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    REMOVAL METHOD OF MANGANESE FROM WASTE WATER
    1.
    发明申请
    REMOVAL METHOD OF MANGANESE FROM WASTE WATER 有权
    从废水中去除锰的方法

    公开(公告)号：US20110163042A1

    公开(公告)日：2011-07-07

    申请号：US12999017

    申请日：2010-02-23

    申请人： Hiroshi Kobayashi ,  Norihisa Toki ,  Hirofumi Shoji ,  Keiji Kudo ,  Tatsuya Higaki

    发明人： Hiroshi Kobayashi ,  Norihisa Toki ,  Hirofumi Shoji ,  Keiji Kudo ,  Tatsuya Higaki

    IPC分类号： C02F1/64 ,  C02F1/52

    CPC分类号： C22B23/043 ,  C02F1/5227 ,  C02F1/74 ,  C02F2101/20 ,  C02F2101/206 ,  C02F2209/04 ,  C02F2209/06 ,  C22B3/44 ,  C22B7/006 ,  C22B23/0461 ,  C22B47/00 ,  C22B47/0045 ,  Y02P10/234

    摘要： A removal method of manganese in which manganese is removed by precipitating manganese selectively from sulfuric acid waste water containing aluminum, magnesium and manganese with inhibiting the precipitation of magnesium.The removal method of manganese from waste water in which manganese is removed by precipitating manganese selectively from the sulfuric acid waste water containing aluminum, magnesium and manganese with inhibiting the precipitation of magnesium, characterized in that said waste water is subjected to the following steps (1) and (2).(1) First, aluminum in said waste water is removed.(2) Subsequently, neutralizing agent is added into the wastewater after removing aluminum, then pH of the waste water is adjusted at 8.0 to 9.0, and oxygen gas is blown.

    摘要翻译： 锰的去除方法，其中通过从含有铝，镁和锰的硫酸废水中选择性地沉淀锰来除去锰，并抑制镁的析出。 通过从含有铝，镁和锰的硫酸废水中选择性地沉淀锰来除去锰的废水中的锰的去除方法，其中抑制镁的沉淀，其特征在于所述废水经受以下步骤（1 ）和（2）。 （1）首先，除去所述废水中的铝。 （2）随后，在除去铝之后，将中和剂加入到废水中，然后将废水的pH调节至8.0-9.0，并吹入氧气。

    Method for recovering nickel from sulfuric acid aqueous solution
    5.
    发明授权
    Method for recovering nickel from sulfuric acid aqueous solution 有权
    从硫酸水溶液中回收镍的方法

    公开(公告)号：US08580213B2

    公开(公告)日：2013-11-12

    申请号：US13057683

    申请日：2010-02-02

    申请人： Hiroshi Kobayashi ,  Hirofumi Shoji ,  Norihisa Toki ,  Keiji Kudo ,  Tatsuya Higaki

    发明人： Hiroshi Kobayashi ,  Hirofumi Shoji ,  Norihisa Toki ,  Keiji Kudo ,  Tatsuya Higaki

    IPC分类号： B01D11/00

    CPC分类号： C01G45/003 ,  C01G51/003 ,  C01G51/04 ,  C01G53/003 ,  C01G53/04 ,  C22B3/44 ,  C22B23/043 ,  C22B23/0461 ,  Y02P10/234

    摘要： A method for recovering nickel from sulfuric acid aqueous solution, for recovering nickel in an effectively utilizable form as a raw material of nickel industry material, by separating efficiently impurity elements of iron, aluminum, manganese, etc., from the sulfuric acid aqueous solution containing nickel and cobalt, and the impurity elements, iron, aluminum, manganese, etc. The method comprises the following steps: subject the sulfuric acid aqueous solution to oxidation neutralization treatment; then subject the solution to neutralization treatment, and separate and recover mixed hydroxides containing nickel and cobalt; subject the mixed hydroxides to dissolution treatment in a sulfuric acid solution having a concentration of equal to or higher than 50% by mass; subject the concentrated solution to solvent extraction treatment, using a phosphate ester-based acidic extraction agent; add a neutralizing agent to the resultant extraction residual liquid; subject the solution to the neutralization treatment, and separate and recover nickel hydroxide generated.

    摘要翻译： 一种从硫酸水溶液中回收镍的方法，用于以有效利用的形式回收镍作为镍工业材料的原料，通过将铁，铝，锰等的杂质元素从含有 镍和钴，以及杂质元素，铁，铝，锰等。该方法包括以下步骤：将硫酸水溶液进行氧化中和处理; 然后对溶液进行中和处理，分离回收含镍和钴的混合氢氧化物; 将混合氢氧化物溶解在浓度等于或高于50质量％的硫酸溶液中; 采用浓缩溶液进行溶剂萃取处理，使用磷酸酯类酸性提取剂; 向所得萃取残余液体中加入中和剂; 对溶液进行中和处理，并分离并回收生成的氢氧化镍。

    METHOD FOR RECOVERING NICKEL FROM SULFURIC ACID AQUEOUS SOLUTION
    6.
    发明申请
    METHOD FOR RECOVERING NICKEL FROM SULFURIC ACID AQUEOUS SOLUTION 有权
    从硫酸水溶液中回收镍的方法

    公开(公告)号：US20110135547A1

    公开(公告)日：2011-06-09

    申请号：US13057683

    申请日：2010-02-02

    申请人： Hiroshi Kobayashi ,  Hirofumi Shoji ,  Norihisa Toki ,  Keiji Kudo ,  Tatsuya Higaki

    发明人： Hiroshi Kobayashi ,  Hirofumi Shoji ,  Norihisa Toki ,  Keiji Kudo ,  Tatsuya Higaki

    IPC分类号： C01G53/04 ,  C01G51/04 ,  C01G51/00

    CPC分类号： C01G45/003 ,  C01G51/003 ,  C01G51/04 ,  C01G53/003 ,  C01G53/04 ,  C22B3/44 ,  C22B23/043 ,  C22B23/0461 ,  Y02P10/234

    摘要： A method for recovering nickel from an sulfuric acid aqueous solution, for recovering nickel in an effectively utilizable form as a raw material of nickel industry material, by separating efficiently impurity elements of iron, aluminum, manganese and the like, from the sulfuric acid aqueous solution containing nickel and cobalt, and the impurity elements, iron, aluminum, manganese and the like.The method is characterized by comprising the following steps (1) to (5). step (1): to subject the sulfuric acid aqueous solution to oxidation neutralization treatment. step (2): then, to subject the solution to neutralization treatment, and to separate and recover mixed hydroxides containing nickel and cobalt. step (3): to subject the mixed hydroxides to dissolution treatment in a sulfuric acid solution having a concentration of equal to or higher than 50% by mass. step (4): to subject the concentrated solution to solvent extraction treatment, using a phosphate ester-based acidic extraction agent. step (5): by adding a neutralizing agent to the resultant extraction residual liquid, to subject the solution to the neutralization treatment, and to separate and recover nickel hydroxide generated.

    摘要翻译： 从硫酸水溶液中回收镍的方法，通过从硫酸水溶液中有效地分离出铁，铝，锰等的杂质元素，以镍工业材料的原料回收镍，以有效利用的形式回收镍 含有镍和钴，以及杂质元素，铁，铝，锰等。 该方法的特征在于包括以下步骤（1）至（5）。 步骤（1）：使硫酸水溶液进行氧化中和处理。 步骤（2）：然后，使溶液进行中和处理，并分离和回收含有镍和钴的混合氢氧化物。 步骤（3）：使混合氢氧化物在浓度等于或高于50质量％的硫酸溶液中进行溶解处理。 步骤（4）：使用浓缩溶液进行溶剂萃取处理，使用磷酸酯基酸性提取剂。 步骤（5）：通过向所得到的萃取残留液中加入中和剂，使溶液进行中和处理，分离并回收生成的氢氧化镍。