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    Transforming crude copper phthalocyanines into a pigmentary state
    1.
    发明授权
    Transforming crude copper phthalocyanines into a pigmentary state 失效
    将粗铜酞菁转变为颜料状态

    公开(公告)号：US5006173A

    公开(公告)日：1991-04-09

    申请号：US370727

    申请日：1989-06-23

    申请人： Wolfgang Fath ,  Rainer Nachtrab ,  Rudolf Polster

    发明人： Wolfgang Fath ,  Rainer Nachtrab ,  Rudolf Polster

    IPC分类号： C09B67/12 ,  C09B67/20

    CPC分类号： C09B67/0016

    摘要： Crude copper phthalocyanines are transformed into a pigmentary state by treating finely divided but imperfectly crystallized and highly aggregated crude copper phthalocyanines having a primary particle size, produced by ball milling, or less than 0.1 .mu.m with an organic solvent by subjecting a suspension of the organic solvent and the milled crude copper phthalocyanine (hereinafter referred to as the solvent/pigment suspension), which has a pigment concentration of from 15 to 55% by weight and a solvent concentration of from 15 to 85% by weight and which may contain water in a concentration of from 0 to 30% by weight, to a shear gradient of from 1000 to 20000 s.sup.-1 for a period of from 2 to 1000 s with an energy uptake during shearing of from 0.01 to 0.02 kWh/kg of pigment throughput, then metering water into the solvent/pigment suspension in an amount of from 0.1 to 10 times the amount of the solvent, to effect a defined discontinuation of the conditioning process, and finally mixing the suspension until homogeneous.

    摘要翻译： 粗铜酞菁通过用有机溶剂处理细分但不完全结晶的高度聚集的粗铜酞菁，其具有初级粒度，通过球磨或小于0.1μm，通过使有机溶剂的悬浮液进行处理而转化为颜料状态 溶剂和研磨的粗铜酞菁（以下称为溶剂/颜料悬浮液），其颜料浓度为15至55重量％，溶剂浓度为15至85重量％，并且可以含有水 浓度为0至30重量％，剪切梯度为1000至20000秒-1，时间为2至1000秒，剪切时的能量摄取为0.01至0.02千瓦时/千克的颜料生产量， 然后将溶剂/颜料悬浮液中的水量定量为溶剂量的0.1至10倍，以实现定义的中止调理过程，最后混合t 他暂停直到均匀。

    Production of fibers by centrifugal spinning
    2.
    发明授权
    Production of fibers by centrifugal spinning 失效
    通过离心纺生产纤维

    公开(公告)号：US5494616A

    公开(公告)日：1996-02-27

    申请号：US239311

    申请日：1994-05-06

    申请人： Heinz Voelker ,  Hans D. Zettler ,  Wolfgang Fath ,  Heinz Berbner

    发明人： Heinz Voelker ,  Hans D. Zettler ,  Wolfgang Fath ,  Heinz Berbner

    IPC分类号： D01D5/08 ,  C08G14/10 ,  D01D5/18 ,  D01F6/76

    CPC分类号： C08G14/10 ,  D01D5/18

    摘要： A process for producing fibers by spinning a resin by a centrifugal spinning process comprises supplying a resin solution having a viscosity from 50 to 200 Pa.s at the spinning temperature to a whirler plate and ensuring that the resin solution is under a sufficient pressure to completely fill the nozzles of the whirler plate as the fibers are being spun. The process is particularly suitable for producing fibers based on amino resins. In the apparatus the supply line for the resin is preferably located within the driveshaft.

    摘要翻译： 通过离心纺丝法纺出树脂来制造纤维的方法包括在旋转温度下将粘度为50-200Pa.s的树脂溶液供给到旋转板，并确保树脂溶液处于足够的压力下完全 当纤维正在旋转时，填充旋转板的喷嘴。 该方法特别适用于生产基于氨基树脂的纤维。 在该设备中，用于树脂的供应线优选位于驱动轴内。

    Modified melamine-formaldehyde resins
    3.
    发明授权
    Modified melamine-formaldehyde resins 失效
    改性三聚氰胺 - 甲醛树脂

    公开(公告)号：US5322915A

    公开(公告)日：1994-06-21

    申请号：US910382

    申请日：1992-07-08

    申请人： Juergen Weiser ,  Wolfgang Reuther ,  Rolf Fikentscher ,  Wolfgang Fath ,  Heinz Berbner ,  Hans D. Zettler ,  Heinz Voelker

    发明人： Juergen Weiser ,  Wolfgang Reuther ,  Rolf Fikentscher ,  Wolfgang Fath ,  Heinz Berbner ,  Hans D. Zettler ,  Heinz Voelker

    IPC分类号： C08G14/09 ,  C08G14/06 ,  C08G14/10

    CPC分类号： C08G14/10

    摘要： A condensation polymer, obtainable by condensation of a mixture containing, as chief components,(A) from 90 to 99.9% molar of a mixture substantially consisting of(a) from 30 to 99% molar of melamine and(b) from 1 to 70% molar of a substituted melamine of the general formula I ##STR1## in which X, X', and X" are selected from the group consisting of --NH.sub.2, --NHR, and --NRR', and only one or two of X, X', and X" denote(s) --NH.sub.2, and R and R' are selected from the group consisting of hydroxy-C.sub.2 -C.sub.10 -alkyl, hydroxy-C.sub.2 -C.sub.4 -alkyl-(oxa-C.sub.2 -C.sub.4 -alkyl).sub.n, where n is an integer from 1 to 5, and amino-C.sub.2 -C.sub.12 -alkyl, or mixtures of melamines I, and(B) from 0.1 to 10% molar, based on (A) and (B), of unsubstituted phenols or phenols substituted by radicals selected from the group consisting of C.sub.1 -C.sub.9 -alkyl and hydroxy, or of C.sub.1 -C.sub.4 -alkanes substituted by two or three phenol groups, di(hydroxyphenyl)sulfones, or mixtures of said phenols,with formaldehyde or formaldehyde-liberating compounds, the molar ratio of melamine to formaldehyde ranging from 1:1.15 to 1:4.5.

    摘要翻译： 缩合聚合物，其可通过以主要组分（A）为90至99.9％摩尔的混合物缩合获得，该混合物基本上由（a）30至99％摩尔的三聚氰胺和（b）1至70 ％摩尔的通式I的取代三聚氰胺（I）其中X，X'和X“选自-NH 2，-NHR和-NRR'，并且只有一个或 X，X'和X“中的两个表示（s）-NH 2，R和R'选自羟基-C 2 -C 10 - 烷基，羟基-C 2 - C 4 - 烷基 - （氧杂-C2 -C 1-4 - 烷基）n，其中n为1至5的整数，氨基-C 2 -C 12 - 烷基或三聚氰胺I和（B）的混合物为0.1至10摩尔％，基于（A）和（ B）的未取代的酚或被选自C 1 -C 9 - 烷基和羟基的基团或被两个或三个苯酚基取代的C 1 -C 4烷烃取代的酚，二（羟基苯基）砜或所述 酚，与甲醛或甲醛释放化合物，摩尔 三聚氰胺与甲醛的比例范围为1：1.15至1：4.5。