公开(公告)号：US20120183470A1

公开(公告)日：2012-07-19

申请号：US13384703

申请日：2010-07-20

申请人： Daniel Aymes ,  Moustapha Ariane ,  Frédéric Bernard ,  Hervé Muhr ,  Frédéric Demolsson

发明人： Daniel Aymes ,  Moustapha Ariane ,  Frédéric Bernard ,  Hervé Muhr ,  Frédéric Demolsson

IPC分类号： C01B13/18 ,  B22F9/24 ,  B01J19/00 ,  B82Y40/00

CPC分类号： B01J2/02 ,  B01J2/06 ,  B01J2219/00123 ,  B82Y30/00 ,  C01B13/36 ,  C01G9/02 ,  C01G23/047 ,  C01G25/02 ,  C01G49/02 ,  C01P2004/64

摘要： The present invention relates to a method for continuously preparing mineral particles by means of the thermolysis of mineral precursors in an aqueous medium, comprising contacting: a reactive flow, including mineral precursors at a temperature lower than the conversion temperature thereof; and a coolant flow that is countercurrent to said reactive flow and contains water at a temperature that is sufficient to bring the precursors to a temperature higher than the conversion temperature thereof, the mixture flow that results from said reactive flow and said coolant flow then being conveyed into a tubular reactor, inside of which particles are formed by gradually converting the precursors, and where the reactive flow and the coolant flow are placed in contact with each other inside a mixing chamber, inside of which the reactive flow and the coolant flow are fed by supply pipes having outlet cross-sections that are smaller than the maximum cross-section of said mixing chamber. The invention also relates to a device for implementing said method.

摘要翻译： 本发明涉及一种通过在水性介质中热分解矿物前体而连续制备矿物颗粒的方法，包括在低于其转化温度的温度下接触包括矿物前体的反应性流; 以及与所述反应流逆流并且在足以使前体达到高于其转化温度的温度的温度下的水的冷却剂流，由所述反应流和所述冷却剂流产生的混合物流随后被传送 进入管状反应器，其中通过逐渐转化前体形成颗粒，并且其中反应流和冷却剂流在混合室内彼此接触地置于其中，其中反应流和冷却剂流被供给 通过具有比所述混合室的最大横截面小的出口横截面的供给管。 本发明还涉及一种用于实现所述方法的装置。

公开(公告)号：US08986648B2

公开(公告)日：2015-03-24

申请号：US13384703

申请日：2010-07-20

申请人： Daniel Aymes ,  Moustapha Ariane ,  Frédéric Bernard ,  Hervé Muhr ,  Frédéric Demoisson

发明人： Daniel Aymes ,  Moustapha Ariane ,  Frédéric Bernard ,  Hervé Muhr ,  Frédéric Demoisson

IPC分类号： C01B13/00 ,  B01J2/02 ,  B01J2/06 ,  B82Y30/00 ,  C01B13/36 ,  C01G9/02 ,  C01G23/047 ,  C01G25/02 ,  C01G49/02

CPC分类号： B01J2/02 ,  B01J2/06 ,  B01J2219/00123 ,  B82Y30/00 ,  C01B13/36 ,  C01G9/02 ,  C01G23/047 ,  C01G25/02 ,  C01G49/02 ,  C01P2004/64

摘要： The present invention relates to a method for continuously preparing mineral particles by means of the thermolysis of mineral precursors in an aqueous medium, comprising contacting: a reactive flow, including mineral precursors at a temperature lower than the conversion temperature thereof; and a heat transfer flow that is countercurrent to said reactive flow and contains water at a temperature that is sufficient to bring the precursors to a temperature higher than the conversion temperature thereof, the mixture flow that results from said reactive flow and said heat transfer flow then being conveyed into a tubular reactor, inside of which particles are formed by gradually converting the precursors, and where the reactive flow and the heat transfer flow are placed in contact with each other inside a mixing chamber, inside of which the reactive flow and the heat transfer flow are fed by supply pipes having outlet cross-sections that are smaller than the maximum cross-section of said mixing chamber. The invention also relates to a device for implementing said method.

摘要翻译： 本发明涉及一种通过在水性介质中热分解矿物前体而连续制备矿物颗粒的方法，包括在低于其转化温度的温度下接触包括矿物前体的反应性流; 以及与所述反应性流逆流并且在足以使前体达到高于其转化温度的温度的温度下的水的传热流，由所述反应流和所述传热流产生的混合物流 被输送到管式反应器中，其中通过逐渐转化前体形成颗粒，并且其中反应流和传热流在混合室内相互接触地形成，其中反应流和热量 输送流由具有小于所述混合室的最大横截面的出口横截面的供给管供给。 本发明还涉及一种用于实现所述方法的装置。