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公开(公告)号：US09273154B2
公开(公告)日：2016-03-01
申请号：US13522757
申请日：2011-01-17
申请人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
发明人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
IPC分类号： C08F8/22 , C08C19/24 , C08F8/30 , C08C19/14 , C08C19/22 , C08F2/06 , C08F8/32 , C08F8/40 , C08F210/12
CPC分类号： C08C19/24 , C08C19/14 , C08C19/22 , C08F2/06 , C08F8/22 , C08F8/30 , C08F8/32 , C08F8/40 , C08F210/12 , C08F236/08
摘要： The invention relates to an energy efficient, environmentally favorable process for the preparation of butyl ionomers that uses a common medium for both solution polymerization and subsequent bromination of butyl rubber. More particularly, the invention relates to a process that employs a common aliphatic medium for both solution polymerization and bromination of butyl rubber in the presence of a brominating agent and optionally for subsequent reaction with at least one nitrogen and/or phosphorus based nucleophile.
摘要翻译： 本发明涉及用于制备丁基离聚物的能量效率高，环境友好的方法，该方法使用普通介质进行溶液聚合和随后溴化丁基橡胶。 更具体地说，本发明涉及一种在溴化剂存在下使用普通脂肪族介质进行丁基橡胶的溶液聚合和溴化的方法，并且任选地随后与至少一种基于氮和/或磷的亲核试剂反应。
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公开(公告)号：US09062185B2
公开(公告)日：2015-06-23
申请号：US13522760
申请日：2011-01-17
申请人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
发明人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
IPC分类号： C08L9/00 , B60C1/00 , B82Y30/00 , C08J5/00 , C08F210/12
CPC分类号： C08L9/00 , B60C1/00 , B82Y30/00 , C08F8/22 , C08F8/40 , C08F8/44 , C08F210/12 , C08J5/005 , C08J2323/28 , C08J2323/36 , Y02T10/862 , C08F236/08 , C08F2500/21
摘要： The invention relates to a processes for preparing nanocomposites comprising rubber ionomers which were prepared by an energy efficient, environmentally favorable process that uses a common medium for solution polymerization, bromination of rubber and optionally subsequent polymer nanocomposite formation. Polymer nanocomposites according to the present invention exhibit high oxygen impermeability.
摘要翻译： 本发明涉及一种制备纳米复合材料的方法，其包括橡胶离聚物，其通过使用普通介质进行溶液聚合，溴化橡胶和任选的后续聚合物纳米复合材料形成的能量有效的，环境友好的方法制备。 根据本发明的聚合物纳米复合材料显示出高的不透气性。
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公开(公告)号：US20130178577A1
公开(公告)日：2013-07-11
申请号：US13522760
申请日：2011-01-17
申请人： Carsten Kreuder , John Lovegrove , Phil Magill , Hanns-Ingolf Paul , Rolf Feller , Adam Gronowski , Dana Adkinson
发明人： Carsten Kreuder , John Lovegrove , Phil Magill , Hanns-Ingolf Paul , Rolf Feller , Adam Gronowski , Dana Adkinson
IPC分类号： C08L9/00
CPC分类号： C08L9/00 , B60C1/00 , B82Y30/00 , C08F8/22 , C08F8/40 , C08F8/44 , C08F210/12 , C08J5/005 , C08J2323/28 , C08J2323/36 , Y02T10/862 , C08F236/08 , C08F2500/21
摘要： The invention relates to a processes for preparing nanocomposites comprising rubber ionomers which were prepared by an energy efficient, environmentally favourable process that uses a common medium for solution polymerization, bromination of rubber and optionally subsequent polymer nanocomposite formation. Polymer nanocomposites according to the present invention exhibit high oxygen impermeability.
摘要翻译： 本发明涉及一种制备纳米复合材料的方法，其包括橡胶离聚物，其通过使用普通介质进行溶液聚合，溴化橡胶和任选的后续聚合物纳米复合材料形成的能量有效，环境友好的方法制备。 根据本发明的聚合物纳米复合材料显示出高的不透气性。
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公开(公告)号：US20130165582A1
公开(公告)日：2013-06-27
申请号：US13522757
申请日：2011-01-17
申请人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
发明人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
CPC分类号： C08C19/24 , C08C19/14 , C08C19/22 , C08F2/06 , C08F8/22 , C08F8/30 , C08F8/32 , C08F8/40 , C08F210/12 , C08F236/08
摘要： The invention relates to an energy efficient, environmentally favourable process for the preparation of butyl ionomers that uses a common medium for both solution polymerization and subsequent bromination of butyl rubber. More particularly, the invention relates to a process that employs a common aliphatic medium for both solution polymerization and bromination of butyl rubber in the presence of a brominating agent and optionally for subsequent reaction with at least one nitrogen and/or phosphorus based nucleophile.
摘要翻译： 本发明涉及用于制备丁基离聚物的能量效率高，环境友好的方法，该方法使用普通介质进行溶液聚合和随后溴化丁基橡胶。 更具体地说，本发明涉及一种在溴化剂存在下使用普通脂肪族介质进行丁基橡胶的溶液聚合和溴化的方法，并且任选地随后与至少一种基于氮和/或磷的亲核试剂反应。
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5.发明授权公开(公告)号：US09505863B2
公开(公告)日：2016-11-29
申请号：US13635793
申请日：2011-03-23
申请人： Hanns-Ingolf Paul , Rolf Feller , Paul Wagner , John Lovegrove , Adam Gronowski , Phil Magill , Dana Adkinson , Jörg Kirchhoff
发明人： Hanns-Ingolf Paul , Rolf Feller , Paul Wagner , John Lovegrove , Adam Gronowski , Phil Magill , Dana Adkinson , Jörg Kirchhoff
IPC分类号： C08F8/40 , C08F290/14 , C08F8/00 , C08F236/16 , C08C2/00 , C08C19/12 , C08C19/32 , C08F6/00 , C08L15/02 , B29C47/36 , B29C47/38
CPC分类号： C08F236/16 , B29C47/364 , B29C47/38 , C08C2/00 , C08C19/12 , C08C19/32 , C08F6/003 , C08L15/02 , C08L23/283
摘要： The invention relates to an energy efficient, environmentally favourable process for preparing water and solvent-free rubber ionomers and/or polymer nanocomposites comprising said rubber ionomers.
摘要翻译： 本发明涉及一种能量有效，环境友好的制备包含所述橡胶离聚物的水和无溶剂橡胶离聚物和/或聚合物纳米复合材料的方法。
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6.发明授权Common solvent process for producing high molecular weight halogenated rubber 有权用于生产高分子量卤化橡胶的常用溶剂方法公开(公告)号：US09273161B2
公开(公告)日：2016-03-01
申请号：US13522762
申请日：2011-01-17
申请人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Udo Wiesner
发明人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Udo Wiesner
CPC分类号： C08F8/22 , B60C1/00 , C08F210/12
摘要： The invention relates to an energy efficient, environmentally favorable process for the preparation of halogenated rubbers, in particular chloro- and bromobutyl rubber, that uses a common aliphatic medium of specific composition for both solution polymerization and subsequent halogenation of the rubber. More particularly, the invention relates to a process that employs a common aliphatic medium for both solution polymerization and halogenation of rubber with intermediate removal of un-reacted monomers.
摘要翻译： 本发明涉及用于制备卤化橡胶，特别是氯代和溴化丁基橡胶的能量有效，环境友好的方法，其使用具有特定组成的普通脂族介质用于溶液聚合和随后的橡胶卤化。 更具体地说，本发明涉及一种使用普通脂肪族介质进行溶液聚合和橡胶卤化的方法，同时中间除去未反应的单体。
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7.发明授权公开(公告)号：US09273160B2
公开(公告)日：2016-03-01
申请号：US13522756
申请日：2011-01-17
申请人： Adam Gronowski , Carsten Kreuder , John Lovegrove , Paul Nguyen , David Thompson , Hanns-Ingolf Paul , Rolf Feller , Udo Weisner
发明人： Adam Gronowski , Carsten Kreuder , John Lovegrove , Paul Nguyen , David Thompson , Hanns-Ingolf Paul , Rolf Feller , Udo Weisner
IPC分类号： C08F8/22 , C08C19/14 , C08F2/06 , C08F6/00 , C08F210/12
CPC分类号： C08F8/22 , C08C19/14 , C08F2/06 , C08F6/003 , C08F210/12 , C08L23/283 , C08F236/08
摘要： The invention relates to an energy efficient, environmentally favorable process for the preparation of brominated rubbers, in particular bromobutyl rubber, that uses a common medium for both solution polymerization and subsequent bromination of the rubber and which further exhibits an enhanced bromine usage due to the use of a oxidizing agent. More particularly, the invention relates to a process that employs a common aliphatic medium for both solution polymerization and bromination of rubber in the presence of a brominating agent and an oxidizing agent with intermediate removal of un-reacted monomers.
摘要翻译： 本发明涉及一种用于制备溴化橡胶，特别是溴化丁基橡胶的能量效率高，环境友好的方法，其使用普通介质进行溶液聚合和随后的溴化溴化，并且由于使用而进一步显示出增强的溴用量 的氧化剂。 更具体地说，本发明涉及一种在溴化剂和氧化剂存在下使用普通脂族介质进行溶液聚合和溴化溴化的方法，同时中间除去未反应的单体。
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8.发明申请COMMON SOLVENT PROCESS FOR PRODUCING HIGH MOLECULAR WEIGHT HALOGENATED RUBBER 有权用于生产高分子量重量橡胶的常用溶剂方法公开(公告)号：US20130137832A1
公开(公告)日：2013-05-30
申请号：US13522762
申请日：2011-01-17
申请人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Udo Wiesner
发明人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Udo Wiesner
IPC分类号： C08F8/22
CPC分类号： C08F8/22 , B60C1/00 , C08F210/12
摘要： The invention relates to an energy efficient, environmentally favourable process for the preparation of halogenated rubbers, in particular chloro- and bromobutyl rubber, that uses a common aliphatic medium of specific composition for both solution polymerization and subsequent halogenation of the rubber. More particularly, the invention relates to a process that employs a common aliphatic medium for both solution polymerization and halogenation of rubber with intermediate removal of un-reacted monomers.
摘要翻译： 本发明涉及用于制备卤化橡胶，特别是氯代和溴化丁基橡胶的能量有效，环境友好的方法，其使用具有特定组成的普通脂族介质用于溶液聚合和随后的橡胶卤化。 更具体地说，本发明涉及一种使用普通脂肪族介质进行溶液聚合和橡胶卤化的方法，同时中间除去未反应的单体。
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9.发明申请公开(公告)号：US20130131281A1
公开(公告)日：2013-05-23
申请号：US13522756
申请日：2011-01-17
申请人： Adam Gronowski , Carsten Kreuder , John Lovegrove , Paul Nguyen , David Thompson , Hanns-Ingolf Paul , Rolf Feller , Udo Weisner
发明人： Adam Gronowski , Carsten Kreuder , John Lovegrove , Paul Nguyen , David Thompson , Hanns-Ingolf Paul , Rolf Feller , Udo Weisner
IPC分类号： C08F8/22
CPC分类号： C08F8/22 , C08C19/14 , C08F2/06 , C08F6/003 , C08F210/12 , C08L23/283 , C08F236/08
摘要： The invention relates to an energy efficient, environmentally favourable process for the preparation of brominated rubbers, in particular bromobutyl rubber, that uses a common medium for both solution polymerization and subsequent bromination of the rubber and which further exhibits an enhanced bromine usage due to the use of a oxidizing agent. More particularly, the invention relates to a process that employs a common aliphatic medium for both solution polymerization and bromination of rubber in the presence of a brominating agent and an oxidizing agent with intermediate removal of un-reacted monomers.
摘要翻译： 本发明涉及一种用于制备溴化橡胶，特别是溴化丁基橡胶的能量效率高，环境友好的方法，其使用普通介质进行溶液聚合和随后的溴化溴化，并且由于使用而进一步显示出增强的溴用量 的氧化剂。 更具体地说，本发明涉及一种在溴化剂和氧化剂存在下使用普通脂族介质进行溶液聚合和溴化溴化的方法，同时中间除去未反应的单体。
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10.发明申请公开(公告)号：US20130217833A1
公开(公告)日：2013-08-22
申请号：US13635793
申请日：2011-03-23
申请人： Hanns-Ingolf Paul , Rolf Feller , Paul Wagner , John Lovegrove , Phil Magill , Dana Adkinson , Jörg Kirchhoff
发明人： Hanns-Ingolf Paul , Rolf Feller , Paul Wagner , John Lovegrove , Phil Magill , Dana Adkinson , Jörg Kirchhoff
IPC分类号： C08F236/16
CPC分类号： C08F236/16 , B29C47/364 , B29C47/38 , C08C2/00 , C08C19/12 , C08C19/32 , C08F6/003 , C08L15/02 , C08L23/283
摘要： The invention relates to an energy efficient, environmentally favourable process for preparing water and solvent-free rubber ionomers and/or polymer nanocomposites comprising said rubber ionomers.
摘要翻译： 本发明涉及一种能量有效，环境友好的制备包含所述橡胶离聚物的水和无溶剂橡胶离聚物和/或聚合物纳米复合材料的方法。
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