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1.发明授权Crystalline form of 2-(4,6-bis-biphenyl-4-yl-1,3,5-triazin-2-yl)-5-(2-ethyl-(n)-hexyloxy)phenol 有权2-（4,6-双 - 联苯-4-基-1,3,5-三嗪-2-基）-5-（2-乙基 - （n） - 己氧基）苯酚的结晶形式公开(公告)号：US08105668B2
公开(公告)日：2012-01-31
申请号：US12744717
申请日：2008-11-26
CPC分类号： C07D251/24 , C08K5/3492 , Y10T428/1345 , Y10T428/1352 , Y10T428/31507 , Y10T428/31786 , Y10T428/31855 , Y10T442/60
摘要： The crystalline form of 2-(4,6-bis-biphenyl-4-yl-1,3,5-triazin-2-yl)-5-(2-ethyl-(n)-hexyloxy)phenol, characterized by a X-ray diffraction pattern obtained by using Cu—Kα-radiation which exhibits the diffraction angles (2-Theta).
摘要翻译： 2-（4,6-双 - 联苯-4-基-1,3,5-三嗪-2-基）-5-（2-乙基 - （n） - 己氧基）苯酚的结晶形式，其特征在于 通过使用具有衍射角（2-Theta）的Cu-Kα-辐射获得的X射线衍射图。
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2.发明授权Crystalline form of 2-(4,6-bis-biphenyl-4-yl-1,3,5-triazin-2-yl)-5-(2-ethyl-(n)-hexyloxy)phenol 有权2-（4,6-双 - 联苯-4-基-1,3,5-三嗪-2-基）-5-（2-乙基 - （n） - 己氧基）苯酚的结晶形式公开(公告)号：US08518503B2
公开(公告)日：2013-08-27
申请号：US13330753
申请日：2011-12-20
CPC分类号： C07D251/24 , C08K5/3492 , Y10T428/1345 , Y10T428/1352 , Y10T428/31507 , Y10T428/31786 , Y10T428/31855 , Y10T442/60
摘要： The crystalline form of 2-(4,6-bis-biphenyl-4-yl-1,3,5-triazin-2-yl)-5-(2-ethyl-(n)-hexyloxy)phenol, characterized by a melting range of 118-126° C.
摘要翻译： 2-（4,6-双 - 联苯-4-基-1,3,5-三嗪-2-基）-5-（2-乙基 - （n） - 己氧基）苯酚的结晶形式，其特征在于 熔点118-126℃
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公开(公告)号：USD546757S1
公开(公告)日：2007-07-17
申请号：US29192750
申请日：2003-10-30
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4.发明申请Process for the Oxidation of Secondary Amines into the Corresponding Nitroxides 有权将二胺氧化成相应的硝基氧化物的方法公开(公告)号：US20100305322A1
公开(公告)日：2010-12-02
申请号：US12854677
申请日：2010-08-11
IPC分类号： C07D211/44 , C07D491/113
CPC分类号： C07D491/10 , C07B61/02 , C07D211/94
摘要： The invention relates to a process for the preparation of secondary nitroxide radicals from their corresponding secondary amines by oxidation with an organic peracid, comprising the steps a) adding to a reaction vessel a secondary amine, optionally together with an organic solvent and in one batch a base selected from the group consisting of alkali metal, alkaline earth metal or ammonium bicarbonates and alkaline earth metal or ammonium carbonates or mixtures thereof in the form of a solid together with water or as an aqueous slurry; b) dosing a peracid under stirring to the reaction mixture in an amount of 1.0 to 2.5 mol per mol of secondary amine; and c) isolating the organic phase.
摘要翻译： 本发明涉及通过用有机过酸氧化从其相应的仲胺制备二级氮氧自由基的方法，包括以下步骤：a）向反应容器中加入仲胺，任选与有机溶剂一起加入一次 碱选自碱金属，碱土金属或碳酸氢铵，碱土金属或铵的碳酸盐或其混合物，其形式为水，或与水相混合; b）在搅拌下将过酸给予反应混合物，其量为每摩尔仲胺为1.0至2.5摩尔; 和c）分离有机相。
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5.发明授权公开(公告)号：US08134009B2
公开(公告)日：2012-03-13
申请号：US12854677
申请日：2010-08-11
IPC分类号： C07D211/00 , C07D213/72 , C07D401/00
CPC分类号： C07D491/10 , C07B61/02 , C07D211/94
摘要： The invention relates to a process for the preparation of secondary nitroxide radicals from their corresponding secondary amines by oxidation with an organic peracid, comprising the steps a) adding to a reaction vessel a secondary amine, optionally together with an organic solvent and in one batch a base selected from the group consisting of alkali metal, alkaline earth metal or ammonium bicarbonates and alkaline earth metal or ammonium carbonates or mixtures thereof in the form of a solid together with water or as an aqueous slurry; b) dosing a peracid under stirring to the reaction mixture in an amount of 1.0 to 2.5 mol per mol of secondary amine; and c) isolating the organic phase.
摘要翻译： 本发明涉及通过用有机过酸氧化从其相应的仲胺制备二级氮氧自由基的方法，包括以下步骤：a）向反应容器中加入仲胺，任选与有机溶剂一起加入一次 碱选自碱金属，碱土金属或碳酸氢铵，碱土金属或铵的碳酸盐或其混合物，其形式为水，或与水相混合; b）在搅拌下将过酸给予反应混合物，其量为每摩尔仲胺为1.0至2.5摩尔; 和c）分离有机相。
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6.发明申请Process for the oxidation of secondary amines into the corresponding nitroxides 审中-公开将仲胺氧化成相应的硝基氧的方法公开(公告)号：US20060229452A1
公开(公告)日：2006-10-12
申请号：US10549526
申请日：2004-03-17
IPC分类号： C07D211/40
CPC分类号： C07D491/10 , C07B61/02 , C07D211/94
摘要： The invention relates to a process for the preparation of secondary nitroxide radicals from their corresponding secondary amines by oxidation with an organic peracid, comprising the steps a) adding to a reaction vessel a secondary amine, optionally together with an organic solvent and in one batch a base selected from the group consisting of alkali metal, alkaline earth metal or ammonium bicarbonates and alkaline earth metal or ammonium carbonates or mixtures thereof in the form of a solid together with water or as an aqueous slurry; b) dosing a peracid under stirring to the reaction mixture in an amount of 1.0 to 2.5 mol per mol of secondary amine; and c) isolating the organic phase.
摘要翻译： 本发明涉及通过用有机过酸氧化从其相应的仲胺制备二级氮氧自由基的方法，包括以下步骤：a）向反应容器中加入仲胺，任选与有机溶剂一起加入一次 碱选自碱金属，碱土金属或碳酸氢铵，碱土金属或铵的碳酸盐或其混合物，其形式为水，或与水相混合; b）在搅拌下将过酸给予反应混合物，其量为每摩尔仲胺为1.0至2.5摩尔; 和c）分离有机相。
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