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公开(公告)号:US20220267245A1
公开(公告)日:2022-08-25
申请号:US17663071
申请日:2022-05-12
Applicant: CARGILL, INCORPORATED
Inventor: Timothy Walter ABRAHAM , Ravi R. GOKARN
Abstract: Methods and systems for producing alkyl hydroxyalkanoate from hydroxycarboxylic acid recovery bottoms. The methods generally comprise the steps of obtaining a hydroxycarboxylic acid recovery bottom, adding a mono-alcohol to the hydroxycarboxylic acid recovery bottom to obtain a first mixture, heating the first mixture, optionally in the presence of a catalyst, to form a reaction product, distilling the reaction product, and recovering an alkyl hydroxyalkanoate fraction.
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公开(公告)号:US20210095181A1
公开(公告)日:2021-04-01
申请号:US16499704
申请日:2018-03-19
Applicant: CARGILL, INCORPORATED
Inventor: Timothy Walter ABRAHAM , Jeffrey J. MALSAM , Eric Stanley SUMNER
Abstract: Readily water-miscible beta-glucan suspensions and methods of making and using the same. A readily water-miscible beta-glucan suspension includes a beta-glucan and a water-miscible organic fluid that comprises an alcohol, an alpha-hydroxy acid alkyl ester, a polyalkylene glycol alkyl ether, or a combination thereof, wherein the suspension is sufficient such that mixing with water at a shear rate of 40,000 s-1 or more forms a homogeneous mixture of the suspension and the water. The present invention also provides methods of dispersing the water-miscible beta-glucan suspension in water to form homogenous mixtures of the suspension and the water, methods of treating subterranean formations with such homogeneous mixtures, and methods of making the suspension.
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公开(公告)号:US20230348353A1
公开(公告)日:2023-11-02
申请号:US17999744
申请日:2021-05-28
Applicant: CARGILL, INCORPORATED
Inventor: Timothy Walter ABRAHAM , Ravi R. GOKARN , Nolan R. MENTE
IPC: C07C51/48
CPC classification number: C07C51/48
Abstract: The disclosure relates to a method for recovering a malonate comprising a compound of the formula HOC(O)CH2C(O)OM, wherein M is a Group I alkali metal cation or ammonium cation, the method comprising the steps of a) removing water from a fermentation broth comprising malonate to obtain an aqueous concentrate; and b) recovering the malonate comprising the compound of the formula I from the aqueous concentrate.
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公开(公告)号:US20220153676A1
公开(公告)日:2022-05-19
申请号:US17649392
申请日:2022-01-31
Applicant: CARGILL, INCORPORATED
Inventor: Timothy Walter ABRAHAM , Erik ALLEN , John J. HAHN , Paraskevas TSOBANAKIS , Eric Christopher BOHNERT , Christopher Lawrence FRANK
Abstract: A method for recovering a composition enriched in 3-hydroxypropionic acid from a fermentation broth comprising 3-hydroxypropionic acid and/or salts thereof comprises the steps of: (a) providing the fermentation broth having a pH of from about 2 to about 8 comprising: 3-hydroxypropionic acid and/or salts thereof, (b) acidifying the fennentation broth; (c) reducing the total sulfate ion and phosphate ion (d) distilling the resulting reduced ion aqueous solution and (e) recovering the product.
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公开(公告)号:US20200277409A1
公开(公告)日:2020-09-03
申请号:US16646871
申请日:2017-09-20
Applicant: CARGILL, INCORPORATED
Abstract: Described herein is a beta glucan material, comprising 1,3-1,6 beta glucan, that when solubilized achieves a filterability ratio ranging from 1 to 2, preferably 1 to 1.5, and a viscosity ratio ranging from 1.5 to 4. The solubilized beta glucan materials has desired viscosity build and filterability property for EOR applications.
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公开(公告)号:US20200039913A1
公开(公告)日:2020-02-06
申请号:US16601034
申请日:2019-10-14
Applicant: CARGILL, INCORPORATED
Inventor: Timothy Walter ABRAHAM , Erik ALLEN , John J. HAHN , Paraskevas TSOBANAKIS , Eric Christopher BOHNERT , Christopher Lawrence FRANK
Abstract: A method for recovering a composition enriched in 3-hydroxypropionic acid from a fermentation broth comprising 3-hydroxypropionic acid and/or salts thereof comprises the steps of: (a) providing the fermentation broth having a pH of from about 2 to about 8 comprising 3-hydroxypropionic acid and/or salts thereof (b) acidifying the fermentation broth; (c) reducing the total sulfate ion and phosphate ion (d) distilling the resulting reduced ion aqueous solution and (e) recovering the product.
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公开(公告)号:US20240059641A1
公开(公告)日:2024-02-22
申请号:US18495725
申请日:2023-10-26
Applicant: CARGILL, INCORPORATED
Inventor: Timothy Walter ABRAHAM , Erik ALLEN , John J. HAHN , Paraskevas TSOBANAKIS , Eric Christopher BOHNERT , Christopher Lawrence FRANK
CPC classification number: C07C51/44 , B01D3/002 , B01D3/10 , B01D3/34 , B01D15/363 , C07C51/412 , C07C51/42 , C12P7/42
Abstract: A method for recovering a composition enriched in 3-hydroxypropionic acid by providing the fermentation broth, acidifying the fermentation broth; reducing the total sulfate ion and phosphate ion concentration of the resulting aqueous solution to produce a reduced ion aqueous solution; distilling the resulting reduced ion aqueous solution and recovering the resulting aqueous distillation product comprising 3-hydroxypropionic acid.
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公开(公告)号:US20210095182A1
公开(公告)日:2021-04-01
申请号:US16499713
申请日:2018-03-19
Applicant: CARGILL, INCORPORATED
Inventor: Timothy Walter ABRAHAM , Jeffrey J. MALSAM , Eric Stanley SUMNER
Abstract: Readily water-miscible beta-glucan suspensions and methods of making and using the same. A readily water-miscible beta-glucan suspension includes a beta-glucan and a water-miscible organic fluid that comprises an alcohol, an alpha-hydroxy acid alkyl ester, a polyalkylene glycol alkyl ether, or a combination thereof, wherein the suspension is sufficient such that mixing with water at a shear rate of 40,000 s−1 or more forms a homogeneous mixture of the suspension and the water. The present invention also provides methods of dispersing the water-miscible beta-glucan suspension in water to form homogenous mixtures of the suspension and the water, methods of treating subterranean formations with such homogeneous mixtures, and methods of making the suspension.
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公开(公告)号:US20190241494A1
公开(公告)日:2019-08-08
申请号:US16270143
申请日:2019-02-07
Applicant: CARGILL, INCORPORATED
Inventor: Timothy Walter ABRAHAM , Ravi R. GOKARN
Abstract: Methods and systems for producing alkyl hydroxyalkanoate from hydroxy carboxylic acid recovery bottoms. The methods generally comprise the steps of obtaining a hydroxy carboxylic acid recovery bottom, adding a mono-alcohol to the hydroxy carboxylic acid recovery bottom to obtain a first mixture, heating the first mixture in the presence of a catalyst to form a reaction product, distilling the reaction product, and recovering an alkyl hydroxyalkanoate fraction.
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公开(公告)号:US20190112518A1
公开(公告)日:2019-04-18
申请号:US16089740
申请日:2017-03-28
Applicant: CARGILL, INCORPORATED
Inventor: Timothy Walter ABRAHAM , Eric Stanley SUMNER
Abstract: Disclosed herein is a method to rapidly solubilize beta glucan (BG) material comprising passing the beta glucan material, in solution, through an in-line high shear system, wherein viscosity of the solubilized beta glucan material is 90% or greater of ultimate viscosity and wherein filterability ratio of the solubilized beta glucan material ranges from about 1-2.
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