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公开(公告)号：US09975994B2
公开(公告)日：2018-05-22
申请号：US15545546
申请日：2016-01-22
Applicant: BASF SE
Inventor： Simon Gramlich , Achim Stammer , Angela Ulzhöfer , Frank Niedermaier
IPC: C08G63/02 , C08G65/46 , C07D207/267 , C07C233/05
CPC classification number: C08G65/46 , C07C233/05 , C07D207/267
Abstract: A method for desalinating a salt-containing polymer (SP) comprising a polyaryl ether having a softening temperature TS and a salt (S), comprising the steps of a) providing the salt-containing polymer (SP) at a first temperature T1 above the softening temperature TS of the polyaryl ether, b) contacting the salt-containing polymer (SP) provided in step a) with an extractant (E) to obtain a desalinated polymer (DP) comprising the polyaryl ether, and a salt-containing extractant (SE) comprising the extractant (E) and the salt (S).
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公开(公告)号：US20150065677A1
公开(公告)日：2015-03-05
申请号：US14016504
申请日：2013-09-03
Applicant: BASF SE
Inventor： Faissal-Ali El-Toufaili , Achim Stammer , Siimon Gramlich , Angela Ulzhöfer
IPC: C08G75/23
Abstract: The process for producing aromatic polyether sulfones via reaction of a dichlorodiphenyl sulfone component with a bisphenol component as monomers in the presence of alkali metal carbonate in the melt in the absence of solvents and diluents comprises carrying out the reaction in a mixing kneader which is operated with a shear rate in the range from 5 to 500 s−1.
Abstract translation: 在不存在溶剂和稀释剂的情况下，在熔融物中，在碱金属碳酸盐存在下，通过二氯二苯砜组分与双酚组分作为单体的反应制备芳族聚醚砜的方法包括在混合捏合机中进行反应，该混合捏合机与 剪切速率在5至500s -1范围内。
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Patent Agency Ranking
公开(公告)号：US09738756B2
公开(公告)日：2017-08-22
申请号：US14888243
申请日：2014-04-30
Applicant: BASF SE
Inventor： Rüdiger Häffner , Rolf-Egbert Grützner , Achim Stammer , Angela Ulzhöfer
CPC classification number: C08G69/46 , C08G69/06 , C08G69/30 , C08J5/18 , C08J2377/02
Abstract: The invention relates to a method for synthesizing a polyamide, in which method an aqueous solution is sprayed onto the polyamide before and/or during a solid-state post-condensation process. The aqueous solution comprises at least a first compound, selected from the group comprising phosphoric acid, fully neutralized salts of phosphoric acid, partially neutralized salts of phosphoric acid, and mixtures thereof, and a second compound, selected from the group comprising an acid, an anhydride, a lactone, ammonia, an amine, and mixtures thereof, with the stipulation that the second compound is not phosphoric acid and is not phosphoric acid anhydride. The spraying occurs at a temperature that lies below the boiling point of water. A polyamide that can be produced by means of the method according to the invention can be used in particular to produce films, monofilaments, fibers, threads, or textile sheet materials.
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公开(公告)号：US09045598B2
公开(公告)日：2015-06-02
申请号：US14016504
申请日：2013-09-03
Applicant: BASF SE
Inventor： Faissal-Ali El-Toufaili , Achim Stammer , Simon Gramlich , Angela Ulzhöfer
Abstract: The process for producing aromatic polyether sulfones via reaction of a dichlorodiphenyl sulfone component with a bisphenol component as monomers in the presence of alkali metal carbonate in the melt in the absence of solvents and diluents comprises carrying out the reaction in a mixing kneader which is operated with a shear rate in the range from 5 to 500 s−1.
Abstract translation: 在不存在溶剂和稀释剂的情况下，在熔融物中，在碱金属碳酸盐存在下，通过二氯二苯基砜组分与双酚组分作为单体的反应制备芳族聚醚砜的方法包括在混合捏合机中进行反应，该混合捏合机与 剪切速率在5至500s -1范围内。
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公开(公告)号：US09534083B2
公开(公告)日：2017-01-03
申请号：US14016520
申请日：2013-09-03
Applicant: BASF SE
Inventor： Achim Stammer , Faissal-Ali El-Toufaili , Simon Gramlich , Angela Ulzhöfer
Abstract: In a process for producing polyamides by polycondensation of polycondensable polyamide-forming monomers and/or oligomers in reaction mixtures comprising same, which may be water-containing but are free from organic solvents, the polycondensation is effected in an agitated reactor under agitation in a first step in the liquid phase and after a phase change taking place during the process in the same reactor is effected in a subsequent second step in the solid state, wherein the temperature in the reactor is below the melting point of the polyamide in the second step at least.
Abstract translation: 在通过可缩聚聚酰胺形成单体和/或低聚物在包含它们的反应混合物（其可以是含水但不含有机溶剂）中缩聚制备聚酰胺的方法中，在搅拌反应器中在第一 步骤在液相中，并且在相同反应器中的相变期间发生在固态的随后的第二步骤中，其中反应器中的温度低于第二步中聚酰胺的熔点 最小。
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公开(公告)号：US08629237B2
公开(公告)日：2014-01-14
申请号：US13682091
申请日：2012-11-20
Applicant: BASF SE
Inventor： Rüdiger Häffner , Faissal-Ali El-Toufaili , Achim Stammer , Rolf-Egbert Grützner , Angela Ulzhöfer , Jens Becker
Abstract: A process for producing polyamides from the corresponding monomers and/or prepolymers comprises the steps of (a) reacting the monomers and/or prepolymers and optionally further components under polyamide-forming reaction conditions to form polyamide, (b) treating the polyamide obtained in step (a) in a kneader above the melting temperature of the polyamide, (c) further processing the polyamide from step (b) into pellet, film, fiber or moldings, preferably pelletizing the polyamide, (d) extracting some or all unconverted monomers and any product dimers and oligomers and also optionally further components from the polyamide and/or drying the polyamide.
Abstract translation: 从相应的单体和/或预聚物制备聚酰胺的方法包括以下步骤：（a）在聚酰胺形成反应条件下使单体和/或预聚物和任选的其它组分反应形成聚酰胺，（b）处理步骤 （a）在高于聚酰胺熔融温度的捏合机中，（c）将步骤（b）中的聚酰胺进一步加工成颗粒，膜，纤维或模制品，优选将聚酰胺造粒，（d）提取一些或所有未转化的单体和 任何产物二聚体和低聚物，并且还任选地来自聚酰胺的另外的组分和/或干燥聚酰胺。
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公开(公告)号：US20130131305A1
公开(公告)日：2013-05-23
申请号：US13682091
申请日：2012-11-20
Applicant: BASF SE
Inventor： Rüdiger Häffner , Faissal-Ali El-Toufaili , Achim Stammer , Rolf-Egbert Grützner , Angela Ulzhöfer , Jens Becker
IPC: C08G69/00
Abstract: A process for producing polyamides from the corresponding monomers and/or prepolymers comprises the steps of (a) reacting the monomers and/or prepolymers and optionally further components under polyamide-forming reaction conditions to form polyamide, (b) treating the polyamide obtained in step (a) in a kneader above the melting temperature of the polyamide, (c) further processing the polyamide from step (b) into pellet, film, fiber or moldings, preferably pelletizing the polyamide, (d) extracting some or all unconverted monomers and any product dimers and oligomers and also optionally further components from the polyamide and/or drying the polyamide.
Abstract translation: 从相应的单体和/或预聚物制备聚酰胺的方法包括以下步骤：（a）在聚酰胺形成反应条件下使单体和/或预聚物和任选的其它组分反应形成聚酰胺，（b）处理步骤 （a）在高于聚酰胺熔融温度的捏合机中，（c）将步骤（b）中的聚酰胺进一步加工成颗粒，膜，纤维或模制品，优选将聚酰胺造粒，（d）提取一些或所有未转化的单体和 任何产物二聚体和低聚物，并且还任选地来自聚酰胺的其它组分和/或干燥聚酰胺。
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