公开(公告)号：US20110318053A1

公开(公告)日：2011-12-29

申请号：US13163958

申请日：2011-06-20

申请人： Hiroshi Yamashita ,  Yuichi Shirasu ,  Masaki Watanabe ,  Tomoki Murayama

发明人： Hiroshi Yamashita ,  Yuichi Shirasu ,  Masaki Watanabe ,  Tomoki Murayama

IPC分类号： G03G15/01 ,  G03G9/093

CPC分类号： G03G15/0126 ,  G03G9/0804 ,  G03G9/09733 ,  G03G2215/0129

摘要： A method for producing an electrophotographic toner including forming a toner base particle by emulsifying or dispersing a solution or dispersion of a toner material comprising a colorant, and any one of a binder resin and a binder resin precursor in an aqueous medium, and adding crystalline organic fine particles having an acid value of 20 mgKOH/g to 80 mgKOH/g into the aqueous medium, before, during or after the forming so as to attach the crystalline organic fine particles onto a surface of the toner base particle.

摘要翻译： 一种电子照相调色剂的制造方法，包括通过将包含着色剂的调色剂材料和任何一种粘合剂树脂和粘合剂树脂前体的溶液或分散体乳化或分散在水性介质中形成调色剂基础颗粒并加入结晶有机物 在形成之前，期间或之后，在水性介质中酸值为20mgKOH / g至80mgKOH / g的细颗粒，以将结晶有机细颗粒附着在调色剂基础颗粒的表面上。

公开(公告)号：US08603719B2

公开(公告)日：2013-12-10

申请号：US13163958

申请日：2011-06-20

申请人： Hiroshi Yamashita ,  Yuichi Shirasu ,  Masaki Watanabe ,  Tomoki Murayama

发明人： Hiroshi Yamashita ,  Yuichi Shirasu ,  Masaki Watanabe ,  Tomoki Murayama

IPC分类号： G03G9/08

CPC分类号： G03G15/0126 ,  G03G9/0804 ,  G03G9/09733 ,  G03G2215/0129

摘要： A method for producing an electrophotographic toner including forming a toner base particle by emulsifying or dispersing a solution or dispersion of a toner material comprising a colorant, and any one of a binder resin and a binder resin precursor in an aqueous medium, and adding crystalline organic fine particles having an acid value of 20 mgKOH/g to 80 mgKOH/g into the aqueous medium, before, during or after the forming so as to attach the crystalline organic fine particles onto a surface of the toner base particle.

摘要翻译： 一种电子照相调色剂的制造方法，包括通过将包含着色剂的调色剂材料和任何一种粘合剂树脂和粘合剂树脂前体的溶液或分散体乳化或分散在水性介质中形成调色剂基础颗粒并加入结晶有机物 在形成之前，期间或之后，在水性介质中酸值为20mgKOH / g至80mgKOH / g的细颗粒，以将结晶有机细颗粒附着在调色剂基础颗粒的表面上。

公开(公告)号：US20130164669A1

公开(公告)日：2013-06-27

申请号：US13819843

申请日：2011-08-18

申请人： Hiroshi Yamashita ,  Yuichi Shirasu ,  Tomoki Murayama ,  Masaki Watanabe

发明人： Hiroshi Yamashita ,  Yuichi Shirasu ,  Tomoki Murayama ,  Masaki Watanabe

IPC分类号： G03G9/087 ,  G03G9/08

CPC分类号： C08G63/916 ,  G03G9/0804 ,  G03G9/0819 ,  G03G9/08755 ,  G03G9/08782 ,  G03G9/08795 ,  G03G9/08797

摘要： A toner including a binder resin containing an ester bond, and a releasing agent, wherein the releasing agent includes first C30-C50 alkyl monoester compound and second C30-C50 alkyl monoester compound, wherein the number of carbon atoms of the first C30-C50 alkyl monoester compound is different from that of the second C30-C50 alkyl monoester compound, wherein the amount of the first C30-C50 alkyl monoester compound is largest and the amount of the second C30-C50 alkyl monoester compound is second largest or same as the amount of the first C3OC50 alkyl monoester compound, wherein the amount of the first C30-C50 alkyl monoester compound is 30% by mass or more but less than 50% by mass to the releasing agent, and wherein the amount of the second C30-C50 alkyl monoester compound is 10% by mass or more but less than 50% by mass to the releasing agent.

摘要翻译： 包含含有酯键的粘合剂树脂的调色剂和脱模剂，其中所述脱模剂包括第一C30-C50烷基单酯化合物和第二C30-C50烷基单酯化合物，其中第一C30-C50烷基的碳原子数 单酯化合物与第二C30-C50烷基单酯化合物不同，其中第一C30-C50烷基单酯化合物的量最大，第二C30-C50烷基单酯化合物的量为第二C30- 的第一C 3 -C 50烷基单酯化合物，其中第一C 30 -C 50烷基单酯化合物的量相对于脱模剂为30质量％以上且小于50质量％，其中第二C30〜C50烷基单酯化合物的量为 单酯化合物相对于脱模剂为10质量％以上且小于50质量％。

公开(公告)号：US08735037B2

公开(公告)日：2014-05-27

申请号：US13635453

申请日：2011-03-16

申请人： Hiroshi Yamashita ,  Masaki Watanabe ,  Tomoki Murayama

发明人： Hiroshi Yamashita ,  Masaki Watanabe ,  Tomoki Murayama

IPC分类号： G03G9/087

CPC分类号： G03G9/0825 ,  G03G9/0806 ,  G03G9/0827 ,  G03G9/08755 ,  G03G9/08795 ,  G03G9/08797

摘要： A toner obtained by a method for producing a toner, which includes dissolving or dispersing in an organic solvent a toner material containing at least a binder resin, and a dispersion liquid of a crystalline polyester resin, so as to prepare a solution or dispersion liquid of the toner material, emulsifying or dispersing the solution or dispersion liquid of the toner material in an aqueous medium, so as to prepare an emulsion or dispersion liquid, and removing the organic solvent from the emulsion or dispersion liquid, wherein the crystalline polyester resin is localized near a surface of the toner.

摘要翻译： 通过调色剂的制造方法得到的调色剂，其特征在于，将包含至少含有粘结剂树脂的调色剂材料和结晶性聚酯树脂的分散液溶解或分散在有机溶剂中，以制备溶液或分散液 调色剂材料，将调色剂材料的溶液或分散液乳化或分散在水性介质中，以制备乳液或分散液，并从乳液或分散液中除去有机溶剂，其中结晶聚酯树脂定位 靠近调色剂的表面。

公开(公告)号：US20130011779A1

公开(公告)日：2013-01-10

申请号：US13635453

申请日：2011-03-16

申请人： Hiroshi Yamashita ,  Masaki Watanabe ,  Tomoki Murayama

发明人： Hiroshi Yamashita ,  Masaki Watanabe ,  Tomoki Murayama

IPC分类号： G03G9/087 ,  B82Y30/00

CPC分类号： G03G9/0825 ,  G03G9/0806 ,  G03G9/0827 ,  G03G9/08755 ,  G03G9/08795 ,  G03G9/08797

摘要： A toner obtained by a method for producing a toner, which includes dissolving or dispersing in an organic solvent a toner material containing at least a binder resin, and a dispersion liquid of a crystalline polyester resin, so as to prepare a solution or dispersion liquid of the toner material, emulsifying or dispersing the solution or dispersion liquid of the toner material in an aqueous medium, so as to prepare an emulsion or dispersion liquid, and removing the organic solvent from the emulsion or dispersion liquid, wherein the crystalline polyester resin is localized near a surface of the toner.

摘要翻译： 通过调色剂的制造方法得到的调色剂，其特征在于，将包含至少含有粘结剂树脂的调色剂材料和结晶性聚酯树脂的分散液溶解或分散在有机溶剂中，以制备溶液或分散液 调色剂材料，将调色剂材料的溶液或分散液乳化或分散在水性介质中，以制备乳液或分散液，并从乳液或分散液中除去有机溶剂，其中结晶聚酯树脂定位 靠近调色剂的表面。

公开(公告)号：US09201326B2

公开(公告)日：2015-12-01

申请号：US13729926

申请日：2012-12-28

申请人： Ryuuta Yoshida ,  Takahiro Honda ,  Junichi Awamura ,  Osamu Uchinokura ,  Masaki Watanabe ,  Daisuke Inoue ,  Tomoki Murayama ,  Mamoru Hozumi

发明人： Ryuuta Yoshida ,  Takahiro Honda ,  Junichi Awamura ,  Osamu Uchinokura ,  Masaki Watanabe ,  Daisuke Inoue ,  Tomoki Murayama ,  Mamoru Hozumi

IPC分类号： G03G9/087 ,  G03G9/08

CPC分类号： G03G9/08755 ,  G03G9/0802 ,  G03G9/08782 ,  G03G9/08797

摘要： A toner including: a binder resin containing a non-crystalline resin and a crystalline resin; a colorant; and, a releasing agent, wherein the releasing agent has a melting point of 55° C. to 80° C., and wherein the toner satisfies the following Expressions 1 and 2: (Expression 1): 20,000 Pa·s≦G1≦50,000 Pa·s; and (Expression 2): (G4/G2)/(G3/G1) 1.00, where G1 is a storage modulus, G2 is a loss modulus, G3 is a storage modulus and G4 is a loss modulus, and the storage modulus G1 and the loss modulus G2 are measured at 80° C. when the toner is heated from 70° C. to 150° C. and the storage modulus G3 and the loss modulus G4 are measured at 80° C. when the toner heated to 150° C. is cooled to 70° C.

摘要翻译： 一种调色剂，包括：含有非结晶性树脂和结晶性树脂的粘合剂树脂; 着色剂 和脱模剂，其中所述脱模剂的熔点为55℃至80℃，并且其中所述调色剂满足以下表达式1和2：（表达式1）：20,000Pa·s＆nlE; G1＆nlE; 50,000 Pa·s; 和（表达式2）：（G4 / G2）/（G3 / G1）1.00其中G1是储能模量，G2是损耗模量，G3是储能模量，G4是损耗模量，储能模量G1和 当调色剂从70℃加热至150℃时，在80℃下测量损耗模量G2，并且当调色剂加热至150°C时，在80℃下测量储能模量G3和损耗模量G4 C.冷却至70℃

公开(公告)号：US08614043B2

公开(公告)日：2013-12-24

申请号：US13666332

申请日：2012-11-01

申请人： Masaki Watanabe ,  Osamu Uchinokura ,  Junichi Awamura ,  Takahiro Honda ,  Satoshi Ogawa ,  Tsuneyasu Nagatomo ,  Hiroshi Yamashita

发明人： Masaki Watanabe ,  Osamu Uchinokura ,  Junichi Awamura ,  Takahiro Honda ,  Satoshi Ogawa ,  Tsuneyasu Nagatomo ,  Hiroshi Yamashita

IPC分类号： G03G9/087

CPC分类号： G03G9/0825 ,  G03G9/09314 ,  G03G9/09321 ,  G03G9/09328 ,  G03G9/09392

摘要： A toner including a core particle, an inner shell layer covering the core, and an outer shell layer covering the inner shell layer is provided. The core particle includes a resin P. The inner shell layer includes fine particles of a resin A. The outer shell layer includes fine particles of a resin B. The toner satisfies the following formulae (1) to (3): 4.5≦T½(P)−Tfb(P)≦14  (1) 20≦T½(A)−Tfb(A)≦40  (2) 23.5≦T½(B)−Tfb(B)≦40  (3) wherein T½(P), T½(A), and T½(B) represent ½ method temperatures of the resins P, A, and B, respectively, and Tfb(P), Tfb(A), and Tfb(B) represent flow beginning temperatures of the resins P, A, and B, respectively, and wherein the ½ method temperatures and the flow beginning temperatures are measured by a flowtester.

摘要翻译： 提供了包括芯颗粒，覆盖芯的内壳层和覆盖内壳层的外壳层的调色剂。 核心颗粒包括树脂P.内壳层包括树脂A的细颗粒。外壳层包括树脂B的细颗粒。调色剂满足下式（1）至（3）：4.5@T 1/2（ P）-Tfb（P）@ 14（1）20 @ T 1/2（A）-Tfb（A）@ 40（2）23.5@T½（B）-Tfb（B）@ 40（3） T 1/2（A）和T 1/2（B）分别表示树脂P，A和B的1/2方法温度，Tfb（P），Tfb（A）和Tfb（B）表示树脂P的流动开始温度 ，A和B，并且其中1/2方法温度和流动开始温度由流动器测量。

公开(公告)号：US08592117B2

公开(公告)日：2013-11-26

申请号：US13336318

申请日：2011-12-23

申请人： Tsuyoshi Sugimoto ,  Hiroshi Yamashita ,  Daisuke Asahina ,  Masaki Watanabe ,  Satoyuki Sekiguchi ,  Rintaro Takahashi

发明人： Tsuyoshi Sugimoto ,  Hiroshi Yamashita ,  Daisuke Asahina ,  Masaki Watanabe ,  Satoyuki Sekiguchi ,  Rintaro Takahashi

IPC分类号： G03G9/00

CPC分类号： G03G9/08795 ,  G03G9/0806 ,  G03G9/0812 ,  G03G9/0821 ,  G03G9/08755 ,  G03G9/08782 ,  G03G9/08784 ,  G03G9/08791 ,  G03G9/08797 ,  G03G9/09733

摘要： A toner including: a binder resin component; crystal nucleating agent; releasing agent; and colorant, wherein the binder resin component contains a crystalline polyester resin and a non-crystalline polyester resin, the crystal nucleating agent is at least one of an aliphatic ester compound and an aliphatic amide compound each having a melting point of 60° C. or higher but lower than 150° C., and wherein the toner satisfies Expressions (I) and (II): Tc>Tp+10  Expression (I) Tm>Tp+2  Expression (II) where Tp denotes lowest exothermic peak temperature [° C.] in 0° C. to 200° C. in DSC curve obtained DSC of the crystalline polyester resin, Tc denotes lowest exothermic peak temperature [° C.] in 0° C. to 200° C. in DSC curve obtained DSC of the crystal nucleating agent, and Tm denotes lowest exothermic peak temperature [° C.] in 0° C. to 200° C. in DSC curve through DSC of the mixture of the crystalline polyester resin and the crystal nucleating agent.

摘要翻译： 一种调色剂，包括：粘合剂树脂组分; 晶体成核剂; 脱模剂; 和着色剂，其中所述粘合剂树脂组分含有结晶聚酯树脂和非结晶性聚酯树脂，所述晶体成核剂是分别具有60℃熔点的脂族酯化合物和脂族酰胺化合物中的至少一种，或 高于但低于150℃，并且其中调色剂满足表达式（I）和（II）：Tc> Tp + 10表达式（I）Tm> Tp + 2表达式（II）其中Tp表示最低放热峰温度[℃ ]在0℃〜200℃的DSC曲线中，得到结晶性聚酯树脂的DSC，Tc表示0℃〜200℃的最低放热峰温度[℃]，DSC曲线得到DSC 晶体成核剂，Tm表示在结晶性聚酯树脂和结晶成核剂的混合物的DSC的DSC曲线中，0℃〜200℃的最低放热峰温度[℃]。

公开(公告)号：US08557491B2

公开(公告)日：2013-10-15

申请号：US12509923

申请日：2009-07-27

申请人： Tsuyoshi Sugimoto ,  Naohito Shimota ,  Hiroshi Yamashita ,  Naohiro Watanabe ,  Shinichi Wakamatsu ,  Masaki Watanabe

发明人： Tsuyoshi Sugimoto ,  Naohito Shimota ,  Hiroshi Yamashita ,  Naohiro Watanabe ,  Shinichi Wakamatsu ,  Masaki Watanabe

IPC分类号： G03G9/08

CPC分类号： G03G9/08755 ,  G03G9/0804 ,  G03G9/08795 ,  G03G9/08797 ,  G03G9/09733 ,  G03G9/09791

摘要： A toner according to the present invention contains at least a polyester resin as a binder resin, a colorant, a releasing agent, a fixing-assisting component, and a fatty acid, wherein the fixing-assisting component has a melting point of 60° C. to 120° C. and contains at least one of an esterified compound obtained by esterification of the fatty acid and an amide compound obtained by amidation of the fatty acid.

摘要翻译： 根据本发明的调色剂至少含有作为粘合剂树脂的聚酯树脂，着色剂，脱模剂，定影助剂和脂肪酸，其中定影助剂的熔点为60℃ 至120℃，并且含有通过酯化脂肪酸获得的酯化化合物和通过脂肪酸酰胺化获得的酰胺化合物中的至少一种。

公开(公告)号：US08486596B2

公开(公告)日：2013-07-16

申请号：US12492511

申请日：2009-06-26

申请人： Masaki Watanabe ,  Hiroshi Yamashita ,  Tsuyoshi Sugimoto ,  Naohiro Watanabe ,  Shinichi Wakamatsu

发明人： Masaki Watanabe ,  Hiroshi Yamashita ,  Tsuyoshi Sugimoto ,  Naohiro Watanabe ,  Shinichi Wakamatsu

IPC分类号： G03G9/087

CPC分类号： G03G9/0806 ,  G03G9/0819 ,  G03G9/0825 ,  G03G9/0827 ,  G03G9/08711 ,  G03G9/08755 ,  G03G9/08793 ,  G03G2215/0604 ,  G03G2215/1623 ,  G03G2221/183

摘要： A toner produced by a method including dissolving or dispersing toner components comprising a colorant and at least one of a binder resin and a precursor thereof in an organic solvent to prepare a toner components liquid, dispersing the toner components liquid in an aqueous medium including a surfactant, a particulate resin A having the same polarity as the surfactant and a volume average particle diameter of from 5 to 50 nm, and a particulate resin B having a volume average particle diameter of from 10 to 500 nm to form liquid droplets, and removing the organic solvent from the liquid droplets. The particulate resin B is incompatible with the binder resin and swells in the organic solvent.

摘要翻译： 一种通过包括将包含着色剂和粘合剂树脂及其前体中的至少一种的调色剂组分溶解或分散在有机溶剂中以制备调色剂组分液体的方法制备的调色剂，将调色剂组分液体分散在包含表面活性剂的水性介质中 ，具有与表面活性剂极性相同的体积平均粒径为5〜50nm的粒状树脂A和体积平均粒径为10〜500nm的粒状树脂B形成液滴，除去 来自液滴的有机溶剂。 颗粒状树脂B与粘合剂树脂不相容并在有机溶剂中溶胀。