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1.发明申请PBO Fibers with Improved Mechanical Properties when Exposed to High Temperatures and High Relative Humidity 有权PBO纤维在暴露于高温和高相对湿度时具有改进的机械性能公开(公告)号：US20150067940A1
公开(公告)日：2015-03-12
申请号：US14391984
申请日：2013-04-11
发明人： Jay R Sayre , Vince McGinniss , C Byron Tolbert , Kelly J Jenkins , Jeffrey L. Ellis , Tim B Hutson , Sundee Angel , Rachel Thurston
IPC分类号： D06M13/513 , C08K5/5435 , B29C35/02 , F41H1/02
CPC分类号： D06M13/513 , B29C35/0227 , B29K2083/00 , B29L2031/731 , C08K5/5435 , D06M23/105 , F41H1/02 , Y02P20/544
摘要： A method of treating fibers to improve resistance to high temperatures and relative humidity includes providing poly(p-phenylene-2,6-benzobisoxazole) (PBO) fibers, exposing the PBO fibers to an atmosphere of supercritical CO2 saturated with an epoxy silane, i.e. 3-glycidoxypropyl methyldimethoxysilane. The PBO fibers are subjected to a first pressurizing and heating stage at a first temperature (50° C.) for a first period of time. The PBO fibers are then subjected to a second pressurizing and heating stage including increasing the temperature to a second temperature (110° C.) and holding at the second temperature for an additional period of time. The PBO fibers include 2-5 wt % of 3-glycidoxypropyl methyldimethoxysilane after diffusing the CO2 out of the PBO fibers. The fibers are particularly useful in making lightweight body armor system components.
摘要翻译： 处理纤维以改善耐高温和相对湿度的方法包括提供聚（对亚苯基-2,6-苯并双恶唑）（PBO）纤维，将PBO纤维暴露于用环氧硅烷饱和的超临界CO 2气氛中，即 3-环氧丙氧基丙基甲基二甲氧基硅烷。 PBO纤维在第一温度（50℃）下经受第一加压和加热阶段第一段时间。 然后将PBO纤维进行第二加压和加热阶段，包括将温度升高至第二温度（110℃），并在第二温度下保持另外的时间。 PBO纤维在将CO 2从PBO纤维中扩散出来之后，包括2-5重量％的3-缩水甘油氧基丙基甲基二甲氧基硅烷。 纤维在制造轻量级的装甲系统部件中特别有用。
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2.发明授权PBO fibers with improved mechanical properties when exposed to high temperatures and high relative humidity 有权当暴露于高温和高相对湿度时，PBO纤维具有改善的机械性能公开(公告)号：US09279214B2
公开(公告)日：2016-03-08
申请号：US14391984
申请日：2013-04-11
发明人： Jay R Sayre , Vince McGinniss , C Byron Tolbert , Kelly J Jenkins , Jeffrey L Ellis , Tim B Hutson , Sundee Angel , Rachel Thurston
IPC分类号： D06M13/513 , D06M23/10 , B29C35/02 , C08K5/5435 , F41H1/02 , B29K83/00 , B29L31/00
CPC分类号： D06M13/513 , B29C35/0227 , B29K2083/00 , B29L2031/731 , C08K5/5435 , D06M23/105 , F41H1/02 , Y02P20/544
摘要： A method of treating fibers to improve resistance to high temperatures and relative humidity includes providing poly(p-phenylene-2,6-benzobisoxazole) (PBO) fibers, exposing the PBO fibers to an atmosphere of supercritical CO2 saturated with an epoxy silane, i.e. 3-glycidoxypropyl methyldimethoxysilane. The PBO fibers are subjected to a first pressurizing and heating stage at a first temperature (50° C.) for a first period of time. The PBO fibers are then subjected to a second pressurizing and heating stage including increasing the temperature to a second temperature (110° C.) and holding at the second temperature for an additional period of time. The PBO fibers include 2-5 wt % of 3-glycidoxypropyl methyldimethoxysilane after diffusing the CO2 out of the PBO fibers. The fibers are particularly useful in making lightweight body armor system components.
摘要翻译： 处理纤维以改善耐高温和相对湿度的方法包括提供聚（对亚苯基-2,6-苯并双恶唑）（PBO）纤维，将PBO纤维暴露于用环氧硅烷饱和的超临界CO 2气氛中，即 3-环氧丙氧基丙基甲基二甲氧基硅烷。 PBO纤维在第一温度（50℃）下经受第一加压和加热阶段第一段时间。 然后将PBO纤维进行第二加压和加热阶段，包括将温度升高至第二温度（110℃），并在第二温度下保持另外的时间。 PBO纤维在将CO 2从PBO纤维中扩散出来之后，包括2-5重量％的3-缩水甘油氧基丙基甲基二甲氧基硅烷。 纤维在制造轻量级的装甲系统部件中特别有用。
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