摘要:
To collect analyte from a supercritical fluid extractor, the collector lifts vials into place by a biasing means that guides the file up to the restrictor where it is sealed. The vial can be moved back down from the collecting mechanism even if frost forms on the vial while the restrictor means remains stationary. This vial is held in place by a guide that contains the seal for sealing the vial when it is raised in place.
摘要:
To collect analyte from a supercritical fluid extractor, the collector lifts vials into place by a biasing device that guides the file up to the restrictor where it is sealed. The vial can be moved back down from the collecting mechanism even if frost forms on the vial while the restrictor remains stationary. This vial is held in place by a guide that contains the seal for sealing the vial when it is raised in place.
摘要:
To supply supercritical fluid to an automatic supercritical fluid extractor and collect extract from the extractor, sample holding cartridges are lifted one by one in series by an elevator plug into a pressure chamber. An inlet at the top of the cartridge engages a pressure vessel inlet for the extractant so that extractant flows into the cartridge and into the space between the cartridge and inner walls of the pressure chamber. The outlets from the cartridge and pressure vessel communicate with the collector and exhaust through passageways in the plug. The plug has cleaning ports for cleaning seals and the outlet from the cartridge flows past the seals. The collector lifts vials into place and can precool the collection solvent, and later as part of the collection procedure, heat and pressurize the collector.
摘要:
An apparatus for supercritical extraction is disclosed herein. The apparatus includes a plurality of containers adapted to hold a different one of a corresponding plurality of samples, a first transport means for carrying the plurality of sample containers, and a second transport means for transporting a selected container from the first transport means to a supercritical extractor. The supercritical extractor includes a heating means having a recess for receiving the selected container, means for passing fluid at a supercritical condition through the selected container, and a receiving means for receiving extractant from the selected container. A programming means is provided to control the first and second transport means.