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    OPTIMIZED SEPARATION TECHNIQUE FOR WORK-UP OF HOMOGENEOUSLY CATALYSED HYDROFORMYLATION MIXTURES
    1.
    发明申请
    OPTIMIZED SEPARATION TECHNIQUE FOR WORK-UP OF HOMOGENEOUSLY CATALYSED HYDROFORMYLATION MIXTURES 有权
    用于均相催化水解混合物的优化分离技术

    公开(公告)号：US20160002136A1

    公开(公告)日：2016-01-07

    申请号：US14770525

    申请日：2014-02-13

    申请人： Hans-Gerd LUEKEN ,  Bart HAMERS ,  Dirk FRIDAG ,  Robert FRANKE ,  Markus PRISKE ,  Dieter HESS ,  Marc BECKER ,  Markus RUDEK

    发明人： Hans-Gerd LUEKEN ,  Bart HAMERS ,  Dirk FRIDAG ,  Robert FRANKE ,  Markus PRISKE ,  Dieter HESS ,  Marc BECKER ,  Markus RUDEK

    IPC分类号： C07C45/78 ,  C07C29/16 ,  C07C45/81 ,  B01J19/00 ,  C07C45/50

    CPC分类号： C07C45/786 ,  B01D61/02 ,  B01D2311/25 ,  B01D2317/025 ,  B01D2325/30 ,  B01D2325/38 ,  B01J19/00 ,  B01J31/185 ,  B01J2231/321 ,  B01J2531/822 ,  C07C29/16 ,  C07C45/50 ,  C07C45/81 ,  C07C45/82 ,  C07C31/02 ,  C07C31/125 ,  C07C47/02

    摘要： The invention relates to a method for producing alcohols by homogeneously catalysed hydroformylation of olefins to aldehydes and subsequent hydration of the aldehydes. The invention further relates to a system for carrying out the method. The main focus is on the separation technique for work-up of the hydroformylation mixture. The problem addressed by the invention is that specifying a work-up method for hydroformylation mixtures that utilises the specific advantages of known separation technologies but at the same time largely avoids the specific disadvantages of said separation technologies. The most important objective is to create a catalyst separation system that is as complete and at the same time conservative as possible and that operates in a technically reliable manner and entails low investment and operating costs. The method should be unrestrictedly suitable for processing the reaction output from oxo systems in “world scale” format. The problem is solved by combining membrane separation units and a thermal separation unit, the thermal separation unit being operated in such a manner that 80% to 98% of the mass introduced with the product stream into the thermal separation unit exits the thermal separation unit again as a head product.

    摘要翻译： 本发明涉及通过将烯烃均匀催化加氢甲酰化成醛并随后醛的水合生产醇的方法。 本发明还涉及一种用于执行该方法的系统。 主要关注加氢甲酰化混合物后处理的分离技术。 本发明解决的问题是指定利用已知分离技术的具体优点但同时大大地避免了所述分离技术的具体缺点的加氢甲酰化混合物的后处理方法。 最重要的目标是创建一个尽可能完整且同时保守的催化剂分离系统，并以技术上可靠的方式运行，并且需要低投资和运营成本。 该方法不受限制地适用于以“世界规模”格式处理氧代系统的反应输出。 通过组合膜分离单元和热分离单元来解决问题，热分离单元以使得进入热分离单元的产物流引入的质量的80％至98％再次离开热分离单元的方式操作 作为头饰产品。

    SEPARATION OF HOMOGENEOUS CATALYSTS BY MEANS OF A MEMBRANE SEPARATION UNIT UNDER CLOSED-LOOP CONTROL
    2.
    发明申请
    SEPARATION OF HOMOGENEOUS CATALYSTS BY MEANS OF A MEMBRANE SEPARATION UNIT UNDER CLOSED-LOOP CONTROL 审中-公开
    在闭环控制下通过膜分离单元分离均相催化剂

    公开(公告)号：US20160082393A1

    公开(公告)日：2016-03-24

    申请号：US14890821

    申请日：2014-04-17

    申请人： Markus PRISKE ,  Bart HAMERS ,  Dirk FRIDAG ,  Robert FRANKE ,  Markus RUDEK ,  Hans-Gerd LUEKEN ,  EVONIK DEGUSSA GMBH

    发明人： Markus PRISKE ,  Bart HAMERS ,  Dirk FRIDAG ,  Robert FRANKE ,  Markus RUDEK ,  Hans-Gerd LUEKEN

    IPC分类号： B01D61/36

    CPC分类号： B01D61/36 ,  B01D2311/14 ,  B01D2311/2696 ,  B01J31/4046 ,  B01J31/4061

    摘要： The invention relates to a method for separating a homogeneous catalyst out of a reaction mixture by means of at least one membrane separation unit, in which method: the reaction mixture coming from a reaction zone and containing the homogeneous catalyst is applied as a feed to the membrane separation unit; the homogeneous catalyst is depleted in the permeate of the membrane separation unit and enriched in the retentate of the membrane separation unit; and the retentate of the membrane separation unit is recirculated into the reaction zone. The invention addresses the problem of specifying a method for separating homogeneous catalyst out of reaction mixtures that simplifies the feeding of fresh catalyst into the reaction zone and avoids disruptions to the hydrodynamics within the reaction zone when the volumetric flow of the reaction mixture output from the reaction zone varies. This problem is solved in that both the retentate volumetric flow of the membrane separation unit and the retention of the membrane separation unit are kept constant by regulation.

    摘要翻译： 本发明涉及一种通过至少一个膜分离单元从反应混合物中分离均相催化剂的方法，其中将来自反应区并含有均相催化剂的反应混合物作为进料施加到 膜分离单元; 均质催化剂耗尽膜分离单元的渗透物并富集膜分离单元的渗余物; 并且膜分离单元的滞留物再循环到反应区中。 本发明解决了从反应混合物中分离均相催化剂的方法的问题，其简化了将新鲜催化剂进料到反应区中，并且当反应物从反应物输出的体积流量反应时避免了反应区内的流体动力学破坏 区域不一。 这个问题的解决在于膜分离单元的滞留体积流量和膜分离单元的保持率通过调节保持恒定。