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1.发明授权Method of decreasing unreacted monomer in vinyl polymer and a toner resin in which unreacted monomer has been decreased 有权降低乙烯基聚合物中未反应单体的方法和其中未反应单体已降低的调色剂树脂公开(公告)号：US06627681B1
公开(公告)日：2003-09-30
申请号：US09913882
申请日：2001-08-16
申请人： Hikoji Ueda , Masamitsu Mogi , Masao Watanabe , Yutaka Kukimoto
发明人： Hikoji Ueda , Masamitsu Mogi , Masao Watanabe , Yutaka Kukimoto
IPC分类号： C08K330
CPC分类号： C08F6/003 , G03G9/0815 , G03G9/08702
摘要： The method of decreasing unreacted monomer in vinyl polymer of the present invention is a method comprising adding a water-soluble inorganic salt that is able to solubilize unreacted monomer contained in vinyl polymer to an aqueous dispersion in which particles of vinyl polymer are dispersed in an aqueous medium, followed by solubilizing the unreacted monomer and removing the unreacted monomer together with the aqueous medium. According to this method, the amount of unreacted monomer present in a polymer can be efficiently and reliably decreased at low cost without requiring a special apparatus or thermal energy, etc. In addition, the toner resin of the present invention has for its constituent component a vinyl polymer in which the amount of unreacted monomer has been decreased by the method described above. In addition to solving the problem of a foul odor being generated during toner production and fixation when copying, the vinyl polymer obtained according to the method of the present invention also has superior effects such as contributing to improvement of toner characteristics.
摘要翻译： 降低本发明的乙烯基聚合物中未反应单体的方法是一种方法，包括将能够将乙烯基聚合物中所含的未反应单体溶解到水分散体中的水溶性无机盐，其中乙烯基聚合物颗粒分散在水性 然后溶解未反应的单体并与水性介质一起除去未反应的单体。 根据该方法，可以以低成本高效可靠地降低存在于聚合物中的未反应单体的量，而不需要特殊设备或热能等。另外，本发明的调色剂树脂的组成成分a 通过上述方法使未反应单体的量减少的乙烯基聚合物。 除了解决在复制时调色剂生产和固色期间产生的恶臭的问题，根据本发明的方法获得的乙烯基聚合物还具有优异的效果，例如有助于改善调色剂特性。
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公开(公告)号：US5317060A
公开(公告)日：1994-05-31
申请号：US983129
申请日：1992-11-30
申请人： Yutaka Kukimoto , Hikoji Ueda , Kozo Suzuki , Yoshihiko Koshiyama
发明人： Yutaka Kukimoto , Hikoji Ueda , Kozo Suzuki , Yoshihiko Koshiyama
CPC分类号： G03G9/0812 , C08L25/14 , G03G9/0804 , C08L2205/02 , G03G9/081
摘要： A process for producing a composite resin for a toner, comprising the steps of: mixing, in water, (a) a low-molecular weight polymer powder comprising particles, not less than 80% by weight of the particles having a diameter of from 20 to 2000 microns with (b) a high-molecular weight polymer emulsion; subjecting the thus obtained mixture to a coagulation treatment; and heating the resulting mixture to obtain a composite resin in which the low-molecular weight polymer particle and the high-molecular weight polymer are fixed and homogeneously mixed with each other.
摘要翻译： 一种制备用于调色剂的复合树脂的方法，包括以下步骤：在水中混合（a）包含颗粒的低分子量聚合物粉末，其不小于直径为20的颗粒的80重量％ （b）高分子量聚合物乳液; 对由此获得的混合物进行凝固处理; 加热得到的混合物，得到低分子量聚合物粒子和高分子量聚合物固定并均匀混合的复合树脂。
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3.发明申请Negative charge controlling agent and static charge image developing toner using the same, and method for producing the same 有权负电荷控制剂和使用其的静电荷图像显影调色剂及其制造方法公开(公告)号：US20060083999A1
公开(公告)日：2006-04-20
申请号：US10542589
申请日：2004-01-21
IPC分类号： C07C39/12
CPC分类号： C07C37/20 , C07C37/115 , C07C2601/14 , G03G9/08746 , G03G9/08748 , G03G9/08762 , G03G9/08795 , G03G9/08797 , G03G9/09733 , G03G9/0975 , C07C39/16 , C07C39/15 , C07C39/17
摘要： A negative charge controlling agent, wherein: the negative charge controlling agent comprises polycondensation product obtained by a polycondensation reaction of phenols and aldehydes; and the phenols comprises a (A) mononucleus phenolic compound which has one phenolic hydroxy group in which a hydrogen is bonded at the ortho position of a hydroxyl group of the phenolic hydroxy group and a (B) multinucleus phenolic compound which has at least two phenolic hydroxy groups in which a hydrogen is bonded at the ortho position of a hydroxyl group of each of the phenolic hydroxy group; and the content of the (B) phenolic compound in the phenols is 1 to 30 mol %.
摘要翻译： 负电荷控制剂，其中：负电荷控制剂包括通过酚和醛的缩聚反应获得的缩聚产物; 酚类包括（A）单酚酚类化合物，其具有一个酚羟基，其中氢在酚羟基的羟基的邻位键合，以及具有至少两个酚的（B）多核酚类化合物 在每个酚羟基的羟基的邻位键合有氢的羟基; 苯酚中的（B）酚类化合物的含量为1〜30摩尔％。
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4.发明授权Negative charge controlling agent and static charge image developing toner using the same, and method for producing the same 有权负电荷控制剂和使用其的静电荷图像显影调色剂及其制造方法公开(公告)号：US08658339B2
公开(公告)日：2014-02-25
申请号：US10542589
申请日：2004-01-21
IPC分类号： G03G9/08
CPC分类号： C07C37/20 , C07C37/115 , C07C2601/14 , G03G9/08746 , G03G9/08748 , G03G9/08762 , G03G9/08795 , G03G9/08797 , G03G9/09733 , G03G9/0975 , C07C39/16 , C07C39/15 , C07C39/17
摘要： A negative charge controlling agent, wherein: the negative charge controlling agent comprises polycondensation product obtained by a polycondensation reaction of phenols and aldehydes; and the phenols comprises a (A) mononucleus phenolic compound which has one phenolic hydroxy group in which a hydrogen is bonded at the ortho position of a hydroxyl group of the phenolic hydroxy group and a (B) multinucleus phenolic compound which has at least two phenolic hydroxy groups in which a hydrogen is bonded at the ortho position of a hydroxyl group of each of the phenolic hydroxy group; and the content of the (B) phenolic compound in the phenols is 1 to 30 mol %.
摘要翻译： 负电荷控制剂，其中：负电荷控制剂包括通过酚和醛的缩聚反应获得的缩聚产物; 酚类包括（A）单酚酚类化合物，其具有一个酚羟基，其中氢在酚羟基的羟基的邻位键合，以及具有至少两个酚的（B）多核酚类化合物 在每个酚羟基的羟基的邻位键合有氢的羟基; 苯酚中的（B）酚类化合物的含量为1〜30摩尔％。
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