公开(公告)号：US20110294064A1

公开(公告)日：2011-12-01

申请号：US13106150

申请日：2011-05-12

申请人： Azumi MIYAAKE ,  Hideki Sugiura ,  Yuka Mizoguchi

发明人： Azumi MIYAAKE ,  Hideki Sugiura ,  Yuka Mizoguchi

IPC分类号： G03G9/087 ,  G03G13/20 ,  G03G15/08 ,  G03G9/12

CPC分类号： G03G9/0806 ,  G03G9/08755 ,  G03G9/08797

摘要： A toner comprising a colorant, a release agent, an amorphous polyester, and a crystalline polyester having an endothermic peak temperature of 60 to 80° C. and an endothermic quantity of 3.0 to 20.0 J/g. The endothermic peak temperature is determined from a constant rate component curve of the crystalline polyester obtained in a second heating of temperature-modulated differential scanning calorimetry. The endothermic quantity is determined from an area between the constant rate component curve and its base line drawn between 0 and 100° C., within a temperature range of 0 to 50° C.

摘要翻译： 包含着色剂，脱模剂，无定形聚酯和吸热峰温度为60〜80℃，吸热量为3.0〜20.0J / g的结晶性聚酯的调色剂。 吸热峰值温度由温度调制差示扫描量热法的第二次加热中得到的结晶聚酯的恒定速率分量曲线确定。 吸热量由0至100℃的0至100℃之间的恒定速率分量曲线和其基线之间的区域确定。

公开(公告)号：US09034550B2

公开(公告)日：2015-05-19

申请号：US13988600

申请日：2011-11-02

申请人： Yuka Mizoguchi ,  Hideki Sugiura ,  Azumi Miyaake

发明人： Yuka Mizoguchi ,  Hideki Sugiura ,  Azumi Miyaake

IPC分类号： G03G9/093 ,  G03G9/087 ,  G03G15/20

CPC分类号： G03G9/093 ,  G03G9/08755 ,  G03G9/08797 ,  G03G9/09328 ,  G03G9/09371 ,  G03G9/09392 ,  G03G15/2064

摘要： A toner including a binder resin and a colorant, the toner having a core-shell structure containing a core and a shell, wherein the binder resin contains a crystalline polyester resin and a non-crystalline polyester resin, wherein a ratio (A/B) of a mass (A) of the crystalline polyester resin to a mass (B) of the non-crystalline polyester resin is 5/95 to 75/25, and wherein a ratio (Ds/Dc) of a hardness (Ds) of the shell to hardness (Dc) of the core is 1.05 to 1.50 where the hardnesses (Ds) and (Dc) are measured with a scanning probe microscope.

摘要翻译： 一种包含粘合剂树脂和着色剂的调色剂，所述调色剂具有包含核和壳的核 - 壳结构，其中所述粘合剂树脂含有结晶聚酯树脂和非结晶性聚酯树脂，其中比例（A / B） 结晶性聚酯树脂的质量（A）与非结晶性聚酯树脂（B）的质量比（A）为5/95〜75/25，其中，硬度（Ds） 芯的硬度（Dc）为1.05〜1.50，硬度（Ds）和（Dc）用扫描探针显微镜测定。

公开(公告)号：US20130244169A1

公开(公告)日：2013-09-19

申请号：US13988926

申请日：2011-11-02

申请人： Azumi Miyaake ,  Hideki Sugiura ,  Yuka Mizoguchi

发明人： Azumi Miyaake ,  Hideki Sugiura ,  Yuka Mizoguchi

IPC分类号： G03G9/087 ,  G03G13/20 ,  G03G15/20

CPC分类号： G03G9/08755 ,  G03G9/0821 ,  G03G9/08782 ,  G03G9/08791 ,  G03G9/08793 ,  G03G9/08795 ,  G03G9/08797 ,  G03G13/20 ,  G03G15/20

摘要： To provide a toner, which contains: a binder resin; a colorant; and wax, wherein the toner has Ta of 30° C. to 55° C., and Tb—Ta of 8° C. to 25° C., where Ta is a glass transition temperature of the toner determined from a constant heating component of a DSC curve of the toner obtained in a second heating process of temperature modulated differential scanning calorimetry, and Tb is a glass transition temperature of the toner determined from a constant heating component of a DSC curve of the toner obtained in a first heating process of temperature modulated differential scanning calorimetry.

摘要翻译： 提供一种调色剂，其包含：粘合剂树脂; 着色剂 和蜡，其中调色剂具有30℃至55℃的Ta和8℃至25℃的Tb-Ta，其中Ta是由恒定加热组分测定的调色剂的玻璃化转变温度 在温度调制差示扫描量热法的第二加热过程中获得的调色剂的DSC曲线，Tb是由在第一加热过程中获得的调色剂的DSC曲线的恒定加热成分确定的调色剂的玻璃化转变温度 温度差示扫描量热法。

公开(公告)号：US09063446B2

公开(公告)日：2015-06-23

申请号：US13988926

申请日：2011-11-02

申请人： Azumi Miyaake ,  Hideki Sugiura ,  Yuka Mizoguchi

发明人： Azumi Miyaake ,  Hideki Sugiura ,  Yuka Mizoguchi

IPC分类号： G03G9/087 ,  G03G9/08 ,  G03G13/20 ,  G03G15/20

CPC分类号： G03G9/08755 ,  G03G9/0821 ,  G03G9/08782 ,  G03G9/08791 ,  G03G9/08793 ,  G03G9/08795 ,  G03G9/08797 ,  G03G13/20 ,  G03G15/20

摘要： To provide a toner, which contains: a binder resin; a colorant; and wax, wherein the toner has Ta of 30° C. to 55° C., and Tb−Ta of 8° C. to 25° C., where Ta is a glass transition temperature of the toner determined from a constant heating component of a DSC curve of the toner obtained in a second heating process of temperature modulated differential scanning calorimetry, and Tb is a glass transition temperature of the toner determined from a constant heating component of a DSC curve of the toner obtained in a first heating process of temperature modulated differential scanning calorimetry.

摘要翻译： 提供一种调色剂，其包含：粘合剂树脂; 着色剂 和蜡，其中调色剂具有30℃至55℃的Ta和8℃至25℃的Tb-Ta，其中Ta是由恒定加热组分测定的调色剂的玻璃化转变温度 在温度调制差示扫描量热法的第二加热过程中获得的调色剂的DSC曲线，Tb是由在第一加热过程中获得的调色剂的DSC曲线的恒定加热分量确定的调色剂的玻璃化转变温度 温度差示扫描量热法。

公开(公告)号：US20130236828A1

公开(公告)日：2013-09-12

申请号：US13988600

申请日：2011-11-02

申请人： Yuka Mizoguchi ,  Hideki Sugiura ,  Azumi Miyaake

发明人： Yuka Mizoguchi ,  Hideki Sugiura ,  Azumi Miyaake

IPC分类号： G03G9/093

CPC分类号： G03G9/093 ,  G03G9/08755 ,  G03G9/08797 ,  G03G9/09328 ,  G03G9/09371 ,  G03G9/09392 ,  G03G15/2064

摘要： A toner including a binder resin and a colorant, the toner having a core-shell structure containing a core and a shell, wherein the binder resin contains a crystalline polyester resin and a non-crystalline polyester resin, wherein a ratio (A/B) of a mass (A) of the crystalline polyester resin to a mass (B) of the non-crystalline polyester resin is 5/95 to 75/25, and wherein a ratio (Ds/Dc) of a hardness (Ds) of the shell to hardness (Dc) of the core is 1.05 to 1.50 where the hardnesses (Ds) and (Dc) are measured with a scanning probe microscope.

摘要翻译： 一种包含粘合剂树脂和着色剂的调色剂，所述调色剂具有包含核和壳的核 - 壳结构，其中所述粘合剂树脂含有结晶聚酯树脂和非结晶性聚酯树脂，其中比例（A / B） 结晶性聚酯树脂的质量（A）与非结晶性聚酯树脂（B）的质量比（A）为5/95〜75/25，其中，硬度（Ds） 芯的硬度（Dc）为1.05〜1.50，硬度（Ds）和（Dc）用扫描探针显微镜测定。

公开(公告)号：US09678450B2

公开(公告)日：2017-06-13

申请号：US14783945

申请日：2014-04-25

申请人： Mio Kumai ,  Hideki Sugiura ,  Yuka Mizoguchi

发明人： Mio Kumai ,  Hideki Sugiura ,  Yuka Mizoguchi

IPC分类号： G03G9/087 ,  G03G9/093 ,  G03G9/08 ,  G03G9/107

CPC分类号： G03G9/093 ,  G03G9/0821 ,  G03G9/08755 ,  G03G9/08764 ,  G03G9/08795 ,  G03G9/08797 ,  G03G9/107

摘要： Provided is [i] a toner including at least a colorant, a resin, and a releasing agent, wherein a spin-spin relaxation time (t2) of the toner at 90° C. obtained by Hahn Echo method of pulse NMR analysis is from 1.80 msec to 7.00 msec. Also provided is [ii] a toner according to [i], wherein the spin-spin relaxation time (t2) of the toner at 90° C. obtained by Hahn Echo method of pulse NMR analysis is from 3.80 msec to 5.90 msec.

公开(公告)号：US08871418B2

公开(公告)日：2014-10-28

申请号：US13103299

申请日：2011-05-09

申请人： Hideki Sugiura ,  Yuka Mizoguchi

发明人： Hideki Sugiura ,  Yuka Mizoguchi

IPC分类号： G03G9/093 ,  G03G9/08 ,  G03G9/087 ,  G03G15/08

CPC分类号： G03G15/08 ,  G03G9/0819 ,  G03G9/0821 ,  G03G9/0827 ,  G03G9/08797 ,  G03G9/09321 ,  G03G9/09371 ,  G03G9/09392 ,  G03G2215/0602

摘要： A toner containing: a core containing at least a first binder resin, a colorant, and a releasing agent; and a shell containing at least a second binder resin; wherein the toner has a core-shell structure, and has a softening index of 86° C. to 95° C. and a thermal hardness of 0.7 to 1.8.

摘要翻译： 一种调色剂，其含有至少含有第一粘合剂树脂，着色剂和脱模剂的核心; 和含有至少第二粘合剂树脂的壳; 其中调色剂具有核 - 壳结构，并且具有86℃至95℃的软化指数和0.7至1.8的热硬度。

公开(公告)号：US20110097659A1

公开(公告)日：2011-04-28

申请号：US12912099

申请日：2010-10-26

申请人： Hideki Sugiura ,  Yuka Mizoguchi

发明人： Hideki Sugiura ,  Yuka Mizoguchi

IPC分类号： G03G9/08 ,  G03G13/20

CPC分类号： G03G9/0827 ,  G03G9/0819 ,  G03G9/09307 ,  G03G9/09328 ,  G03G9/0935 ,  G03G9/09392 ,  G03G15/6558 ,  G03G15/6564

摘要： A toner including a mother toner particle having a core-shell structure formed of a core containing a binder resin, a coloring agent, and an optional releasing agent, and a shell having a layer thickness of from 0.01 to 2.00 μm, the core having a softening index of from 60 to 85° C. as measured by a flow tester, and the shell having a thermal hardness of from 0.7 to 1.8 m, and an optional external additive.

摘要翻译： 包括具有由包含粘合剂树脂的芯，着色剂和任选的脱模剂形成的核 - 壳结构的母体调色剂颗粒和层厚度为0.01至2.00μm的壳的调色剂，所述芯具有 软化指数为60至85℃，通过流动测试仪测量，并且具有0.7至1.8μm的热硬度的外壳和任选的外部添加剂。

公开(公告)号：US09618864B2

公开(公告)日：2017-04-11

申请号：US14330109

申请日：2014-07-14

申请人： Hideki Sugiura ,  Yuka Mizoguchi ,  Mio Kumai

发明人： Hideki Sugiura ,  Yuka Mizoguchi ,  Mio Kumai

IPC分类号： G03G9/087 ,  G03G9/08 ,  G03G9/093

CPC分类号： G03G9/08755 ,  G03G9/0806 ,  G03G9/0819 ,  G03G9/0825 ,  G03G9/0827 ,  G03G9/08795 ,  G03G9/08797 ,  G03G9/093 ,  G03G9/09392

摘要： A toner comprised of mother toner particles each including a colorant, a resin A capable of forming a crystalline structure, and a resin B incapable of forming a crystalline structure is provided. The resin A is dispersed in the resin B in the state of phase separation. The long axis of each dispersed particle of the resin A has a length of from 30 to 200 nm and the length ratio of the long axis to the short axis is from 2 to 15. The DSC endothermic quantity attributable to the resin A is from 8 to 20 J/g.

公开(公告)号：US09341971B2

公开(公告)日：2016-05-17

申请号：US14338614

申请日：2014-07-23

申请人： Yuka Mizoguchi ,  Hideki Sugiura ,  Mio Kumai

发明人： Yuka Mizoguchi ,  Hideki Sugiura ,  Mio Kumai

IPC分类号： G03G9/087 ,  G03G15/08

CPC分类号： G03G9/08788 ,  G03G9/08724 ,  G03G9/08755 ,  G03G9/08795 ,  G03G9/08797 ,  G03G15/08

摘要： A toner comprised of toner particles including an amorphous resin and a crystalline resin is provided. The coefficient of variation in softening temperature among resin portions in the toner particles is 15% or less when the softening temperature is measured with a scanning probe microscope equipped with a heatable cantilever.

摘要翻译： 提供由包括无定形树脂和结晶树脂的调色剂颗粒组成的调色剂。 当用装有可加热悬臂的扫描探针显微镜测量软化温度时，调色剂颗粒中树脂部分中软化温度的变化系数为15％以下。