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公开(公告)号：US5844039A
公开(公告)日：1998-12-01
申请号：US910082
申请日：1997-08-12
申请人： Alec B. Scranton , Arvind M. Mathur , John Klier
发明人： Alec B. Scranton , Arvind M. Mathur , John Klier
IPC分类号： A61K9/28 , A61K9/50 , A61K47/34 , A61L15/60 , C08F2/24 , C08F283/06 , C08F290/06 , C08F8/14
CPC分类号： C08F290/062 , A61K47/34 , A61L15/60 , C08F2/24 , C08F283/06 , A61K9/2853 , A61K9/5031
摘要： Polymers comprising reversible hydrophobic functionalities are disclosed. The preferred embodiment polymers comprise Lewis acid segments and Lewis base segments. The polymer segments are, by themselves, hydrophilic and will either swell or dissolve in water. When the segments are incorporated into a polymer according to the present invention, the segments form water-insoluble or hydrophobic complexes. Upon changes in pH, temperature or solvent type, these complexes may dissociate, giving large transitions in polymer viscosity, emulsification ability, mechanical strength or transport properties. These polymers are useful as reversible emulsifiers which form stable emulsions at acidic pH and unstable emulsions at basic pH, as water-borne thickeners having low viscosity at low pH and high viscosity at high pH, as superabsorbing resins, or as coatings for pharmaceutical or agricultural agents.
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公开(公告)号：US5739210A
公开(公告)日：1998-04-14
申请号：US695237
申请日：1996-08-08
申请人： Alec B. Scranton , Arvind M. Mathur , John Klier
发明人： Alec B. Scranton , Arvind M. Mathur , John Klier
IPC分类号： A61K9/28 , A61K9/50 , A61K47/34 , A61L15/60 , C08F2/24 , C08F283/06 , C08F290/06 , C08F8/14
CPC分类号： C08F290/062 , A61K47/34 , A61L15/60 , C08F2/24 , C08F283/06 , A61K9/2853 , A61K9/5031
摘要： Polymers comprising reversible hydrophobic functionalities are disclosed. The preferred embodiment polymers comprise Lewis acid segments and Lewis base segments. The polymer segments are, by themselves, hydrophilic and will either swell or dissolve in water. When the segments are incorporated into a polymer according to the present invention, the segments form water-insoluble or hydrophobic complexes. Upon changes in pH, temperature or solvent type, these complexes may dissociate, giving large transitions in polymer viscosity, emulsification ability, mechanical strength or transport properties. These polymers are useful as reversible emulsifiers which form stable emulsions at acidic pH and unstable emulsions at basic pH, as water-borne thickeners having low viscosity at low pH and high viscosity at high pH, as superabsorbing resins, or as coatings for pharmaceutical or agricultural agents.
摘要翻译： 公开了包含可逆疏水官能度的聚合物。 优选的实施方案聚合物包含路易斯酸区段和路易斯碱段。 聚合物段本身是亲水性的，并且将溶胀或溶解在水中。 当根据本发明将片段并入聚合物时，片段形成水不溶性或疏水性复合物。 当pH，温度或溶剂类型发生变化时，这些配合物可能会离解，从而产生聚合物粘度，乳化能力，机械强度或运输性能的巨大转变。 这些聚合物可用作在酸性pH下形成稳定乳液的可逆乳化剂和在碱性pH下形成不稳定乳液，作为在低pH下具有低粘度和在高pH下具有高粘度的水性增稠剂，作为超吸收性树脂，或作为药物或农业用涂料 代理商
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3.发明申请METHOD FOR DETERMINING THE PRODUCTION PARAMETERS FOR A SUBSTRATE COATING PROCESS 有权用于确定基底涂层工艺的生产参数的方法公开(公告)号：US20110166687A1
公开(公告)日：2011-07-07
申请号：US12683001
申请日：2010-01-06
IPC分类号： G05B13/02
CPC分类号： G03F7/038 , C08G59/24 , C08G59/68 , C08G59/683 , C08L2312/06 , C09D4/00
摘要： A method to evaluate, determine and optimize production parameters for a coating application of a UV cationic polymerizable coating system to a substrate is provided. The method is based on a simulation model which includes both shadow and dark cure processes. Both of an active center generation process and the active center diffusion process are mathematically described. In the model, the two processes are considered separately since they are driven by different fundamental phenomena and occur on different timescales. Evaluation or prediction of the effect of process variables on the curing of a cationic coating of a complex substrate according to the described method allows characterization and understanding of process variables which may save set-up costs and improve production efficiency.
摘要翻译： 提供了一种评估，确定和优化将UV阳离子可聚合涂层体系涂覆在基材上的生产参数的方法。 该方法基于包括阴影和暗固化过程的模拟模型。 在数学上描述了活性中心产生过程和活性中心扩散过程。 在模型中，这两个过程被分开考虑，因为它们是由不同的基本现象驱动的，并且发生在不同的时间尺度上。 根据所述方法评价或预测过程变量对复合基底的阳离子涂层固化的影响允许表征和理解可以节省设置成本并提高生产效率的过程变量。
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公开(公告)号：US08197911B2
公开(公告)日：2012-06-12
申请号：US11759984
申请日：2007-06-08
IPC分类号： C08F2/50
CPC分类号： C08F2/46
摘要： An object of complex three-dimensional configuration, such as an automotive vehicle body, is coated with a combination of a coating formulation and a photoactivated mixture containing active centers that have been produced prior to application. The two liquids can be intimately mixed prior to application to the object, or the coating formulation can be applied prior to the application of the photoactivated mixture. The coating formulation is cured by the active centers that have been produced prior to application.
摘要翻译： 复合三维构造的目的，例如机动车体，涂覆有涂层制剂和含有活性中心的光活化混合物的组合，所述活性中心在施用前已经生产。 两种液体在施用于物体之前可以紧密混合，或者可以在施加光活化混合物之前涂覆涂料配方。 涂层制剂由施用前已经生产的活性中心固化。
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5.发明授权
公开(公告)号：US6099783A
公开(公告)日：2000-08-08
申请号：US130672
申请日：1998-08-07
CPC分类号： B29C35/0888 , C08F2/48 , B29C2035/0827 , B29C2035/0838 , B29K2105/0854 , B29K2105/16
摘要： A novel method for producing thick composite parts based upon photopolymerizable compositions is disclosed. Also disclosed are novel methods for encapsulation of microelectronic devices based upon novel photopolymerizable compositions. The constituents of the photopolymerizable mixture comprise a monomer or monomers capable of polymerizing by free radical or cationic mechanisms, and a photoinitiator system which possesses an absorbance characteristic which is effectively reduced, or self-eliminating, upon initiation of the polymerization reaction. Parts having thicknesses up to 2 cm and thicker for varying end use applications are made by photopolymerizing such compositions. In addition, using such compositions composite parts can be made using a reinforcement material such as a glass fiber mat present in an amount by weight of from about 5 to about 70%.
摘要翻译： 公开了一种基于光聚合组合物生产厚复合材料的新方法。 还公开了基于新型可光聚合组合物封装微电子器件的新方法。 可光聚合混合物的组分包含能够通过自由基或阳离子机理聚合的单体或单体，以及在引发聚合反应时具有有效降低或自消除的吸光度特性的光引发剂体系。 通过光聚合这种组合物，可以制成厚度达2厘米且厚度更厚的零件。 此外，使用这样的组合物复合部件可以使用增强材料制成，例如玻璃纤维垫，其重量为约5至约70％。
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6.发明授权Thick, composite parts made from photopolymerizable compositions and methods for making such parts 失效由光聚合组合物制成的厚的复合部件和用于制造这些部件的方法
公开(公告)号：US5855837A
公开(公告)日：1999-01-05
申请号：US467729
申请日：1995-06-06
CPC分类号： C08F2/48 , B29C35/0888 , B29C2035/0827 , B29C2035/0838 , B29K2105/0854 , B29K2105/16 , Y10T428/31525
摘要： A novel method for producing thick composite parts based upon photopolymerizable compositions is disclosed. The constituents of the photopolymerizable mixture comprise a monomer or monomers capable of polymerizing by free radical or cationic mechanisms, and a photoinitiator system which possesses an absorbance characteristic which is effectively reduced, or self-eliminating, upon initiation of the polymerization reaction. Parts having thicknesses up to 2 cm and thicker for varying end use applications are made by photopolymerizing such compositions. In addition, using such compositions composite parts can be made using a reinforcement material such as a glass fiber mat present in an amount by weight of from about 5 to about 70%.
摘要翻译： 公开了一种基于光聚合组合物生产厚复合材料的新方法。 可光聚合混合物的组分包含能够通过自由基或阳离子机理聚合的单体或单体，以及在引发聚合反应时具有有效降低或自消除的吸光度特性的光引发剂体系。 通过光聚合这种组合物，可以制成厚度达2厘米且厚度更厚的零件。 此外，使用这样的组合物复合部件可以使用增强材料制成，例如玻璃纤维垫，其重量为约5至约70％。
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7.发明授权Method for determining the production parameters for a substrate coating process 有权确定基材涂布工艺的生产参数的方法公开(公告)号：US08993042B2
公开(公告)日：2015-03-31
申请号：US12683001
申请日：2010-01-06
CPC分类号： G03F7/038 , C08G59/24 , C08G59/68 , C08G59/683 , C08L2312/06 , C09D4/00
摘要： A method to evaluate, determine and optimize production parameters for a coating application of a UV cationic polymerizable coating system to a substrate is provided. The method is based on a simulation model which includes both shadow and dark cure processes. Both of an active center generation process and the active center diffusion process are mathematically described. In the model, the two processes are considered separately since they are driven by different fundamental phenomena and occur on different timescales. Evaluation or prediction of the effect of process variables on the curing of a cationic coating of a complex substrate according to the described method allows characterization and understanding of process variables which may save set-up costs and improve production efficiency.
摘要翻译： 提供了一种评估，确定和优化将UV阳离子可聚合涂层体系涂覆在基底上的生产参数的方法。 该方法基于包括阴影和黑暗固化过程的模拟模型。 在数学上描述了活性中心产生过程和活性中心扩散过程。 在模型中，这两个过程被分开考虑，因为它们是由不同的基本现象驱动的，并且发生在不同的时间尺度上。 根据所述方法评价或预测过程变量对复合基底的阳离子涂层固化的影响允许表征和理解可以节省设置成本并提高生产效率的过程变量。
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8.发明申请METHOD FOR PRODUCING LAYERED MATERIALS USING LONG-LIVED PHOTO-INDUCED ACTIVE CENTERS 审中-公开使用长效照相感应中心生产层状材料的方法公开(公告)号：US20110059265A1
公开(公告)日：2011-03-10
申请号：US12555933
申请日：2009-09-09
CPC分类号： G03F7/16 , B05D1/36 , B05D1/38 , B05D3/067 , B05D7/53 , B05D2202/10 , C08F2/48 , G03F7/2002
摘要： The invention relates to a method for applying a photo-activated layered polymer coating to a substrate material in which one or more layers do not contain photoinitiator, or are not exposed to initiating light, but cure due to migration of cationic active centers. At least two separate monomer layers are applied to the substrate material. At least one of the monomer layers includes a photoinitiator capable of producing cationic active centers. The at least one layer including the photoinitiator is exposed to a source of UV radiation at a desired wavelength forming cationic active centers. The at least two separate monomer layers react in a polymerization reaction forming a cured layered material. The cationic active centers of the exposed monomer layer migrate to the unexposed layer such that both layers cure via the polymerization reaction.
摘要翻译： 本发明涉及一种将光活化层状聚合物涂层施用于其中一层或多层不含光引发剂或不暴露于起始光但由阳离子活性中心的迁移而固化的基材的材料。 将至少两个单独的单体层施加到基底材料上。 至少一个单体层包括能够产生阳离子活性中心的光引发剂。 将包含光引发剂的至少一层暴露于形成阳离子活性中心的所需波长的UV辐射源。 所述至少两个分离的单体层在形成固化的分层材料的聚合反应中发生反应。 暴露的单体层的阳离子活性中心迁移到未曝光层，使得两层通过聚合反应固化。
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9.发明授权Method for forming reversible colloidal gas or liquid aphrons and compositions produced 失效用于形成可逆胶体气体或液体泡沫的方法和制备的组合物
公开(公告)号：US6022727A
公开(公告)日：2000-02-08
申请号：US5939
申请日：1998-01-12
CPC分类号： C12N1/34 , B01D17/047 , B01D53/1493 , B01J13/02 , Y02E50/343 , Y10S435/818 , Y10S435/821 , Y10S977/904 , Y10S977/92
摘要： A method for forming gas or liquid aphrons with reversible surfactants or emulsifiers is described. Polymers which change their emulsifying properties upon change of pH, temperature or other condition are used to form the aphrons. The aphrons are useful for chemical reactions and separations, mass transfer processes, and for biological processes.
摘要翻译： 描述了用可逆表面活性剂或乳化剂形成气体或液体香料的方法。 使用在pH，温度或其他条件改变时改变其乳化性能的聚合物形成香料。 ap s可用于化学反应和分离，传质过程和生物过程。
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公开(公告)号：US5707587A
公开(公告)日：1998-01-13
申请号：US752830
申请日：1996-11-20
CPC分类号： G01N21/643 , B29C35/0288 , C08J3/248 , G01N33/44
摘要： A method and apparatus (10) for detection of the degree of cure of a polymer in situ and non-invasively. The method and apparatus uses a solvatochromic probe molecule which upon curing produces a shift in the fluorescence emission spectrum as compared to a liquid polymerizable composition. The method and apparatus is particularly adapted for poly(vinyl) polymers. Preferred solvatochromic probe molecules are oxazones and pyrene.
摘要翻译： 一种用于原位和非侵入性地检测聚合物的固化程度的方法和装置（10）。 该方法和装置使用溶剂化色素探针分子，其在固化时与液体可聚合组合物相比产生荧光发射光谱的偏移。 该方法和装置特别适用于聚（乙烯基）聚合物。 优选的溶剂化色素探针分子是恶唑酮和芘。
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