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    Process for recovering 3-methylbut-3-en-1-ol
    1.
    发明授权
    Process for recovering 3-methylbut-3-en-1-ol 有权

    公开(公告)号：US10919827B2

    公开(公告)日：2021-02-16

    申请号：US16636474

    申请日：2018-08-10

    Applicant: BASF SE

    Inventor： Albert Werner ,  Miriam Bru Roig ,  Andrei-Nicolae Parvulescu ,  Roland Minges ,  Andreas Keller ,  Stephan Maurer ,  Ulrich Mueller ,  Wolfgang Siegel

    IPC: C07C29/80 ,  C07C29/38 ,  C07C33/025 ,  C07C33/03 ,  B01D3/14 ,  B01J29/70 ,  B01J37/02 ,  B01J37/08

    Abstract: The present invention relates to a process for recovering 3-methylbut-3-en-1-ol from a feed stream F1 comprising 3-methylbut-3-en-1-ol, one or more solvents, water, and isobutene, wherein 3-methylbut-3-en-1-ol, the one or more solvents and water are separated from isobutene by distillation, the process comprising subjecting the feed stream F1 to distillation conditions in a distillation unit, obtaining a bottoms stream B1 which is enriched in -methylbut-3-en-1-ol, in the one or more solvents and in water compared to the feed stream F1 subject The present invention relates to a process for recovering 3-methylbut-3-en-1-ol from a feed stream F1 comprising 3-methylbut-3-en-1-ol, one or more solvents, water, and isobutene, wherein 3-methylbut-3-en-1-ol, the one or more solvents and water are separated from isobutene by distillation, the process comprising subjecting the feed stream F1 to distillation conditions in a distillation unit, obtaining a bottoms stream B1 which is enriched in -methylbut-3-en-1-ol, in the one or more solvents and in water compared to the feed stream F1 subjected to distillation conditions, and a top stream T1 which is enriched in isobutene, further subjecting the bottoms stream B1 to distillation conditions in a second distillation unit and obtaining a bottoms stream B2 which is enriched in 3-methylbut-3-en-1-ol compared to the bottoms stream B1 and a top stream T2 which is enriched in water compared to the bottoms stream B1, further subjecting the bottoms stream B2 to distillation conditions in a third distillation unit and obtaining a top stream T3 which is enriched in 3-methylbut-3-en-1-ol compared to the bottoms stream B2 and a bottoms stream B3. ted to distillation conditions, and a top stream T1 which is enriched in isobutene, further subjecting the bottoms stream B1 to distillation conditions in a second distillation unit and obtaining a bottoms stream B2 which is enriched in 3-methylbut-3-en-1-ol compared to the bottoms stream B1 and a top stream T2 which is enriched in water compared to the bottoms stream B1, further subjecting the bottoms stream B2 to distillation conditions in a third distillation unit and obtaining a top stream T3 which is enriched in 3-methylbut-3-en-1-ol compared to the bottoms stream B2 and a bottoms stream B3.

    METHOD AND APPARATUS FOR PERFORMING A CHEMICAL REACTION UNDER ELEVATED PRESSURE
    3.
    发明申请
    METHOD AND APPARATUS FOR PERFORMING A CHEMICAL REACTION UNDER ELEVATED PRESSURE 有权

    公开(公告)号：US20210322941A1

    公开(公告)日：2021-10-21

    申请号：US17272546

    申请日：2019-09-17

    Applicant: BASF SE

    Inventor： Simon Kokolakis ,  Rocco Paciello ,  Annebart Wentink ,  Albert Werner

    IPC: B01J3/04 ,  B01J19/24 ,  B01J10/00

    Abstract: The invention relates to a method of performing a chemical reaction under elevated pressure. It is suggested that the method comprises the steps of pressurizing a first vessel (3) and a second vessel (5) with reactant-containing liquid and gas to a predetermined pressure, providing reaction conditions in one of the vessels (3, 5) such that the chemical reaction is effected and a product-containing liquid is obtained, withdrawing liquid from the respective vessel (3, 5) as reaction product when a predetermined amount of reaction product has formed, preferably after the chemical reaction in the respective vessel (3, 5) has concluded, and synchronously supplying reactant-containing liquid to the respective other vessel (3, 5), wherein the first and second vessels (3, 5) are in fluid communication by way of a gas communication passage (27). The invention also relates to an apparatus and use thereof for performing said chemical reaction.

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