3,3′-Dinitro-4,4′-hydrazofurazan and methods of preparation
    1.
    发明授权
    3,3′-Dinitro-4,4′-hydrazofurazan and methods of preparation 失效
    3,3'-二硝基-4,​​4'-咔唑和其制备方法

    公开(公告)号:US06388087B1

    公开(公告)日:2002-05-14

    申请号:US09718947

    申请日:2000-11-21

    CPC classification number: C06B25/34 C07D271/08

    Abstract: The novel compound 3,3-Dinitro-4,4′-hydrozofurazan and the methods of preparation. The method of preparation 3,3-Dinitro-4,4′-hydrazofurazan which comprises partially reducing 3,3′-Dinitro-4,4′-azoxyfurazan. The method of preparing 3,3′-Dinitro-4,4′-hydrazofurazan by the partial reduction of 3,3′-Dinitro-4,4′-azofurazan.

    Abstract translation: 新型化合物3,3,3-二硝基-4,​​4'-氢唑唑烷及其制备方法。 制备3,3,3-二硝基-4,​​4'-咔唑的方法,该方法包括部分还原3,3'-二硝基-4,​​4'-氮杂氧杂呋喃。 通过部分还原3,3'-二硝基-4,​​4'-唑烷来制备3,3'-二硝基-4,​​4'-咔唑的方法。

    Nitrocubanes
    2.
    发明授权
    Nitrocubanes 失效
    硝基异氰酸酯

    公开(公告)号:US5214222A

    公开(公告)日:1993-05-25

    申请号:US955213

    申请日:1992-10-01

    CPC classification number: C07C205/10 C07C2103/90

    Abstract: An efficient direct functionalization of nitrocubanes has been achieved byrradiation of a solution in an oxalyl halide to yield halogenated and halocarbonylated derivatives of nitrocubanes.

    Abstract translation: 已经通过在草酰卤中的溶液照射产生氮化碳的卤代和卤代羰基化衍生物来实现氮代烷的有效直接官能化。

    Process for the manufacture of diaminofurazan
    3.
    发明申请
    Process for the manufacture of diaminofurazan 审中-公开
    制备二氨基呋咱的方法

    公开(公告)号:US20090137816A1

    公开(公告)日:2009-05-28

    申请号:US09738780

    申请日:2000-12-15

    CPC classification number: C07D271/08

    Abstract: This invention consists of a method for converting diaminoglyoxime to diaminofurazan that can be carried out efficiently at about atmospheric pressure without the need for high pressure containment apparatus.This invention also consists of a method which comprises converting diaminoglyoxime to diaminofurazan at about atmospheric pressure in the presence of a strong base and/or an organic polar solvent.

    Abstract translation: 本发明包括将二氨基肟转化为二氨基呋咱的方法,其可以在大气压下有效地进行而不需要高压遏制装置。 本发明还包括在强碱和/或有机极性溶剂的存在下,将二氨基肟在大气压下转化为二氨基呋咱的方法。

    Halogenated polycarboxycubanes
    4.
    发明授权
    Halogenated polycarboxycubanes 失效
    卤代多羧基乙烷

    公开(公告)号:US5378333A

    公开(公告)日:1995-01-03

    申请号:US28709

    申请日:1993-03-05

    CPC classification number: C07C69/00 C07C2103/00

    Abstract: The disclosure describes photochemical synthesis of halogenated polycarboxycubanes from simple carboxycubanes and an oxalyl halide. It is possible to synthesize 6-Chloro-1,2,4,7-tetracarbomethoxycubane and 2-Chloro-1,3,5,7-tetracarbomethoxycubane. Photochemical synthesis of halogenated polycarboxycubanes from carboxy cubane and an oxalyl halide is reported.

    Abstract translation: 本公开内容描述了由简单羧基和草酰卤衍生的卤代聚羧基烷烃的光化学合成。 可以合成6-氯-1,2,4,7-四甲基甲氧基亚烷基和2-氯-1,3,5,7-四甲基甲氧基亚烷基。 报道了羧基立方烷和草酰卤的卤代聚羧基的光化学合成。

    Conversion of trinitrotoluene into high value compounds
    6.
    发明授权
    Conversion of trinitrotoluene into high value compounds 失效
    三硝基甲苯转化为高价值化合物

    公开(公告)号:US5969155A

    公开(公告)日:1999-10-19

    申请号:US57950

    申请日:1998-04-09

    CPC classification number: C07D209/08

    Abstract: The present invention is directed to the synthesis of useful products from the explosive trinitrotoluene. This substance has a limited shelf life as a reliable explosive and large quantities of it have and will become surplus. Ecologically safe, and preferably commercially useful ways of disposing of it are therefore much to be desired. In the present invention the end products are nitroindoles of the general formula 4-Z.sup.1,6-Z.sup.2 indole wherein Z.sup.1 and Z.sup.2 are the same or different and are halo or nitro provided at least one of said groups is nitro.

    Abstract translation: 本发明涉及从爆炸性三硝基甲苯合成有用的产物。 这种物质作为可靠的爆炸物具有有限的保质期,并且大量已经并将会变得过剩。 因此,非常希望生态安全,并且优选商业上有用的处置方式。 在本发明中,最终产物是通式为4-Z1,6-Z2吲哚的硝基吲哚,其中Z1和Z2相同或不同,是卤素或硝基,其中至少一个所述基团是硝基。

    Nitrocubanes
    8.
    发明授权
    Nitrocubanes 失效
    硝基异氰酸酯

    公开(公告)号:US06222068B1

    公开(公告)日:2001-04-24

    申请号:US08228245

    申请日:1994-04-14

    CPC classification number: C07C205/55 C07C205/10 C07C2603/90

    Abstract: An efficient direct functionalization of nitrocubanes has been achieved by irradiation of a solution in an oxalyl halide to yield halogenated and halocarbonylated derivatives of nitrocubanes.

    Abstract translation: 已经通过在草酰卤中的溶液照射产生氮化碳的卤代和卤代羰基化衍生物来实现氮代烷的有效直接官能化。

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