公开(公告)号：US08829081B2

公开(公告)日：2014-09-09

申请号：US13427361

申请日：2012-03-22

申请人： Hui Chen ,  Ming-Yu Lo ,  Yu-Cheng Kuo

发明人： Hui Chen ,  Ming-Yu Lo ,  Yu-Cheng Kuo

IPC分类号： C08F265/06 ,  C09D183/04 ,  C08G77/20

CPC分类号： C08F265/06 ,  B01J13/18 ,  C08F257/02 ,  C08G77/20 ,  C08L2207/53 ,  C09D183/04 ,  Y10S525/902 ,  C08F2/22

摘要： A method of preparing core-shell submicron spheres is disclosed. The method comprises steps hereafter. An emulsion containing a core monomer is heated to a temperature of 10° C. below its boiling point to the boiling point. A core forming step is performed by adding an initiator solution to the heated emulsion to form cores by polymerizing the core monomer. When the conversion of the above polymerization is 10% to 95%, a shell forming step is performed by adding a shell monomer into the emulsion, at a temperature of 50° C. below the emulsion's boiling point to the boiling point thereof, to form shells, respectively surrounding the cores, by polymerizing the shell monomer.

摘要翻译： 公开了制备核 - 壳亚微米球的方法。 该方法包括以下步骤。 将含有核心单体的乳液加热至低于沸点至10℃的温度。 通过将引发剂溶液加入到加热的乳液中以通过聚合核心单体形成核来进行核心形成步骤。 当上述聚合的转化率为10％至95％时，通过在低于乳液沸点至其沸点的50℃的温度下将壳单体加入到乳液中进行壳形成步骤，以形成 壳，分别围绕芯，通过聚合壳单体。

公开(公告)号：US20130102733A1

公开(公告)日：2013-04-25

申请号：US13427361

申请日：2012-03-22

申请人： Hui Chen ,  Ming-Yu Lo ,  Yu-Cheng Kuo

发明人： Hui Chen ,  Ming-Yu Lo ,  Yu-Cheng Kuo

IPC分类号： C08L33/12 ,  C08L33/26 ,  C08L83/04 ,  C08L41/00

CPC分类号： C08F265/06 ,  B01J13/18 ,  C08F257/02 ,  C08G77/20 ,  C08L2207/53 ,  C09D183/04 ,  Y10S525/902 ,  C08F2/22

摘要： A method of preparing core-shell submicron spheres is disclosed. The method comprises steps hereafter. An emulsion containing a core monomer is heated to a temperature of 10° C. below its boiling point to the boiling point. A core forming step is performed by adding an initiator solution to the heated emulsion to form cores by polymerizing the core monomer. When the conversion of the above polymerization is 10% to 95%, a shell forming step is performed by adding a shell monomer into the emulsion, at a temperature of 50° C. below the emulsion's boiling point to the boiling point thereof, to form shells, respectively surrounding the cores, by polymerizing the shell monomer.

摘要翻译： 公开了制备核 - 壳亚微米球的方法。 该方法包括以下步骤。 将含有核心单体的乳液加热至低于沸点至10℃的温度。 通过将引发剂溶液加入到加热的乳液中以通过聚合核心单体形成核来进行核心形成步骤。 当上述聚合的转化率为10％至95％时，通过在低于乳液沸点至其沸点的50℃的温度下将壳单体加入到乳液中进行壳形成步骤，以形成 壳，分别围绕芯，通过聚合壳单体。