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    Method of making hydroxygallium phthalocyanine type V photoconductive imaging members
    1.
    发明授权
    Method of making hydroxygallium phthalocyanine type V photoconductive imaging members 失效
    羟基镓酞菁V型感光成像剂的制备方法

    公开(公告)号：US5482811A

    公开(公告)日：1996-01-09

    申请号：US332304

    申请日：1994-10-31

    申请人： Barkev Keoshkerian ,  George Liebermann ,  Cheng-Kuo Hsiao ,  James D. Mayo ,  Dasarao K. Murti ,  Sandra J. Gardner

    发明人： Barkev Keoshkerian ,  George Liebermann ,  Cheng-Kuo Hsiao ,  James D. Mayo ,  Dasarao K. Murti ,  Sandra J. Gardner

    IPC分类号： C07D487/22 ,  C09B67/16 ,  C09B67/50 ,  G03G5/06 ,  G03G5/047

    CPC分类号： G03G5/0696

    摘要： A process for the preparation of hydroxygallium phthalocyanines which comprises hydrolyzing a gallium phthalocyanine precursor pigment by dissolving said hydroxygallium phthalocyanine in a strong acid and then reprecipitating the resulting dissolved pigment in basic aqueous media; removing any ionic species formed by washing with water, concentrating the resulting aqueous slurry comprised of water and hydroxygallium phthalocyanine to a wet cake; removing water from said slurry by azeotropic distillation with an organic solvent, and subjecting said resulting pigment slurry to mixing with the addition of a second solvent to cause the formation of said hydroxygallium phthalocyanine polymorphs.

    摘要翻译： 一种制备羟基镓酞菁的方法，其包括通过将所述羟基镓酞菁溶解在强酸中，然后将所得溶解的颜料再沉淀在碱性水性介质中来水解镓酞菁前体颜料; 去除通过用水洗涤形成的任何离子物质，将由水和羟基镓酞菁组成的所得水性浆料浓缩到湿饼; 通过与有机溶剂共沸蒸馏从所述浆料中除去水，并将所得颜料浆料加入第二溶剂进行混合，形成所述羟基镓酞菁多晶型物。

    Hydroxygallium phthalocyanine photoconductive imaging members
    3.
    发明授权
    Hydroxygallium phthalocyanine photoconductive imaging members 失效
    羟基镓酞菁光导成像构件

    公开(公告)号：US5563261A

    公开(公告)日：1996-10-08

    申请号：US469240

    申请日：1995-06-06

    申请人： Barkev Keoshkerian ,  George Liebermann ,  Cheng-Kuo Hsiao ,  James D. Mayo ,  Dasarao Murti ,  Sandra J. Gardner

    发明人： Barkev Keoshkerian ,  George Liebermann ,  Cheng-Kuo Hsiao ,  James D. Mayo ,  Dasarao Murti ,  Sandra J. Gardner

    IPC分类号： C07D487/22 ,  C09B67/16 ,  C09B67/50 ,  G03G5/06 ,  C09B67/12

    CPC分类号： G03G5/0696

    摘要： A process for the preparation of hydroxygallium phthalocyanines which comprises hydrolyzing a gallium phthalocyanine precursor pigment by dissolving said hydroxygallium phthalocyanine in a strong acid and then reprecipitating the resulting dissolved pigment in basic aqueous media; removing any ionic species formed by washing with water, concentrating the resulting aqueous slurry comprised of water and hydroxygallium phthalocyanine to a wet cake; removing water from said slurry by azeotropic distillation with an organic solvent, and subjecting said resulting pigment slurry to mixing with the addition of a second solvent to cause the formation of said hydroxygallium phthalocyanine polymorphs.

    摘要翻译： 一种制备羟基镓酞菁的方法，其包括通过将所述羟基镓酞菁溶解在强酸中，然后将所得溶解的颜料再沉淀在碱性水性介质中来水解镓酞菁前体颜料; 去除通过用水洗涤形成的任何离子物质，将由水和羟基镓酞菁组成的所得水性浆料浓缩到湿饼; 通过与有机溶剂共沸蒸馏从所述浆料中除去水，并将所得颜料浆料加入第二溶剂进行混合，形成所述羟基镓酞菁多晶型物。

    Aryl amine polycondensation polymers
    5.
    发明授权
    Aryl amine polycondensation polymers 失效
    芳胺缩聚聚合物

    公开(公告)号：US5419992A

    公开(公告)日：1995-05-30

    申请号：US36162

    申请日：1993-03-24

    申请人： Walter Mychajlowskij ,  George Liebermann ,  William W. Limburg ,  John F. Yanus ,  Dasarao K. Murti

    发明人： Walter Mychajlowskij ,  George Liebermann ,  William W. Limburg ,  John F. Yanus ,  Dasarao K. Murti

    IPC分类号： G03G5/07 ,  G03G15/02

    CPC分类号： G03G5/076

    摘要： A process for the preparation of aryl amine polycondensation polymers useful in electrophotographic imaging members, which process comprises the interfacial polymerization of an aryl amine diol dissolved in an alkaline aqueous phase with a bifunctional acid halide dissolved in an organic solvent, resulting in polymers with high molecular weight and narrow molecular weight distribution (M.sub.w /M.sub.n) of from between about 50,000 to about 350,000, and a M.sub.w /M.sub.n of from about 1 to about 4.

    摘要翻译： 用于制备用于电子照相成像构件的芳基胺缩聚聚合物的方法，该方法包括将溶解在碱性水相中的芳基胺二醇与溶于有机溶剂中的双功能酰卤的界面聚合，得到高分子量的聚合物 重量和窄分子量分布（Mw / Mn）为约50,000至约350,000，Mw / Mn为约1至约4。

    Preparation of micromultichromal spheres
    7.
    发明授权
    Preparation of micromultichromal spheres 失效
    微复合球的制备

    公开(公告)号：US07172712B2

    公开(公告)日：2007-02-06

    申请号：US10249483

    申请日：2003-04-14

    申请人： Peter M. Kazmaier ,  Barkev Keoshkerian ,  George Liebermann ,  Naveen Chopra ,  Hadi K. Mahabadi ,  Jaan Noolandi ,  Francisco E. Torres

    发明人： Peter M. Kazmaier ,  Barkev Keoshkerian ,  George Liebermann ,  Naveen Chopra ,  Hadi K. Mahabadi ,  Jaan Noolandi ,  Francisco E. Torres

    IPC分类号： B29D11/00 ,  G02B26/00

    CPC分类号： G02B26/026 ,  B01J13/04 ,  B01J13/08 ,  B01J13/16 ,  Y10T428/2991

    摘要： A method of making a multichromal sphere includes the steps of preparing a composition of at least (1) a matrix material and (2) at least two sets of particles, each of the sets of particles having a color different from at least one of another of the sets of particles and a segregation (e.g., an electrical or magnetic) property different from at least one of another of the sets of particles, encapsulating the composition within a shell to form an encapsulated sphere, immobilizing the encapsulated sphere in a manner to restrict at least rotation of the encapsulated sphere, subjecting the immobilized encapsulated sphere to an external field associated with the segregation property different among the sets of particles, under conditions in which the sets of particles are able to migrate within the matrix material, thereby producing color segregation in the immobilized encapsulated sphere, and solidifying the matrix material while substantially maintaining the color segregation. In the multichromal spheres, each of the sets of particles is segregated within a separate segment of the solidified matrix material of the core on the basis of the different segregation property.

    摘要翻译： 制备多重色球的方法包括以下步骤：制备至少（1）基质材料的组合物和（2）至少两组颗粒，每组颗粒具有不同于其它颗粒中的至少一种的颜色 的颗粒组以及不同于另一组颗粒的分离（例如，电或磁）性质，将组合物包封在壳体内以形成封装的球体，将封装的球体以 限制封装球体的至少旋转，使固定的包封球体在与该组颗粒之间不同的分离特性相关联的外部场中，在该组颗粒能够在基体材料内迁移的条件下，由此产生颜色 在固定化的包封球体中分离，并固化基质材料，同时基本上保持颜色偏析。 在多重色粉球中，基于不同的分离性质，将这些颗粒组中的每一组分离在核心的固化基质材料的单独部分内。

    Process for tuning photoreceptor sensitivity
    8.
    发明授权
    Process for tuning photoreceptor sensitivity 失效
    调整感光度感光度的过程

    公开(公告)号：US06492080B1

    公开(公告)日：2002-12-10

    申请号：US09815116

    申请日：2001-03-23

    申请人： Richard A. Burt ,  George Liebermann ,  Cheng-Kuo Hsiao ,  Ah-Mee Hor

    发明人： Richard A. Burt ,  George Liebermann ,  Cheng-Kuo Hsiao ,  Ah-Mee Hor

    IPC分类号： G03G5047

    CPC分类号： G03G5/0696

    摘要： A process including: forming a first chlorogallium phthalocyanine (ClGaPc) in N-methyl-2-pyrrolidone (NMP) to form a ClGaPc (NMP) Type-I product; forming a second chlorogallium phthalocyanine in dimethyl sulfoxide (DMSO) to form a ClGaPc (DMSO) Type-I product; separately dry milling and then wet treating the Type-I products to form respective Type-II products; blending the Type-II products together along with a resin to form a coating mixture; and coating the mixture to form a charge generator layer in an electrostatographic imaging article.

    摘要翻译： 一种方法，包括：在N-甲基-2-吡咯烷酮（NMP）中形成第一氯镓酞菁（ClGaPc）以形成ClGaPc（NMP）I型产物; 在二甲基亚砜（DMSO）中形成第二氯镓酞菁以形成ClGaPc（DMSO）I型产物; 分别干磨，然后湿式处理I型产品以形成相应的II型产品; 将II型产品与树脂一起混合以形成涂料混合物; 并在该静电成像制品中涂覆混合物以形成电荷发生器层。