0815 ,  G03G9/0817

摘要： A method of making toner particles, includes: mixing a latex emulsion, a colorant emulsion an optional was emulsion, and optional additives in a first reactor to form a slurry; discharging the slurry from the first reactor to a second reactor through a homogenizer; heating the slurry in the second reactor to form aggregated particles in said slurry; discharging the aggregated particles and slurry from the second reactor to a third reactor; heating the aggregated particles and slurry in the third reactor to coalesce the aggregated particles into toner particles; discharging the toner particles and slurry from the third reactor to a fourth reactor; cooling the toner particles; optionally classifying said toner particles to remove coarse particles; and optionally washing and drying said toner particles, wherein the first reactor, second reactor, third reactor, and fourth reactor are at least two different reactors.

摘要翻译： 制备调色剂颗粒的方法包括：在第一反应器中混合胶乳乳液，着色剂乳液，任选的是乳液和任选的添加剂以形成浆料; 通过均化器将浆料从第一反应器排出到第二反应器; 加热第二反应器中的浆料以在所述浆料中形成凝集颗粒; 将凝集的颗粒和浆料从第二反应器排出到第三反应器; 加热第三反应器中的聚集颗粒和浆料以将聚集的颗粒聚结成调色剂颗粒; 将调色剂颗粒和浆料从第三反应器排出到第四反应器; 冷却调色剂颗粒; 任选分级所述调色剂颗粒以除去粗颗粒; 以及任选地洗涤和干燥所述调色剂颗粒，其中第一反应器，第二反应器，第三反应器和第四反应器是至少两个不同的反应器。

公开(公告)号：US20050136352A1

公开(公告)日：2005-06-23

申请号：US10743097

申请日：2003-12-23

申请人： Judith Vandewinckel ,  Vincenzo Marcello ,  Grazyna Kmiecik-Lawrynowicz ,  Tie Ng ,  Chieh-Min Cheng

发明人： Judith Vandewinckel ,  Vincenzo Marcello ,  Grazyna Kmiecik-Lawrynowicz ,  Tie Ng ,  Chieh-Min Cheng

IPC分类号： G03G9/08 ,  G03G9/087 ,  G03G9/09 ,  G03G9/097

CPC分类号： G03G9/08795 ,  G03G9/0806 ,  G03G9/0819 ,  G03G9/0821 ,  G03G9/08708 ,  G03G9/08711 ,  G03G9/08793 ,  G03G9/08797 ,  G03G9/09708 ,  G03G9/09791

摘要： A toner including toner particles of a styrene acrylate binder and at least one colorant, wherein the styrene acrylate binder has a weight average molecular weight of about 20 to about 30 kpse and a molecular peak of about 23 to about 28 kpse, the toner particles have a weight average molecular weight of about 28 to about 130 kpse, a number average molecular weight to about 9 to about 13.4 and a MWD of about 2.2 to about 10, and the toner particles have a cohesion of about 55 to about 98% at a mean circularity of about 0.94 to about 0.98. Also included is a set of toners for forming a color image, comprising a cyan toner, a magenta toner, a yellow toner and a black toner, wherein each of the cyan toner, the magenta toner, the yellow toner and the black toner have toner particles of about 70 to about 95% by weight, solids basis, of a styrene acrylate binder, about 5 to about 15% by weight, solids basis, of a wax dispersion, and at least one colorant.

摘要翻译： 一种调色剂，包括苯乙烯丙烯酸酯粘合剂和至少一种着色剂的调色剂颗粒，其中苯乙烯丙烯酸酯粘合剂的重均分子量为约20至约30kpse，分子峰为约23至约28kpse，调色剂颗粒具有 约28至约130kpse的重均分子量，数均分子量至约9至约13.4，MWD为约2.2至约10，并且调色剂颗粒的粘度为约55至约98％ 平均圆形度为约0.94至约0.98。 还包括用于形成彩色图像的一组调色剂，包括青色调色剂，品红色调色剂，黄色调色剂和黑色调色剂，其中每个青色调色剂，品红色调色剂，黄色调色剂和黑色调色剂都具有调色剂 约70至约95重量％，基于固体的苯乙烯丙烯酸酯粘合剂，约5至约15重量％的基于固体的蜡分散体和至少一种着色剂的颗粒。