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公开(公告)号：US09840587B2
公开(公告)日：2017-12-12
申请号：US14437523
申请日：2013-10-23
发明人： Tomomich Kanda , Tomoaki Shimoda
CPC分类号： C08G69/30 , C08G69/26 , C08G69/265 , C08G69/28 , C08G69/46
摘要： The polyamide production method of the present invention comprises the steps of: producing a low-order condensate by effecting a polycondensation reaction between a dicarboxylic acid component containing between about 5 and about 40 mol. % of terephthalic acid, and a diamine component containing between about 70 and about 100 mol. % of a xylylenediamine in which the content of paraxylylenediamine is between about 50 and about 100 mol. %, under conditions of a reaction temperature of at least about 200° C. and less than about 230° C.; discharging and cooling the low-order condensate at a pressure at or below atmospheric pressure, in an inert gas atmosphere; and subjecting the discharged and cooled low-order condensate to solid state polymerization. The production method makes it possible to obtain a polyamide having outstanding mechanical strength, heat resistance, color tone and the like without problems such as gelling.
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公开(公告)号：US20150329672A1
公开(公告)日：2015-11-19
申请号：US14437523
申请日：2013-10-23
发明人： Tomomich Kanda , Tomoaki Shimoda
CPC分类号： C08G69/30 , C08G69/26 , C08G69/265 , C08G69/28 , C08G69/46
摘要： The polyamide production method of the present invention comprises the steps of: producing a low-order condensate by effecting a polycondensation reaction between a dicarboxylic acid component containing between about 5 and about 40 mol. % of terephthalic acid, and a diamine component containing between about 70 and about 100 mol. % of a xylylenediamine in which the content of paraxylylenediamine is between about 50 and about 100 mol. %, under conditions of a reaction temperature of at least about 200° C. and less than about 230° C.; discharging and cooling the low-order condensate at a pressure at or below atmospheric pressure, in an inert gas atmosphere; and subjecting the discharged and cooled low-order condensate to solid state polymerization. The production method makes it possible to obtain a polyamide having outstanding mechanical strength, heat resistance, colour tone and the like without problems such as gelling.
摘要翻译： 本发明的聚酰胺制造方法包括以下步骤：通过在含有约5〜约40mol的二羧酸成分之间进行缩聚反应来制造低级缩合物。 ％的对苯二甲酸和含有约70至约100mol的二胺组分。 ％的对二甲苯二胺的含量为约50至约100摩尔的苯二甲胺。 在反应温度为至少约200℃且小于约230℃的条件下; 在惰性气体气氛中在低于或低于大气压的压力下排放和冷却低级冷凝物; 并将排出和冷却的低级缩合物进行固态聚合。 制造方法可以获得具有突出的机械强度，耐热性，色调等的聚酰胺，而没有诸如凝胶化的问题。
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3.发明申请公开(公告)号：US20140303341A1
公开(公告)日：2014-10-09
申请号：US14363875
申请日：2012-12-11
发明人： Seung Hyun Jang , Ki Yon Lee , Young Sub Jin , Suk Min Jun , Tomoaki Shimoda , Sang Kyun Im
CPC分类号： C08G69/265 , C08G69/04 , C08L77/06
摘要： The present invention relates to: a polyamide resin which is a copolymer of a mixture comprising (a1) one or more aliphatic diamine monomers selected from C4 to C10 aliphatic diamines, and (a2) one or more aliphatic diamine monomers selected from C11 to C18 aliphatic diamines, and a mixture comprising (b1) one or more aromatic dicarboxylic acid monomers selected from aromatic dicarboxylic acids, and (b2) one or more aliphatic dicarboxylic acid monomers selected from C4 to C14 aliphatic dicarboxylic acids, and has an amine and acid end group number greater than about 0 μeq/g to about 150 μeq/g; a preparation method thereof; and an article comprising the same.
摘要翻译： 本发明涉及：聚酰胺树脂，其是包含（a1）选自C4-C10脂族二胺的一种或多种脂族二胺单体和（a2）一种或多种选自C 11 -C 18脂族二胺的脂族二胺单体的混合物的共聚物 二胺和包含（b1）一种或多种选自芳族二羧酸的芳族二羧酸单体和（b2）一种或多种选自C 4至C 14脂族二羧酸的脂族二羧酸单体的混合物，并且具有胺和酸端基 大于约0μeq/ g至约150μeq/ g; 其制备方法 和包含该物品的物品。
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