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    CATALYST THAT CAN BE USED IN HYDROTREATMENT, COMPRISING METALS OF GROUPS VIII AND VIB, AND PREPARATION WITH ACETIC ACID AND DIALKYL SUCCINATE C1-C4
    3.
    发明申请
    CATALYST THAT CAN BE USED IN HYDROTREATMENT, COMPRISING METALS OF GROUPS VIII AND VIB, AND PREPARATION WITH ACETIC ACID AND DIALKYL SUCCINATE C1-C4 有权
    催化剂可用于水合物，包含VIII和VIB族金属，以及乙酸和二烷基邻苯二甲酸酯C1-C4的制备

    公开(公告)号：US20130008829A1

    公开(公告)日：2013-01-10

    申请号：US13516411

    申请日：2010-12-08

    申请人： Karin Marchand ,  Bertrand Guichard ,  Mathieu Digne ,  Michael Rebeilleau ,  Sylvie Lopez ,  Antoine Hugon

    发明人： Karin Marchand ,  Bertrand Guichard ,  Mathieu Digne ,  Michael Rebeilleau ,  Sylvie Lopez ,  Antoine Hugon

    IPC分类号： C10G45/04 ,  C10G49/02 ,  B01J27/16

    CPC分类号： B01J27/14 ,  B01J23/28 ,  B01J23/75 ,  B01J27/19 ,  B01J37/0201 ,  C10G45/04 ,  C10G45/08 ,  C10G45/46 ,  C10G45/48 ,  C10G47/12 ,  C10G49/04 ,  C10G2300/1055 ,  C10G2300/202 ,  C10G2300/70 ,  C10G2400/04

    摘要： The invention relates to a catalyst usable in hydrotreatment processes, which comprises an alumina-based amorphous support, phosphorus, a C1-C4 dialkyl succinate, acetic acid and a hydro-dehydrogenizing function comprising at least one group VIII element and at least one group VIB element, preferably made up of cobalt and molybdenum, a catalyst whose Raman spectrum comprises the most intense bands characteristic of the Keggin heteropolyanions (974 and/or 990 cm−1), C1-C4 dialkyl succinate and acetic acid (896 cm−1). Preferably, the dialkyl succinate concerned is dimethyl succinate and its main band is at 853 cm−1.The invention also relates to the method of preparing said catalyst, wherein a catalytic precursor comprising the group VIB and group VIII elements, in particular the molybdenum-cobalt pair, and phosphorus, introduced by impregnation, then dried at a temperature below 180° C., is impregnated by the C1-C4 dialkyl succinate, the acetic acid and the phosphorus compound, if the latter has not been entirely introduced beforehand, then, after maturation, dried at a temperature below 180° C. prior to being optionally sulfurized.The invention also relates to the use of this catalyst in any hydrotreatment process.

    摘要翻译： 本发明涉及可用于加氢处理方法的催化剂，其包含基于氧化铝的无定形载体，磷，C 1 -C 4二烷基琥珀酸酯，乙酸和加氢脱氢功能，其包含至少一种VIII族元素和至少一种VIB族 元素，优选由钴和钼组成的催化剂，其拉曼光谱包括Keggin杂多阴离子（974和/或990cm-1），C1-C4二烷基琥珀酸酯和乙酸（896cm -1）特征的最强烈的带， 。 优选地，琥珀酸二烷基酯是琥珀酸二甲酯，其主带是853cm -1。 本发明还涉及制备所述催化剂的方法，其中通过浸渍引入的包含VIB族和VIII族元素，特别是钼 - 钴对的催化前体和磷，然后在低于180℃的温度下干燥。 由C1-C4二烷基琥珀酸酯，乙酸和磷化合物浸渍，如果后者尚未完全引入，则成熟后，在任选硫化之前，在低于180℃的温度下干燥。 本发明还涉及该催化剂在任何加氢处理方法中的用途。