公开(公告)号：US20230226509A1

公开(公告)日：2023-07-20

申请号：US17919617

申请日：2021-04-19

Applicant: HTE GMBH THE HIGH THROUGHPUT EXPERIMENTATION COMPANY

Inventor： Marius Kirchmann ,  Kurt-Erich Finger ,  Markus Friess

IPC: B01J8/18 ,  B01J8/22 ,  B01J8/00 ,  G01N31/10 ,  C10G11/18 ,  B01D45/08

CPC classification number: B01J8/1809 ,  B01D45/08 ,  B01J8/0065 ,  B01J8/228 ,  B01J8/1863 ,  B01J8/1881 ,  C10G11/187 ,  G01N31/10 ,  B01J2208/00539 ,  B01J2208/00628

Abstract: The invention relates to an apparatus for analyzing heterogeneously catalyzed reactions comprising at least one reactor (3) through which a particulate catalyst flows and at least one reactant feed, wherein arranged downstream of each reactor (3) is a separation apparatus (17) for separating the particulate catalyst from a reaction product comprising condensable gases and arranged downstream of the separation apparatus (17) is a liquid separator (31) for separating liquid constituents from the reaction product, wherein the liquid separator (31) comprises a metallic tube (103) and a deflection body (119), wherein the metallic tube (103) is closed at its ends and the deflection body (119) is accommodated in the metallic tube (103) and the metallic tube (103) comprises a side feed (135) at a first end (105) and a gas outlet (113) at a second end (107) and the gas outlet (113) is connected to at least one sample vessel (37). The invention further relates to a process for analyzing heterogeneously catalyzed reactions in the apparatus.

公开(公告)号：US11207652B2

公开(公告)日：2021-12-28

申请号：US16631270

申请日：2018-07-25

Applicant: hte GmbH the high throughput experimentation company

Inventor： Josef Find ,  Kurt-Erich Finger ,  Markus Friess

IPC: B01J8/18 ,  B01J8/24 ,  C10G11/18

Abstract: Disclosed herein is an apparatus and a method for catalytic conversion of chemical substances in the presence of pulverulent catalysts in a trickle bed reactor with residence times in the range of 0.1-10 seconds, wherein the apparatus includes a trickle bed reactor (2), the inlet side of which is functionally connected to a catalyst reservoir vessel (1) and a reactant feed, and the outlet side of which is functionally connected to a separator (3). The separator (3) has an exit conduit for leading off product stream, wherein the apparatus has the characteristic feature that the exit conduit disposed on the separator (3) for leading off product stream has a continuously acting valve connected via a controller to a pressure measurement sensor, wherein the continuously acting valve and the pressure measurement sensor form a pressure control circuit with a controller.

公开(公告)号：US20210379553A1

公开(公告)日：2021-12-09

申请号：US17286320

申请日：2019-10-15

Applicant: hte GmbH the high throughput experimentation company

Inventor： Marius Kirchmann ,  Christoph Hauber ,  Edgar Jordan ,  Kurt-Erich Finger ,  Markus Friess ,  Oliver Koechel

IPC: B01J19/00 ,  G01N1/14 ,  G01N1/24

Abstract: The invention relates to an apparatus for analyzing reactions, comprising at least one reactor (1) and at least two sample vessels (13), wherein, in the case of an apparatus having one reactor (1), the reactor (1) is connected to at least two sample vessels (13), and, in the case of an apparatus having more than one reactor (1), each reactor (1) is connected to at least one sample vessel (13). The invention further relates to a method of analyzing reactions in such an apparatus.

公开(公告)号：US20230211266A1

公开(公告)日：2023-07-06

申请号：US17915770

申请日：2021-03-30

Applicant: HTE GMBH THE HIGH THROUGHPUT EXPERIMENTATION COMPANY

Inventor： Oliver Koechel ,  Markus Friess ,  Kurt-Erich Finger ,  Josef Find

IPC: B01D45/08 ,  B01D45/02 ,  B01D46/00 ,  B01D39/20 ,  G01N5/04

CPC classification number: B01D45/08 ,  B01D39/2017 ,  B01D45/02 ,  B01D46/0005 ,  B01D46/0031 ,  G01N5/04 ,  B01D2271/027 ,  B01D2277/30

Abstract: The invention relates to a separation unit for separating off liquid components from a gas stream comprising liquid components, the separation unit (1) comprising a metallic tube (3) and a baffler (19), the metallic tube (3) having a first end (5) and a second end (7) and being closed at the first and second ends (5, 7), the baffler (19) being placed inside the metallic tube (3), the metallic tube (3) having a side feed (35) at the first end (5) and a gas outlet (13) at the second end (7). The invention further relates to the use of the separation unit and a process for determining the amount of liquid components in a two phase stream comprising a gaseous phase and liquid components.

公开(公告)号：US10562050B2

公开(公告)日：2020-02-18

申请号：US15565594

申请日：2016-04-13

Applicant: hte GmbH the high throughput experimentation company

Inventor： Josef Find ,  Kurt-Erich Finger ,  Alfred Haas ,  Markus Friess ,  Oliver Koechel ,  Michael Dejmek

IPC: B05B7/04 ,  B05B7/16 ,  B01J4/00 ,  B01J8/18

Abstract: An apparatus and process for spraying liquids and producing very fine mist with the apparatus, the apparatus including: a needle injector that includes a capillary line (1) and an outer tube (8); a liquid supply (5); and a gas supply (4), where: the capillary line (1) is arranged in the interior space of the outer tube (2); the internal diameter of the capillary line in the needle injector is in the range of 2-1000 μm; the capillary line is in active communication with a gas supply (4); and the outer tube (2) is in active communication with a liquid supply (5).